以9,10-双蒽酸(H2L)和2,6-二甲基吡啶(Hdmpy)为配体,合成了一个二维结构的稀土配合物{[Tb(L)2(H2O)2] (Hdmpy) (H2O)2｝∞；用原位聚合法将该稀土配合物与丙烯酸类聚氨酯大分子单体复合,制备出{[Tb(L)2(H2O)2](Hdmpy)(H2O)2｝∞/丙烯酸酯类聚氨酯稀土高分子材料,并研究了稀土配合物在材料中的分散及材料的热稳定性、荧光性能等.研究结果表明,配合物在稀土高分子材料中主要以200～500nm颗粒均匀分散；且该材料具有良好的热稳定性能(＞300℃),在波长372nm的激发光下,材料在440nm出现最大荧光发射峰,有望应用于发光材料领域.
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