Quantitative phase analysis of Portland cement clinker samples was performed using an adaptation of the Rietveld method.The Rietveld quantitative analysis program,originally in Fortran 77 code,was significantly modified in visual basic code with windows 9X graph-user interface,which is free from the constraint of direct utilizable memory 640 k,and can be conveniently operated under the windows environment.The Rietveld quantitative method provides numerous advantages over conventional XRD quantitative method,especially in the intensity anomalies and superposition problems.Examples of its use are given with the results from other methods.It is concluded that,at present,the Rietveld method is the most suitable one for quantitative phase analysis of Portland cement clinker.
参考文献
| [1] | L P Aldridge .Accuracy and Precision of Phase Analysis in Portland Cement by Bogue,Microscopic and X-ray Diffraction Methods[J].Cement and Concrete Research,1982,12(02):381-398. |
| [2] | D L Bish;S J Chipera.Problems and Solutions in Quantitative Analysis of Complex Mixtures by X-ray Powder Diffraction[A].York:Plenum,1988:295-308. |
| [3] | R J Hill;C J Howard .Quantitative Phase Analysis from Neutron Powder Diffraction Data Using the Rietveld Method[J].Journal of Applied Crystallography,1987,20:467-474. |
| [4] | H M Rietveld .A Profile Refinement Method for Nuclear and Magnetic Structures[J].Journal of Applied Crystallography,1969,2:65-71. |
| [5] | G X Shao.Silicate Petrography[M].武汉:武汉大学出版社,1991 |
| [6] | D B Wiles;R A Young .A New Computer Program for Rietveld Analysis of X-ray Powder Diffraction Patterns[J].Journal of Applied Crystallography,1981,14:149-151. |
| [7] | D L Bish;S A Howard .Quantitative Phase Analysis Using the Rietveld Method[J].Journal of Applied Crystallography,1988,21:86-91. |
| [8] | D K Smith;G G Johnson;A Schieble et al.Ullman,Quantitative X-ray Powder Diffraction Method Using the Full Diffraction Pattern[J].Powder Diffraction,1987,2:73-77. |
| [9] | J C Taylor .Computer Programs for Standardless Quantitative Analysis of Minerals Using the Full Powder Diffraction Profile[J].Powder Diffraction,1991,6:2-9. |
| [10] | D L Bish;J E Post .Quantitative Analysis of Geological Materials Using X-ray Powder Diffraction Data and the Rietveld Refinement Method[J].Geological Society of America Abstracts with Programs,1988,20:A233. |
| [11] | S A Howard;K D Preston .Profile Fitting of Powder Diffraction Patterns[J].Mineralogical Society of America Reviews in Mineralogy,1989,20:217-275. |
| [12] | Jiang Yonghui;Huang Shiyuan .The Quantitative Analysis of Cement Clinker Minerals by XRD Using an External Standard[J].Acta Silicate,1984,12:374-381. |
| [13] | D L Bish;J E Post .Quantitative Mineralogical Analysis Using the Rietveld Full-pattern Fitting Method[J].American Mineralogist,1993,78:932-940. |
| [14] | Sun Wenhua;Yang Shuzhen;Qian Jinfu et al.The Superposing Peak Self-flushing Method for Quantitative Analysis of Cement Clinker Minerals by XRD[J].武汉理工大学学报(材料科学版)英,1992,7:53-60. |
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