采用固态杂化微波加热技术,以Ti粉与Se粉为反应物,30 min内成功合成了单相TiSe2.与普通加热方式下的固相反应法相比,固态杂化微波加热使TiSe2的产率有了显著提高且能效更高.采用X射线粉末衍射、扫描电子显微镜、X射线能谱、高分辨透射电子显微镜及电子衍射对产物的结构、组份和形貌进行了表征.
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