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开发了用溶胶-凝胶法制备纳米晶镍锌钴复合铁氧体颗粒的技术,并对溶胶-凝胶工艺的影响因素进行了研究探讨.用扫描电镜(SEM)、电子探针(EPMA)和X射线衍射(XRD)对样品进行了表征,得到球状分布的纳米晶镍锌钴铁氧体/二氧化硅复合颗粒,并优化了制备工艺.

参考文献

[1] 李凤生;杨毅;马振叶.纳米功能复合材料及应用[M].北京:国防工业出版社,2003:177.
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[6] Hiratsuka N.;Kakizaki K.;Nozawa M. .MAGNETIC PROPERTIES OF COBALT FERRITE FILMS WITH PERPENDICULAR MAGNETIC ANISOTROPY[J].Journal of Magnetism and Magnetic Materials,1997(1):31-35.
[7] 李春;何惠良;李升章.镍锌铁氧体粉体合成新方法[J].四川有色金属,2000(02):49.
[8] 罗康碧,李沪萍,杨波,赵榆林,胡亮.镍锌铁氧体共沉淀前驱物经水热处理后的性能变化研究[J].有色金属(冶炼部分),2004(01):35-37.
[9] Choi Yong;Shim H S;Lee J S .Study on magnetic properties and structural analysis of Ni-Zn ferrite prepared through selfpropagating high-temperature synthesis reaction by neutron diffractometry[J].Journal of Alloys and Compounds,2001,326(01):56.
[10] 胡林,张朝平,勾华.镍/铁复合纳米微粒中与粒径相关的控制参数及磁性能分析[J].化学物理学报,2001(05):518-522.
[11] 张红芳,佘正国.探讨溶胶-凝胶工艺制备PZT薄膜[J].江苏大学学报(自然科学版),2002(02):83-87,94.
[12] Adriana S;Ardisson J;Waldemar A .A study of nanocrystalline NiZn-ferrite/SiO2 synthesized by sol-gel[J].Journal of Magnetism and Magnetic Materials,2000,192(02):277.
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