本文主要研究了在Nd-Fe-B烧结磁体晶界上添加WC对显微组织和磁性能的影响实验结果表明,添加少量WC时,随WC含量的增加,晶粒逐渐变细,矫顽力也逐渐升高,并且在0.6%处晶粒最细,而矫顽力则出现峰值。进一步增加WC的含量,晶粒又开始粗化,并伴随着矫顽力的下降。扫描电镜的观察显示,加WC的磁体中主相晶界和晶界附近的主相晶内出现了一些杆状相.能谱分析表明,该相为W-Fe-B相,在此化合物附近区域和晶界处的C和W含量高于其它基体区域.
The coercivity of sintered Nd-Fe-B magnets is enhanced by the addition of a small amount of WC and the highest one corresponds to an amount of 0.6% WC addition. But a higher amount of WC addition leads to the decrease in coercivity. The grain size decreases first and then increases with increasing the WC content. SEM observation revealed that W-Fe-B phase with colony-like shape appears at grain boundaries or in some matrix regions, and that the contents of C and W in the regions near to W-Fe-B phase are higher than other regions. Correspondent: SONG Xiaoping,(College of Materials Science, Xi'an Jiaotong University, Xi'an 710049)
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