为研究高压熔渗金刚石/铜复合材料导热率在低温区的变化规律,采用高压熔渗(HRF)的方法分别制备了不同粒度(100 μm,250 μm,400 μm)的金刚石/铜复合材料,利用扫描量热法分析评价了高压熔渗法制备的不同粒度金刚石/铜复合材料的低温导热特性,采用扫描电子显微镜(SEM)分析其显微组织.研究结果表明:由于高压熔渗制备的金刚石/铜复合材料中的部分金刚石发生聚晶反应,导致金刚石颗粒间晶界传热的热阻远小于界面传热热阻;高压熔渗条件下,金刚石颗粒内部变形破碎导致缺陷增多,且100～150 K低温下以声子为主要热载子的传热对裂纹和间隙等缺陷敏感,导致在较低温区内金刚石/铜复合材料的导热率低于普通压力熔渗(PF)所制备的金刚石/铜复合材料的导热率.
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