分别以氯化镉、草酸镉、碳酸镉、柠檬酸镉和钨酸钠为原料,在没有采用模板和表面活性剂的条件下,采用水热法可控制备出了钨酸镉纳米颗粒、纳米棒、纳米束和纳米线.利用X射线衍射(XRD)、透射电镜(TEM)、高分辨透射电子显微镜(HRTEM)和选区电子衍射(SAED)对样品进行了表征.结果表明:[WO42-]/[Cd2+]摩尔比、反应时间及先驱体的类型对产物的形貌和尺寸有着重要的影响.
参考文献
| [1] | Rzhevskaya OV;Spasskii DA;Kolobanov VN;Mikhailin VV;Nagornaya LL;Tupitsina IA;Zadneprovskii BI .Optical and luminescence properties of CdWO4 and CdWO4 : Mo single crystals[J].Optics and Spectroscopy,2008(3):366-373. |
| [2] | 周英智,刘峥,袁帅.脉冲电沉积结合水热法制备ZnS纳米条及其光学性质的研究[J].人工晶体学报,2012(05):1381-1385. |
| [3] | A. Mano Priya;R. Kalai Selvan;B. Senthilkumar .Synthesis and characterization of CdWO_4 nanocrystals[J].CERAMICS INTERNATIONAL,2011(7):2485-2488. |
| [4] | Wang YG;Ma JF;Tao JT;Zhu XY;Zhou J;Zhao ZQ;Xie LJ;Tian H .Morphology-controlled synthesis of CdWO4 nanorods and nanoparticles via a molten salt method[J].Materials Science & Engineering, B. Solid-State Materials for Advanced Technology,2006(1/3):277-281. |
| [5] | Ye, D;Li, DZ;Chen, W;Shao, Y;Xiao, GC;Sun, M;Fu, XZ .Characterization and properties of Eu3+-doped CdWO4 prepared by a hydrothermal method[J].Research on Chemical Intermediates,2009(6/7):675-683. |
| [6] | Wenming Tong;Liping Li;Wanbiao Hu .Systematic Control of Monoclinic CdWO4 Nanophase for Optimum Photocatalytic Activity[J].The journal of physical chemistry, C. Nanomaterials and interfaces,2010(3):1512-1519. |
| [7] | Wang HL;Ma XD;Qian XF;Yin J;Zhu ZK .Selective synthesis of CdWO4 short nanorods and nanofibers and their self-assembly[J].International Journal of Quantum Chemistry,2004(12):4588-4596. |
| [8] | Gang Xu;Zhaohui Ren;Piyi Du;Wenjian Weng;Ge Shen;Gaorong Han .Polymer-Assisted Hydrothermal Synthesis of Single-Crystalline Tetragonal Perovskite PbZr_(0.52)Ti_(0.48)O_3 Nanowires[J].Advanced Materials,2005(7):907-910. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%