Yttrium aluminum garnet (Y3Al5O12) nanopowders synthesized by the chemical method

稀有金属（英文版）, 2005, 24(2): 166-184.

^1, , ^2, , ^3, , ^4, , ^5,

1.School of Materials, Changchun University of Science and Technology, Chuangchun 130022, China

2.School of Materials, Changchun University of Science and Technology, Chuangchun 130022, China

3.The First Research Laboratory, China North Vehicle Research Institute, Beijing 10072, China

4.School of Materials, Changchun University of Science and Technology, Chuangchun 130022, China

5.School of Materials, Changchun University of Science and Technology, Chuangchun 130022, China

基金项目: 教育部高校优秀青年教师资助计划(KB200226)

Yttrium aluminum garnet (Y3Al5O12) nanopowders synthesized by the chemical method

Keywords： inorganic materials

The homogeneously dispersed, less agglomerated YAG nanopowders are synthesized by the citrate-gel method followed by low-temperature self-propagating combustion reaction, using Y2O3, Al(NO3)y9H2O and citric acid as starting materials. This method effectively solves the problems caused by solid-state reaction at high temperature and the hard agglomerates brought by the chemical precipitation method. The powders are characterized by TG-DTA, XRD, FT-IR and TEM respectively. The experiments show that the forming temperature of YAG crystal phase is 850℃ and the pseudo-YAG crystalline appears during the calcination and transforms to pure YAG at 1050℃. The powders with sizes less than 50 nm are observed by TEM micrography, which is consistent with the result calculated by Scherrer's formula. The powders consist of single grains.

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Yttrium aluminum garnet (Y3Al5O12) nanopowders synthesized by the chemical method

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