通过测定热膨胀系数研究了热处理工艺对NiTi合金负热膨胀(NTE)行为的影响,并采用XRD和TEM分析对其机理进行了探讨.研究表明:360℃,130 h约束时效时,随着外加应力的增加,NiTi合金的负热膨胀系数先增后减,在250 Mpa时可获得峰值-87.0×10-6 K-1;时效温度升高或高温下时效时间延长,其NTE行为变差.母相中Ti3Ni4相定向析出所形成的内应力场有效控制了相变的发生并促使产生体积变化和双程形状记忆效应,二者的联合作用导致了NTE行为的产生.
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