通过在Y-TZP中加入适量的硅酸盐玻璃添加剂,使其烧结温度明显降低,并且制备出具有细晶粒、高强度的四方相氧化锆增韧陶瓷材料.分析了添加剂含量及烧结温度与材料致密度、显微结构及力学性能的关系,发现在Y-TZP材料中加入1wt%的添加剂,可以使材料在1400℃下烧结,氧化锆晶粒尺寸约为100~200nm;其抗折强度可达950MPa.
Tetragonal Zirconia Polycrystals (TZP) with superfine grains and high flexural strength were obtained by adding certain glass additives into Y-TZP powder and sintered at low temperature. The relationship between the density, mechanical properties arid the amount of additives, sintering temperature were investigated. The results show that Y-TZP with 1wt% glass additives can be densifed at 1400℃. The grain size of Y-TZP is 100-200nm and flexural strength can reach 950MPa.
参考文献
[1] | Boutz M, Winnubst A J, Burggraaf A J A. J. Europ. Ceram. Soc., 1994, 13 (2): 89--102. [2] lange F F, Schubert H, Claussen N, et al. J. Mater. Sci., 1986, 21: 768--774. [3] Qin Haixia, Huang Xiaoxian. J. Am. Ceram. Soc., 2000, 83 (11): 2881--2883. [4] 张玉峰, 郭景坤, 黄校先(ZHANG Yu-Feng, et al). 硅酸盐学报(Journal of Chinese Ceramics Society), 1998, 26 (3): 373--377. [5] Lu H Y, Bow J S. J. Am. Ceram. Soc., 1989, 72: 228--231. [6] Wu S, Brook R J. Trans. J. Brit. Ceram. Soc., 1983, 82: 200--205. [7] Hyatt E P, Christensen C J, Cutler I B. Am. Ceram. Soc. Bull., 1957, 36: 307--309. [8] Verkerk M J, Winnubst A J A, Burggraaf A J. J. Mater. Sci., 1982, 17: 3113--3122. [9] Radford K C, Bratton R J. J. Mater. Sci., 1979, 14: 59--65. [10] Rǖhle M, Claussen N, Heuer A H. In: Claussen N, Rǖhle M, Heuer A H. eds. Advances in Ceramics, Volume 12: Science and Technology of Zirconia Ⅱ. Columbus, OH: The American Ceramic Society, Inc., 1984. 352--381. [11] Shackelford J F, Nicholson P S, Smeltzer W W. Am. Ceram. Soc. Bull., 1974, 53: 865--867. [12] Mecartney M L. J. Am. Ceram. Soc., 1987, 70: 54--58. [13] Kobayashi S. J. Mater. Sci. Lett., 1985, 4: 268--270. [14] Kingery W D, Bowen H K, Uhlmann D R. Introduction to Ceramics (second edition), 1976. 520. [15] 周玉. 陶瓷材料学. 哈尔滨: 哈尔滨工业大学出版社, 1999. 345. [16] M. V. 斯温主编, 郭景坤等译. 陶瓷的结构与性能. 北京: 科学出?版社, 1998. 101. |
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