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采用低温水溶液法合成三水碳酸镁晶须,考查了反应温度、反应时间、表面活性剂用量及反应溶液初始pH等因素对三水碳酸镁晶须的长度及长径比的影响.研究结果表明:在反应温度45~50℃、反应时间50~60 min、表面活性剂添加量(质量分数)为1%、反应溶液初始pH =9.5的条件下,可以合成出高长径比三水碳酸镁晶须产品.

参考文献

[1] Freitag F;Kleinebudde P How Roll .Compaction and Dry Granulation Affect the Tableting Behaviour of Inorganic Materials:Comparison of Four Magnesium Carbonates[J].European Journal of Pharmical Sciences,2003,19:281-289.
[2] A. Botha;C. A. Strydom .Preparation of a magnesium hydroxy carbonate from magnesium hydroxide[J].Hydrometallurgy,2001(3):175-183.
[3] Kloprogge J T;Martens W N;Nothdurft L et al.Low Temperature Synthesis and Characterization of Nesquehonite[J].Journal of Materials Science,2003,22(1 1):825-829.
[4] Mitsuhashi K;Tagami N;Tanabe K;Ohkubo T;Sakai H;Koishi M;Abe M .Synthesis of microtubes with a surface of "house of cards" structure via needlelike particles and control of their pore size[J].Langmuir: The ACS Journal of Surfaces and Colloids,2005(8):3659-3663.
[5] 三觜幸平;田迈克幸;田上直树 .碱式碳酸镁及其制备方法和用途[P].国际专利申请:PCT/JP2003/001437,2003-2-12.
[6] Wang W P;Zhang Y .Preparation of Magnesia Whisker by the Pyrolysls of Magnesium Carbonate[J].Journal of the Chinese Ceraric Sociay,2002,30(z1):93-95.
[7] X. Wang;D. Xue .Direct observation of the shape evolution of MgO whiskers in a solution system[J].Materials Letters,2006(25/26):3160-3164.
[8] 邵平平,李志宝,密建国.碳酸镁水合物在283-363 K范围内的晶体组成及晶型[J].过程工程学报,2009(03):520-525.
[9] Chen M;Li Y Y;Wang J D et al.Preparation of Magnesium Carbonate Whiskers by Magmesite[J].Jourrnl of the Chinese Ceramic Society,2009,37(10):1649-1653.
[10] Coleyshaw EE.;Crump G.;Griffith WP. .Vibrational spectra of the hydrated carbonate minerals ikaite, monohydrocalcite, lansfordite and nesquehonite[J].Spectrochimica acta, Part A. Molecular and biomolecular spectroscopy,2003(10):2231-2239.
[11] GiesterG;GengauerC L;Rieek B .The Crystal Strueture of Nesquehonite,MgCO3 @ 3H2O,from Lavrion,Greeee[J].Mineralogy and Petrology,2000,70(3-4):153-163.
[12] 闫小星,李云飞,薛冬峰,晏成林,王雷.基于水合碳酸镁结晶过程的化学键分析[J].人工晶体学报,2007(05):991-999.
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