采用传统的陶瓷工艺制备少量掺杂Y2O3,CeO2的Mg-PSZ陶瓷,材料在较低的温度(≤1550 ℃)下烧结致密并实现了微晶化(晶粒尺寸~10 μm).探讨了Y2O3,CeO2的复合稳定作用和1100 ℃热处理过程对材料相组成、显微结构和力学性能的影响.经1100 ℃适当时间热处理,Y2O3,CeO2的复合稳定作用有效抑制亚共析分解反应发生,优化调整c-ZrO2晶粒中的t-ZrO2析出体成核长大过程.断裂特征为穿晶、沿晶兼有,相变增韧和微裂纹增韧的协同效应使材料具有优良的力学性能.
参考文献
[1] | Buykx W J;Swain M V.Thermal diffusivity of zirconia partically and fully stabilized with magnesia[A].Ohio:The American ceramic Society Inc,1984:518. |
[2] | Hannink R H J .Microstructural development of subeutoctidly aged MgO-ZrO2 alloys[J].Journal of Materials Science,1983,18:457. |
[3] | 马亚鲁;王树强;谈家琪 等.化学共沉淀法制备微晶PSZ陶瓷的显微结构与性能[J].硅酸盐学报,1995,23(05):495. |
[4] | 马亚鲁;张国亮;王树强 等.湿化学法制备微晶(Y,Mg)-PSZ/MgAl2O4陶瓷的研究[J].硅酸盐学报,1996,24(01):38. |
[5] | Montross C S .Precipitation adn bulk propert6y behaviour in the yttria-magnesia-zirconia ternary system[J].British Ceramic Transactions,1991,90:175. |
[6] | Garvie R C;Nicholson P S .Phase analysis in zirconia system[J].Journal of the American Ceramic Society,1972,55(06):303. |
[7] | Hughan R R;Hannink R H J .Precipitation during controlled cooling of magnesia-partially-stabilized zirconia[J].Journal of the American Ceramic Society,1986,69(07):556. |
[8] | Bateman C A;Notis M R .Coarsening kinetics in Mg(Ca,Ti,Y)-partially-stabilized airconia[J].Journal of the American Ceramic Society,1992,75(06):1566. |
[9] | Nettleship I;Stevens R .Tetragonal zirconia polycrystal(TZP)[J].Int J High Technology Ceramics,1987,3:1. |
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