本文通过对Al_2O_3-Nb封接界面Na腐蚀情况的研究,证明玻璃焊料与Nb界面结合不好是影响Al_2O_3-Nb封接质量和高压钠灯寿命的主要原因.并利用透射电子显微镜,研究了不同寿命的高压钠灯中玻璃焊料与Nb界面的显微组织结构,揭示了界面结构对Al_2O_3-Nb封接质量的影响.根据热力学分析和Pask的金属-陶瓷界面结合理论,讨论了在焊接过程中发生在玻璃焊料与Nb界面的物理化学过程和界面结合机制.
Through a study on Na corrosion of Al_2O_3/Nb seal interface, itis shown that the main factor influencing the Al_2O_3/Nb seal and the lifetime ofhigh pressure natrium lamp is the interface bonding between glass seal and Nb. The microstructure of interface of high pressure natrium lamp with differentlifetime has been studied by means of TEM, and the influence of interface struc-ture on the quality of Al_2O_3/Nb seal has been revealed. Based on the thermodyna-mic analysis and Pask theory of metal/ceramic interface bonding, the physicoche-mical process of glass seal/Nb interfaces and bonding mechanism during sealing hasalso been discussed.
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