综述了纳米二硫化钼材料的几种主要制备方法:高温硫化法、前驱体分解法、水热法、溶液法和表面活性剂促助法,着重阐述了各种制备方法的研究现状及优缺点,并对纳米二硫化钼的制备方法进行了展望,认为表面活性剂促助法最具有发展潜力.
参考文献
[1] | Ogilvy J A .Predicting the friction and durability of MoS2coating using a numerical contact model[J].Wear,1993,160:171. |
[2] | Takur D S;Delmon B .The role of group Ⅷ metal promoter in MoS2and WS2 hydrotreating catalysts[J].Journal of Catalysis,1985,91:308. |
[3] | Tributac H;Faraday D .Photoelectrochemiatry of layer-typezirconium disulfide[J].Journal of the Electrochemical Society,1981,128:1261. |
[4] | Golub AS.;Slovokhotov YL.;Novikov YN.;Danot M.;Zubavichus YV. .Layered compounds assembled from molybdenum disulfide single-layers and alkylammonium cations[J].Solid state ionics,2000(1/4):151-160. |
[5] | Peter W E .Thermoplastic elastomer-containing bitumen and asphat modifiers and their manufacture[P].US 5393819,1993. |
[6] | Huggins G E .Flyropolymer surface coated products[P].US 5262241,1995. |
[7] | Muijsers J C;Weber T;Vanhardeveld R M et al.Sulfidation study of molybdenum oxide using MoO3/SiO2/Si (100) model catalysts and Mo-3IV-sulfur cluster compounds[J].Journal of Catalysis,1995,157:698. |
[8] | Feldman Y;Wasserman E;Srolovitz DJ;Tenne R .HIGH-RATE, GAS-PHASE GROWTH OF MOS2 NESTED INORGANIC FULLERENES AND NANOTUBES[J].Science,1995(5195):222-225. |
[9] | 高宾,许启明,赵鹏,姚燕燕,田晓珍.化学气相反应合成MoS2纳米管的研究[J].功能材料与器件学报,2006(02):143-146. |
[10] | Eggertsen F T;Roberts R M .Molybdenum disulfide of high surface area[J].Journal of the American Chemical Society,1959,63:1981. |
[11] | Brito JL.;Hernandez P.;Ilija M. .THERMAL AND REDUCTIVE DECOMPOSITION OF AMMONIUM THIOMOLYBDATES[J].Thermochimica Acta: An International Journal Concerned with the Broader Aspects of Thermochemistry and Its Applications to Chemical Problems,1995(2):325-338. |
[12] | Afanasiev P;Bezverkhyy I .Ternary transition metals sulfides in hydrotreating catalysis[J].Applied Catalysis,2007,322:129. |
[13] | Walton RI.;Hibble SJ.;Dent AJ. .In situ investigation of the thermal decomposition of ammonium tetrathiomolybdate using combined time-resolved X-ray absorption spectroscopy and X-ray diffraction[J].Chemistry of Materials,1998(11):3737-3745. |
[14] | Genuit D;Afanasiev P;Vrinat M .Solution syntheses of unsupported Co(Ni)-Mo-S hydrotreating catalysts[J].Journal of Catalysis,2005,235:302. |
[15] | Muller A;Diemann E;Branding A et al.New method for the preparation of hydrodesulphurization catalysts:Use of the molybdenum sulphur cluster compound (NH4)2[Mo3IV S13][J].Applied Catalysis,1990,62:L13. |
[16] | Leist A.;Loken S.;Finckh EW.;Ludtke S.;Unger KK. Assenmacher W.;Mader W.;Tremel W.;Stauf S. .Semiporous MoS2 obtained by the decomposition of thiomolybdate precursors[J].Journal of Materials Chemistry: An Interdisciplinary Journal dealing with Synthesis, Structures, Properties and Applications of Materials, Particulary Those Associated with Advanced Technology,1998(1):241-244. |
[17] | Afanasiev P .Synthetic approaches to the molybdenum sulfide materials[J].Comptes Rendus Chimie,2008,11:159. |
[18] | Devers E.;Afanasiev P.;Jouguet B.;Vrinat M. .Hydrothermal syntheses and catalytic properties of dispersed molybdenum sulfides[J].Catalysis Letters,2002(1/2):13-17. |
[19] | Peng Y Y;Meng Z Y;Zhong C et al.Hydrothermal Synthesis of MoS2 and its pressure-related crystallization[J].Journal of Solid State Chemistry,2001,159:170. |
[20] | Bokhimi X;Toledo J A et al.Thermal evolution in air and argon of nanocrystalline MoS2synthesized under hydrothermal conditions[J].International Journal of Hydrogen Energy,2001,26:1271. |
[21] | Tian Y;He Y;Zhu YF .Low temperature synthesis and characterization of molybdenum disulfide nanotubes and nanorods[J].Materials Chemistry and Physics,2004(1):87-90. |
