采用红外热波成像技术分别对二维叠层C/SiC(2D C/SiC)复合材料的无SiC涂层盲孔试样和有SiC涂层的三点弯曲强度试样的氧化损伤进行无损检测。分析了材料氧化损伤与热辐射强度信号之间的关系,以及热扩散系数与材料密度、抗弯强度之间的关系,探索了采用红外热波成像检测和评价2D C/SiC氧化损伤的可行性。检测结果表明:红外热波成像可以直观地反映2D C/SiC复合材料的氧化损伤。2D C/SiC氧化后的密度随热扩散系数的减小呈对数降低,其抗弯强度随热扩散系数的减小呈抛物线降低。由此得出,热扩散系数可以作为衡量陶瓷基复合材料的氧化损伤程度的依据,红外热波成像是一种无损检测陶瓷基复合材料氧化损伤的有效方法。
In order to explore the feasibility for testing and evaluating oxidative damages in 2D C/SiC composite by thermography,the oxidative damages of 2D C/SiC samples with a blind hole without SiC coatings and three point bending 2D C/SiC samples with SiC coatings were investigated by means of thermography.The relationship between the thermography signal and the oxidative damage was analyzed,and the relationship between the thermal diffusivity and the density as well as the relationship between the thermal diffusivity and the bending strength were established.The results show that the oxidative damage can be visually recognized by thermography.The density of C/SiC logarithmically reduces with the decrease of the thermal diffusivity,and the bending strength parabolically decrease with the decrease of thermal diffusivity.The thermal diffusivity can measure the degree of oxidative damages of the ceramic matrix composite and thermography is an effective method of non-destructive testing of oxidation damage in the ceramic matrix composite.
参考文献
[1] | Berton B, Bacos M P, Demange D, et al. High temperature behavior of the hot structure of Hermes Space Shuttle [M]/ / Naslain R, Lamalle J, Zulian J L. Composite Materials for High Temperature Applications. Paris: AMAC, 1990: 315-325. |
[2] | Calalier J C, Lacombe A, Rouges J M. Ceramic matrix composites, new high performance materials [M]/ / Bunsell A R, Lanicq P, Massiah A. The Development in the Science and Technology of Composite Materials. UK, 1989: 99-110. |
[3] | Aparicio M, Duran A. Infiltration of C/SiC composites with silica sol-gel solutions, Part Ⅰ : Infiltration by dipping [J]. J Mater Res, 1999, 14(11): 4230-4238. |
[4] | Aparicio M, Duran A. Infiltration of C/SiC composites with silica sol-gel solutions, Part Ⅱ : Infiltration under isostatic pressure and oxidation resistance [J]. J Mater Res, 1999, 14(11): 4239-4245. |
[5] | Cheng L F, Xu Y D, Zhang L T, et al. Oxidation behavior of three dimension C/SiC composites in air and combustion gas environment [J]. Carbon, 2000, 38: 2103-2108. |
[6] | Cheng L F, Xu Y D, Zhang L T, et al. Effect of carbon interlayer on oxidation behavior of C/SiC composites with a coating from room temperature to 1500 ℃ [J]. Material Science and Engineering A, 2001, 300(12): 219-222. |
[7] | Lamourou F, Bourra X, Naslain R, et al. Structure/oxidation behavior relationship in the carbonaceous constituents of 2D C/PyC/SiC composites [J]. Carbon, 1993, 31(8): 1273-1288. |
[8] | Lamourou F, Camus G. Oxidation effects on the mechanical properties of 2D woven C/SiC composites [J]. J Euro Ceram Soc, 1994, 14(2): 177-188. |
[9] | Naslain R, Guette A, Rebillat F, et al. Oxidation mechanisms and kinetics of SiC matrix composites and their constituents [J]. J Mater Sci, 2004, 39(24): 7303-7316. |
[10] | 殷小玮. 3D C/SiC复合材料的环境氧化行为[D]. 西安: 西北工业大学, 2001: 21-22. |
[11] | Lamouroux F, Camus G. Kinetics and mechanisms of oxidation of 2D woven C/SiC composites Ⅰ : Experimental approach [J]. J Am Ceram Soc, 1994, 77(8): 2049-2057. |
[12] | Xu Y D, Cheng L F, Zhang L T, et al. Oxidation behavior and mechanical properties of C/SiC composites with Si-MoSi2 oxidation protection coating [J]. J Mater Sci, 1999, 34: 6009-6014. |
[13] | Sun J G, Deemer C M, Ellingson W A, et al. NDT technologies for ceramic matrix composites: Oxide and nonoxide [J]. Mater Eval, 2006, 64(1): 52-60. |
[14] | Sun J G. Analysis of pulsed thermography methods for detects depth prediction [J]. Journal of Heat Transfer, 2006, 128(4): 329-338. |
[15] | Sun J G, Verrilli M J, Stephan R, et al. Nondestructive evaluation of ceramic matrix composite combustor components: NASA/TM-2003-212014 . 2003. |
[16] | Sun J G. Evaluation of ceramic matrix composites by thermal diffusivity imaging [J]. J Appl Ceram Technol, 2007, 4(1): 75-87. |
[17] | 孙磊, 张立同, 梅辉, 等. 2D C/SiC缺陷的无损检测与评价[J]. 复合材料学报, 2008, 25(5): 85-90. |
[18] | 邓晓东, 成来飞, 梅辉, 等. C/SiC 复合材料的定量红外热波无损检测[J]. 复合材料学报, 2009, 26(5): 112-119. |
[19] | 张青. C/SiC复合材料热物理性能与微结构表征[D]. 西安: 西北工业大学, 2008: 21-23. |
[20] | Glime W H, Cawley J D. Oxidation of carbon fibers and films in ceramic matrix composites: A weak link process [J]. Carbon, 1995, 33(8): 1053-1060. |
[21] | Tawil H, Bentsen L D, Baskaran S, et al. Thermal diffusivity of chemically vapor deposited silicon carbide reinforced with silicon carbide or carbon fibers [J]. J Mater Sci, 1985, 20: 3201-3212. |
[22] | Bhatt H, Donaldson K Y, Hasselman D P Ⅱ , et al. Role of interfacial carbon layer in the thermal diffusivity/conductivity of silicon carbide fiber-reinforced reaction-bonded silicon nitride matrix composites [J]. J Am Ceram Soc, 1992, 75(2): 334-340. |
[23] | Hasselman D P Ⅱ , Johnson L F. Effective thermal conductivity of composites with interfacial thermal barrier resistance [J]. J Compos Mater, 1987, 21: 508-514. |
[24] | Benveniste Y. Effective thermal conductivity of composites with a thermal contact resistance between the constituents: Non-dilute case [J]. J Appl Phys, 1987, 61(8): 2840-2843. |
[25] | Chiew Y C, Glandt E D. Effective conductivity of dispersions: The effect of resistance at the particle surfaces [J]. Chem Eng Sci, 1987, 42(11): 2677-2685. |
[26] | Yamada R, Igawa N, Taguchi T, et al. Highly thermal conductive, sintered SiC fiber-reinforced 3D-SiC/SiC composites: Experiments and finite-element analysis of the thermal diffusivity/conductivity [J]. Journal of Nuclear Materials, 2002, 307/311(2): 1215-1220. |
[27] | 李建章, 张立同, 成来飞, 等. 高温氧化气氛下3D C/SiC质量变化率与剩余强度的相关性[J]. 复合材料学报, 2007, 24(4): 101-105. |
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