用单辊急冷法制备(Fe1-xCox)86Hf7B6Cu1(x=0.05,x=0.3)合金薄带,分别用XRD、TEM、HRTEM、MS分析方法研究其微观结构;测算了非晶薄带中纳米晶的晶粒尺寸和晶化量,对比分析了各种表征方法的适用条件、敏感性和精度.选出完全非晶态合金薄带进行磁脉冲处理使其晶化,表征其结构和晶化量.
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