采用水热法,以Pb(NO3)2和K2S2O8为原料,十二烷基苯磺酸钠(SDBS)为表面活性剂,在碱性溶液中制备纯相的β-PbO2微米球.利用粉末X射线衍射仪(XRD)和扫描电子显微镜(SEM)对所得产物进行分析表征,并考察表面活性剂对其形貌的影响.以聚乙烯吡咯烷酮(PVP)为表面活性剂时可得到微米空球.
参考文献
| [1] | Cattarin S.;Guerriero P.;Musiani M.;Frateur I. .Electrodeposition of PbO2+CoOx composites by simultaneous oxidation of Pb2+ and Co2+ and their use as anodes for O-2 evolution[J].Electrochimica Acta,2000(14):2279-2288. |
| [2] | Lee Jaeyoung et al.[J].Electrochemistry Communications,2000,2(09):646. |
| [3] | Kuhn A T.The electrochemistry of Lead[M].London,UK:Academic Press,1979:22. |
| [4] | Pohl J P.Electrodes of conductive metal oxides,Part A[M].Amsterdam:Elsevier Science,1980:183. |
| [5] | Ellis S R;Hampson N A;Ball M C et al.[J].Journal of Applied Electrochemistry,1986,16(02):159. |
| [6] | Burbank J;Simon A C;Willihnganz E.Advances in electrochemistry and electrochemistry engineering[M].New York:Wiley-Interscience,1971:88. |
| [7] | 董占能,张皓东,张召述.云南湿法磷酸化学沉淀法脱氟研究[J].昆明理工大学学报(理工版),2003(06):96-98. |
| [8] | 龚良玉,曹艳霞,刘海东.低热固相氧化反应合成二氧化铅纳米片[J].无机盐工业,2008(10):21-22,25. |
| [9] | 庄京,邓兆祥,梁家和,李亚栋.β-PbO2纳米棒及Pb3O4纳米晶的制备与表征[J].高等学校化学学报,2002(07):1223-1226. |
| [10] | Xi Guangcheng;Peng Yiya;Xu Liqiang et al.[J].Inorganic Chemistry Communications,2004,7(05):607. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%