[22] | Li W J;Shi E W;Ko J M et al.Hydrothermal synthesis of MoS2 nanowires[J].Journal of Crystal Growth,2003,250:418. |
[23] | Li Q;Li M;Chen Z et al.Simple solution route to uniform MoS2particles with randomly stacked layers[J].Materials Research Bulletin,2004,39:981. |
[24] | Peng YY.;Meng ZY.;Zhong C.;Lu J.;Yang ZP.;Qian YT. .Tube- and ball-like amorphous MoS2 prepared by a solvothermal method[J].Materials Chemistry and Physics,2002(2/3):327-329. |
[25] | 田野,何俣,朱永法,王威.MoS2的水热合成及其润滑性能[J].物理化学学报,2003(11):1044-1048. |
[26] | 田野,何俣,尚静,朱永法.水热法合成MOS2层状材料及其结构表征[J].化学学报,2004(18):1807-1810. |
[27] | Bezverkhy I.;Lacroix M.;Afanasiev P. .Aqueous preparation of highly dispersed molybdenum sulfide[J].Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics,2000(24):5416-5417. |
[28] | Bezverkhy I;Afanasiev P;Geantet C et al.Highly active (Co)MoS2/Al2O3 hydrodesulfurization catalysts prepared in aqueous solution[J].Journal of Catalysis,2001,204:495. |
[29] | Bezverkhy I;Afanasiev P;Lacroix M .Promotion of highly loaded MoS2/Al2 O3 hydrodesulfurization catalysts prepared in aqueous solution[J].Journal of Catalysis,2005,230:133. |
[30] | Afanasiev P;Geantet C;Thomazeau C et al.Molybdenum polysulfide hollow microtubules grown at room temperature from solution[J].Chemical Communications,2000,12:1001. |
[31] | Afanasiev P;Bezverkhy L .Genesis of vesicle-like and tubular morphologies in inorganic precipitates:Amorphous Mo oxysulfides[J].Journal of Physical Chemistry B,2003,107:2678. |
[32] | Liao HW.;Zhang SY.;Qian YT.;Wang YF. .A solution low-temperature route to MoS2 fiber[J].Chemistry of Materials,2001(1):6-8. |
[33] | Tian Y M;Zhao J Z;Fu W Y et al.A facile route to synthesis of MoS2 nanorods[J].Materials Letters,2005,59:3452. |
[34] | 胡献国,沃恒洲,胡坤宏,韩效钊.用硫化钠制备二硫化钼纳米颗粒[J].机械工程材料,2004(01):32-34. |
[35] | Afanasiev P;Xia G F;Berhault G et al.Surfactant-assisted synthesis of highly dispersed molybdenum sulfide[J].CHEMISTRY OF MATERIALS,1999,11:3216. |
[36] | Genuit D;Bezverkhyy I;Afanasiev P .Solution preparation of the amorphous molybdenum oxysulfide MoOS2 and its use for catalysis[J].International Journal of Quantum Chemistry,2005(9):2759-2765. |
[37] | Xiong YJ.;Xie Y.;Li ZQ.;Li XX.;Zhang R. .Micelle-assisted fabrication of necklace-shaped assembly of inorganic fullerene-like molybdenum disulfide nanospheres[J].Chemical Physics Letters,2003(1/2):180-185. |
[38] | Bezverkhyy I;Afanasiev P;Lacriox M .Preparation and chemical transformation of surfactant-templated hybrid phase containing[MoS42-anions[J].Materials Research Bulletin,2002,37:161. |
[39] | Trikalities P N;Kerr T A;Kanatzidis M G .Mesostructured cobalt and nickel molybdenum sulfides[J].Microporous and Mesoporous Materials,2005,88:187. |
[40] | Albu-Yaron A;Levy-Clement C;Hutchison J L .A study on MoS2 thin films electrochemically deposited in ethylene glycol at 165℃[J].Electrochemical and Solid-State Letters,1999,2:627. |
[41] | Catherine M Z;Peter K D .Template synthesis of near-monodisperse microscale nanofibers and nanotubules of MoS2[J].Journal of the American Chemical Society,1998,120:734. |
[42] | Zheng XW.;Zhu LY.;Yan AH.;Bai CN.;Xie Y. .Ultrasound-assisted cracking process to prepare MoS2 nanorods[J].Ultrasonics sonochemistry,2004(2):83-88. |
[43] | Chu G S;Bian G Z;Fu Y L et al.Preparation and structural characterization of nano-sized amorphous powders of MoS2 by,γ-irradiation method[J].Materials Letters,2000,43:81. |
[44] | Afanasiev P.;Rawas L.;Vrinat M. .Synthesis of dispersed Mo sulfides in the reactive fluxes containing liquid sulfur and alkali metal carbonates[J].Materials Chemistry and Physics,2002(2/3):295-300. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%