综述了20世纪90年代以来的有关环境水体中四乙基铅分析方法的研究报道.对各种样品前处理方法和检测技术的优缺点进行了评价,其中吹脱捕集-气相色谱/质谱联用法(P&T-GC/MS),样品前处理过程可全自动化、灵敏度高及无需有机萃取试剂,检测技术具有高效分离、定性及定量的能力,值得在环境水体四乙基铅的监测中推广使用.部分文献报道的P&T-GC/MS法测定水样中四乙基铅时,出现的疑似捕集阱或质谱检测器“中毒”现象,可能是由四乙基铅在水样中的短期稳定性较差造成,影响其稳定性的关键因素及解决办法还需进一步研究.
参考文献
| [1] | Kovarik W .Ethyl-leaded gasoline: how a classic occupational disease became an international public health disaster.[J].International journal of occupational and environmental health: Official journal of the International Commission on Occupational Health,2005(4):384-397. |
| [2] | Rhue R D;Mansell R S;Ou L T et al.The fate and behavior of lead alkyls in the environment:a review[J].Critical Reviews in Environmental Science and Technology,1992,22(3-4):169-193. |
| [3] | 曾北危 .环境样晶中四烷基铅的测定[J].环境科学,1980,5(05):55-57. |
| [4] | Wa'il Y. Abu-El-Sha'r;Eyad S. Batarseh;Bashaar Y. Ammary .Experimental assessment of the adequacy of clayey soils in Irbid to retard lead from aqueous solutions and leaded gasoline[J].Environmental geology: International journal of geosciences,2003(5):526-531. |
| [5] | Krystyna Pyrzynska .Organolead Speciation in Environmental Samples: a Review[J].Mikrochimica Acta: An International Journal for Physical and Chemical Methods of Analysis,1996(3/4):279-293. |
| [6] | 常晓峰,舒平,白伟.四乙基铅中毒临床研究进展[J].工业卫生与职业病,2008(05):312-314. |
| [7] | Craig P J.Organometallic compounds in the environment,principles and reactions[M].New York:John Wiley and Sons,Inc,1986:30. |
| [8] | GBZ 36-2002.职业性急性四乙基铅中毒诊断标准[S]. |
| [9] | Fayerweather W E;Karns M E;Nuwayhid I A et al.Case-control study of cancer risk in tetraethyl lead manufacturing[J].American Journal of Industrial Medicine,1997,31(01):28-35. |
| [10] | Tara M. Lovestead;Thomas J. Bruno .Application of the Advanced Distillation Curve Method to the Aviation Fuel Avgas 100LL[J].Energy & Fuels,2009(2):2176-2183. |
| [11] | Al-Rashdan A;Vela N P;Caruso J A et al.Lead speciation by gradient high-performance liquid chromatography with inductively coupled plasma mass spectrometric detection[J].Journal of Analytical Atomic Spectrometry,1992,7(03):551-555. |
| [12] | 穆肃,刘雯,丁曦宁.地表水环境四乙基铅监测分析方法研讨[J].科技传播,2012(24):107-108. |
| [13] | 王玲玲;梁晶;靳朝喜.地表水中四乙基铅分析方法及样品保存探讨研究[A].福建厦门,2012 |
| [14] | 周树杰,古健,黄卓尔,王少毅.三氯甲烷萃取-石墨炉法测定地表水、饮用水中的四乙基铅[J].仪器仪表与分析监测,2012(02):34-37. |
| [15] | GB/T5750.6-2006.生活饮用水标准检验方法金属指标[S]. |
| [16] | Gallert C;Winter J .Bioremediation of soil contaminated with alkyllead compounds[J].Water Research,2002,36(12):3130-3140. |
