利用原位反应自发渗透技术制备了组织均匀且致密度高的TiCp/Mg复合材料, 研究了原位反应温度以及碳颗粒尺寸对制备的TiCp/Mg复合材料微观组织的影响.结果表明: 当使用大尺寸碳粒子(≤100μm)时, 随着反应温度的提高, 原位生成物TiCp的含量增加, 但有残留反应物Ti和C的存在; 碳粒子尺寸减小(≤30μm)时, 原位反应较完全, 不再有残留物存在; 原位反应产物组织中, 增强相TiCp主要呈互穿网络状、颗粒状以及片状等形态; 增强相的尺寸随碳粒子尺寸的减小而减小, 在碳颗粒尺寸为1.5μm时TiC更易呈现等轴颗粒状, 尺寸约为0.5~2.0μm.
参考文献
[1] | 李荣华,黄继华,殷声.镁基复合材料研究现状与展望[J].材料导报,2002(08):17-19. |
[2] | 李荣华,黄继华,殷声.镁基复合材料研究现状与展望[J].材料导报,2002(08):17-19. |
[3] | Hryn J N.Magnesium Technology 2001Warrendale[M].PA,2001:TMS. |
[4] | D. W. Lee;B. K. Kim .Synthesis of nano-structured titanium carbide by Mg-thermal reduction[J].Scripta materialia,2003(11):1513-1518. |
[5] | 李劲风,张昭,张鉴清.金属基复合材料(MMCs)的原位制备[J].材料科学与工程,2002(03):453-456,392. |
[6] | LI Jin-feng;ZHANG Zhao;ZHANG Jian-qing .In situ fabrication of metal matrix composites[J].材料科学与工程学报,2002,20(03):453-456. |
[7] | Q. Dong;L. Q. Chen;M. J. Zhao .Synthesis of TiCp reinforced magnesium matrix composites by in situ reactive infiltration process[J].Materials Letters,2004(6):920-926. |
[8] | 陈礼清,董群,赵明久,毕敬.原位反应渗透法TiCp/Mg复合材料的制备和性能[J].材料研究学报,2004(02):193-198. |
[9] | 陈礼清,董群,赵明久,毕敬.原位反应渗透法TiCp/Mg复合材料的制备和性能[J].材料研究学报,2004(02):193-198. |
[10] | Qun Dong,Liqing CHEN,Mingjiu ZHAO,Jing BI.Analysis of in situ Reaction and Pressureless Infiltration Process in Fabricating TiC/Mg Composites[J].材料科学技术学报(英文版),2004(01):3-7. |
[11] | AGHAJANIAN M K;Burke J T;White D R et al.A new infiltration process for the fabrication of metal matrix composites[J].SAMPE Quarterly,1989,20(04):43-46. |
[12] | AGHAJANIAN M K;Rocazella M A;Burke J T et al.The fabrication of metal matrix composites by a pressureless infiltration technique[J].Journal of Materials Science,1991,26:447-454. |
[13] | Lee K B;Sim H S;Cho S Y .Reaction products of Al-Mg/B4C composite fabricated by pressureless infiltration technique[J].Materials Science and Engineering A,2001,A302:227-234. |
[14] | KON BAE LEE;JAE PYOUNG AHN;HOON KWON .Characteristics of AA6061/BN Composite Fabricated by Pressureless Infiltration Technique[J].Metallurgical and Materials Transactions, A. Physical Metallurgy and Materials Science,2001(4):1007-1018. |
[15] | 边涛,潘颐,崔岩,益小苏.金属基复合材料的自发浸渗制备工艺[J].材料导报,2002(01):21-24. |
[16] | 边涛,潘颐,崔岩,益小苏.金属基复合材料的自发浸渗制备工艺[J].材料导报,2002(01):21-24. |
[17] | 郝元恺;赵恂;杨盛良 等.纯镁对碳化硼颗粒的常压浸渗[J].复合材料学报,1995,12(03):12-16. |
[18] | HAO Yuan-kai;ZHAO Xun;YANG Sheng-liang et al.Investigation of normal pressure infiltration of pure magnesium into boron carbide particle[J].复合材料学报,1995,12(03):12-16. |
[19] | Tjong SC.;Ma ZY. .Microstructural and mechanical characteristics of in situ metal matrix composites [Review][J].Materials Science & Engineering, R. Reports: A Review Journal,2000(3/4):49-113. |
[20] | 李青,华文君,崔岩,张少卿.无压浸渗法制备B4C/Al复合材料研究[J].材料工程,2003(04):17-20. |
[21] | 李青,华文君,崔岩,张少卿.无压浸渗法制备B4C/Al复合材料研究[J].材料工程,2003(04):17-20. |
[22] | B. SRINIVASA RAO;V. JAYARAM .PRESSURELESS INFILTRATION OF Al-Mg BASED ALLOYS INTO Al_2O_3 PREFORMS: MECHANISMS AND PHENOMENOLOGY[J].Acta materialia,2001(13):2373-2385. |
[23] | A. Contreras;C. A. Leon;R. A. L. Drew;E. Bedolla .Wettability and spreading kinetics of Al and Mg on TiC[J].Scripta materialia,2003(12):1625-1630. |
[24] | Delannay F;Froyen L;Deruyttere A .Review-the wetting of solids by molten metals and its relation to the preparation of metal-matrix composites[J].Journal of Materials Science,1987,22:1-16. |
[25] | Munir Z A;Tamburini U A .Self-propagating exothermic reactions: the synthesis of high temperature materials by combustion[J].Materials Science Reports,1989,3(7-8):227-358. |
[26] | Lu W J;Zhang D;Zhang X N .Growth mechanism of reinforcement in in situ processed (TiB+TiC)/Ti composites[J].Transactions of Nonferrous Metals Society of China,2001,11(01):67-71. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%