借助于SEM和TEM研究了Al-TiO2-B2O3系热扩散反应法合成铝基复合材料的界面结构. 结果表明:在B2O3与TiO2摩尔比小于1时,增强相由棒状的Al3Ti及颗粒状的TiB2和α-Al2O3组成. Al3Ti与基体的界面干净、相容性好,在基体中分布均匀;TiB2与铝基体界面干净,并存在以下位向关系:[231]Al∥[0001]TiB2, (204)Al∥(2420)TiB2,可成为基体结晶时的核心,细化基体晶粒;α-Al2O3与铝基体的润湿性差,被推挤到基体颗粒的界面呈偏聚状态,并存有孪晶现象,其孪晶面为(111),孪生方向为[112 ].
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