| [17] | C. Gallert;J. Winter .Degradation of alkyllead compounds to inorganic lead in contaminated soil[J].Water research: A journal of the international water association,2004(19):4204-4212. |
| [18] | Teeling H;Cypionka H .Microbial degradation of tetraethyl lead in soil monitored by microcalorimetry[J].Applied Microbiology and Biotechnology,1997(2):275-279. |
| [19] | 杨丽莉,王美飞,李娟,胡恩宇.气相色谱-质谱法测定水中痕量的四乙基铅[J].色谱,2010(10):993-996. |
| [20] | 王晋宇,彭亮,陈玲瑚,赵辰,郭志宇.液液萃取处理样品-毛细管柱气相色谱法测定水中四乙基铅[J].理化检验：化学分册,2011(08):972-973. |
| [21] | 李世荣,吕鹂,娄涛,杨华,文新宇.液液萃取-高效液相色谱法测定水中四乙基铅[J].环境监测管理与技术,2011(02):45-47. |
| [22] | 刘梅.液液萃取-气相色谱／质谱联用法测定地表水中四乙基铅[J].新疆环境保护,2012(03):37-40. |
| [23] | 李世荣,吕鹂,娄涛,杨华,文新宇.高效液相色谱法测定地表水中四乙基铅[J].中国环境监测,2012(04):95-97. |
| [24] | 程滢,杨文武,张宗祥.石墨炉原子吸收光谱法测定水中四乙基铅[J].环境监测管理与技术,2009(02):40-41. |
| [25] | 程滢,杨文武,倪刘建,张宗祥.石墨炉原子吸收法快速测定水中的四乙基铅[J].中国环境监测,2009(05):42-44. |
| [26] | 彭利,罗钰,朱奕,许雄飞,丁庆云.石墨炉原子吸收法测定环境水样中四乙基铅的方法探讨[J].中国环境监测,2009(06):46-49. |
| [27] | 孙平昊,尚艳红.浅议石墨炉原子吸收法测定水中的四乙基铅[J].环境科学与管理,2009(09):108-109. |
| [28] | 公丕峰.水中四乙基铅的氢化原子吸收测定法[J].环境与健康杂志,2011(05):435-436. |
| [29] | Elfering H.;Poll KG.;Andersson JT. .Determination of organic lead in soils and waters by hydride generation inductively coupled plasma atomic emission spectrometry[J].The Analyst: The Analytical Journal of the Royal Society of Chemistry: A Monthly International Publication Dealing with All Branches of Analytical Chemistry,1998(4):669-674. |
| [30] | 周敏,杜晓婷,李玮,孙亮.分散液相微萃取-气相色谱-质谱联用法测定水样中的四乙基铅[J].质谱学报,2011(06):355-359. |
| [31] | 胡文凌,叶朝霞,庞明,李蕾,李莉.分散液液微萃取-气相色谱/质谱联用法测定饮用水源水中的四乙基铅[J].中国环境监测,2011(04):57-60. |
| [32] | 曹志斌,王晋宇,陆文娟,郭志宇,陈玲瑚.固相萃取-气相色谱法测定水中四乙基铅含量[J].理化检验：化学分册,2012(12):1421-1423. |
| [33] | 王灵,郑江,钱翌,张江丽,刘金伟.固相萃取-气相色谱/质谱法测定水中四乙基铅的方法研究[J].环境科学与技术,2012(11):145-147. |
| [34] | Arthur C L;Pawliszyn J .Solid phase microextraction with thermal desorption using fused silica optical fibers[J].Analytical Chemistry,1990,62(19):2145-2148. |
| [35] | Fragueiro MS.;Lavilla I.;Bendicho C.;Alava-Moreno F. .Determination of tetraethyllead by solid phase microextraction-thermal desorption-quartz furnace atomic absorption spectrometry[J].Journal of Analytical Atomic Spectrometry,2000(6):705-709. |
| [36] | Gorecki T;Pawliszyn J .DETERMINATION OF TETRAETHYLLEAD AND INORGANIC LEAD IN WATER BY SOLID PHASE MICROEXTRACTION GAS CHROMATOGRAPHY[J].Analytical chemistry,1996(17):3008-3014. |
