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采用两种不同素坯成型工艺制备层状C/ZrB2-SiC复合材料,并对其微观结构和力学性能进行研究.结果表明:高温下预压成型制备的层状ZrB2-SiC复合材料层厚均匀,界面平直,弯曲强度和断裂韧性较高,分别达到427MPa和11.3 MPa·m1/2.而室温下预压成型各层厚度不均,界面弯曲,出现界面交叉现象,弯曲强度和断裂韧性较低,分别为277 MPa和9.4 MPa·m1/2.采用素坯高温预压成型制备的层状C/ZrB2-SiC复合材料力学性能较高,主要归因于界面平直,裂纹交替通过基体层和界面层,裂纹的扩展路径变长,断裂功增加.

参考文献

[1] Wei-Ming Guo;Guo-Jun Zhang .Oxidation resistance and strength retention of ZrB_2- SiC ceramics[J].Journal of the European Ceramic Society,2010(11):2387-2395.
[2] Haitang Wu;Weigang Zhang .Fabrication and properties of ZrB2-SiC-BN machinable ceramics[J].Journal of the European Ceramic Society,2010(4):1035-1042.
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[6] Xu Yongdong;Cheng Laifei;Zhang Litong .Carbon /silicon carbide composites prepared by chemical vapor infiltration combined with silicon melt infiltration[J].Carbon: An International Journal Sponsored by the American Carbon Society,1999(8):1179-1187.
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[8] Xiao-Jun Zhou;Guo-Jun Zhang;Yao-Gang Li .Hot pressed ZrB_2-SiC-C ultra high temperature ceramics with polycarbosilane as a precursor[J].Materials Letters,2007(4/5):960-963.
[9] Rezaie A;Fahrenholtz WG;Hilmas GE .Effect of hot pressing time and temperature on the microstructure and mechanical properties of ZrB2-SiC[J].Journal of Materials Science,2007(8):2735-2744.
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