欢迎登录材料期刊网

材料期刊网

高级检索

对双氧水行业含钯废催化剂的回收工艺作了研究。采用湿法工艺分两步实现了钯的高效富集,富集物精炼得到99.95%的钯粉,全流程钯的回收率为98.66%。此外,对取样、除有机物、渣的处理等关键过程做了讨论,提出了优化的工艺流程。

The recovery process of palladium from spent hydrogen peroxide industry catalyst was investigated. By two steps hydrometallurgy process to achieve the enrichment of palladium, the enrichment was refined to obtain high purity palladium powder; the whole process of recovery was 98.66%. In addition, the key process was discussed, including sampling, remove organics and residue treatment, the optimized process was proposed on this basis.

参考文献

[1] 刘昭维 .蒽醌法双氧水生产工艺改进及35%双氧水生产技术研究[D].华东理工大学,2012.
[2] 李泽江.我国双氧水生产技术与市场分析[J].精细与专用化学品,2010(11):1-5.
[3] 王玉强.双氧水的应用及其工艺进展[J].广东化工,2006(01):45-46.
[4] 陈韡.浅析蒽醌法生产双氧水氢化工序[J].化学推进剂与高分子材料,2012(04):94-96.
[5] 陈冠群,周涛,曾平,葛志强.蒽醌法生产双氧水的研究进展[J].化学工业与工程,2006(06):550-555,561.
[6] 史宗民.钯触媒在葸醌法生产双氧水的应用[J].中国氯碱,2011(10):43-45.
[7] 沈秀凯.蒽醌法双氧水生产中钯催化剂的使用[J].中国氯碱,2007(04):43-45.
[8] 刘向来.双氧水生产中钯催化剂的使用若干问题的探讨[J].无机盐工业,2009(04):43-46.
[9] 贺小塘,郭俊梅,王欢,李勇,吴喜龙,赵雨,韩守礼,李锟,谭文进,刘文.中国的铂族金属二次资源及其回收产业化实践[J].贵金属,2013(02):82-89.
[10] GUO Junmei,HE Xiaotang,WANG Huan,WU Xilong,ZHAO Yu,LI Yong,LI Kun,HAN Shouli.Reviews of Metallurgical Technology to Recovery Platinum Group Metals from Secondary Resource in China[J].贵金属,2012(z1):18-23.
[11] 贺小塘;韩守礼;王欢 等.一种从废催化剂中回收贵金属的方法[P].中国,201310214870.4,2013-06-03.
[12] 从Pd/C废料中回收钯及制备试剂PdCl2的新工艺[J].贵金属,2012(04):9-13.
[13] 杨茂才;孙萼庭;周扬霁 .从废铝基催化剂回收贵金属及铝的方法和消化炉[P].中国,CN95109350.9,1995-08-23.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%