| [37] | Xiaomei Yu;Janusz Pawllszyn .Speciation of Alkyllead and Inorganic Lead by Derivatization with Deuterium-Labeled Sodium Tetraethylborate and SPME-GC/MS[J].Analytical chemistry,2000(8):1788-1792. |
| [38] | Sturgeon R E;Willie S N;Berman S S .Atomic absorption determination of lead at picogram per gram levels by ethylation with in-situ concentration in a graphite furnace[J].Analytical Chemistry,1989,61(17):1867-1869. |
| [39] | Sibylle Mothes;Rainer Wennrich .Coupling of SPME and GC-AED for the Determination of Organometallic Compounds[J].Mikrochimica Acta: An International Journal for Physical and Chemical Methods of Analysis,2000(1/2):91-95. |
| [40] | 帅琴,杨薇,张生辉,郑楚光,郑岳君.顶空固相微萃取-气相色谱质谱联用测定烷基铅的研究[J].分析试验室,2004(02):14-17. |
| [41] | 李爱荣,李明,帅琴,胡圣虹.固相微萃取-电感耦合等离子体质谱联用接口及其分析性能研究[J].分析科学学报,2005(03):280-282. |
| [42] | 李明,李爱荣,帅琴,胡圣虹.双气路校正-固相微萃取电感耦合等离子体质谱法测定四乙基铅[J].分析试验室,2007(06):107-110. |
| [43] | 赖永忠.顶空-固相微萃取法测定地表水中四乙基铅[J].广州化工,2011(07):130-131. |
| [44] | 秦宏兵,顾海东,孙欣阳,朱健禾.顶空固相微萃取-气相色谱法测定水中四乙基铅[J].中国环境监测,2012(04):82-84. |
| [45] | Reuther R.;Allard B.;Jaeger L. .Determination of organometallic forms of mercury, tin and lead by in situ derivatization, trapping and gas chromatography - atomic emission detection[J].Analytica chimica acta,1999(2/3):259-269. |
| [46] | Ceulemans M.;Adams FC. .INTEGRATED SAMPLE PREPARATION AND SPECIATION ANALYSIS FOR THE SIMULTANEOUS DETERMINATION OF METHYLATED SPECIES OF TIN, LEAD AND MERCURY IN WATER BY PURGE-AND-TRAP INJECTION-CAPILLARY GAS CHROMATOGRAPHY ATOMIC EMISSION SPECTROMETRY[J].Journal of Analytical Atomic Spectrometry,1996(3):201-206. |
| [47] | Gianni Andreottola;Loris Dallago;Elisa Ferrarese .Feasibility study for the remediation of groundwater contaminated by organolead compounds[J].Journal of hazardous materials,2008(1/3):488-498. |
| [48] | 刘劲松,马荻荻,叶伟红,孙晓慧,潘荷芳,冯元群.地表水中四乙基铅吹扫捕集-气相色谱/质谱分析方法研究及其应用[J].中国环境监测,2010(04):20-23. |
| [49] | 李振宇;胡平;赵世民.地表水中四乙基铅吹脱-捕集-气相色谱法/质谱联用检测方法研究[A].福建厦门,2012 |
| [50] | 秦明友,张新申,康莉,陈刚才,杨清玲.吹扫捕集气质联用法测定水中4种挥发性有机物[J].环境科学与技术,2013(01):93-96. |
| [51] | Cukrowska,EM;Nsengimana,H;Chimuka,L .Speciation of alkyllead in aqueous samples with application of liquid membrane probe for extraction and preconcentration.[J].Journal of Separation Science,2007(16):2754-2759. |
| [52] | Carbonell V;de la Guardia M;Salvador A et al.On-line microwave oven digestion flame atomic absorption analysis of solid samples[J].Analytica Chimica Acta,1990,238(02):417-421. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%