以不同粒径的苯乙烯-丙稀酸(酯)共聚物(PSA)乳胶粒为模板,制备出均匀的PSA/CdS核壳复合结构的微球,用有机溶剂溶去模板PSA后,分别制备了不同粒径的CdS空心微球.透射电镜分析结果表明,以直径250、340和600nm的PSA乳胶粒为模板,所得CdS空心球的粒径均匀,直径分别为340、450和800nm.紫外可见吸收光谱显示3个CdS空心球样品的最大吸收分别为480nm、410nm和485nm.
参考文献
[1] | 张军,孙聆东,钱程,廖春生,严纯华.CTAB-正己醇-正庚烷-水四元反相胶束体系制备CdS纳米微粒及其光学性质[J].科学通报,2001(17):1423-1427. |
[2] | Shao MW.;Xu F.;Peng YY.;Wu J.;Li Q.;Zhang SY.;Qian YT. .Microwave-templated synthesis of CdS nanotubes in aqueous solution at room temperature[J].New Journal of Chemistry,2002(10):1440-1442. |
[3] | Zhu JJ.;Wang H.;Zhu JM.;Wang J. .A rapid synthesis route for the preparation of CdS nanoribbons by microwave irradiation[J].Materials Science & Engineering, B. Solid-State Materials for Advanced Technology,2002(2/3):136-140. |
[4] | Paul V. Braun;Samuel I. Stupp .CdS MINERALIZATION OF HEXAGONAL, LAMELLAR, AND CUBIC LYOTROPIC LIQUID CRYSTALS[J].Materials Research Bulletin: An International Journal Reporting Research on Crystal Growth and Materials Preparation and Characterization,1999(3):463-469. |
[5] | Huang JX.;Li B.;Liu Y.;Qian YT.;Zhang SY.;Xie Y. .In-situ source-template-interface reaction route to semiconductor CdS submicrometer hollow spheres[J].Advanced Materials,2000(11):808-811. |
[6] | Jiang X;Xie Y;Lu J et al.Low temperature interfacemineralizing route to Cus,Cds,NiS spheres[J].Canadian Journal of Chemistry,2002,80:263-7. |
[7] | 宋彩霞,王德宝,古国华,傅洵,胡正水.无机空心球材料的乳胶粒模板法制备及应用[J].材料导报,2003(07):32-34. |
[8] | 郭玉,古国华,焦艳荣,傅洵,胡正水.用两亲聚合物制备大颗粒苯丙乳液[J].高分子材料科学与工程,2003(04):40-43. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%