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以Al(NO3)3·9H2O和尿素为原料、无水乙醇-水混合液为溶剂,采用溶剂热法150℃、6h条件下制备了叶片状分级结构γ-AlOOH.通过X射线衍射(XRD)、透射电镜(TEM)及紫外-可见吸收光谱测试(UV-vis)等手段对所得产物进行表征,研究了尿素对纳米γ-AlOOH形貌以及对刚果红吸附性能的影响.实验结果表明,当尿素摩尔量为0.4 mmol时产物为叶片状分级结构γ-AlOOH,由长度在1.5~2 μn范围、厚度约几个nm的纳米片自组装而成,且对刚果红表现出吸附性能最佳,其吸附率为98%.

参考文献

[1] Zhang J;Wei SY;Lin J;Luo JJ;Liu SJ;Song HS;Elawad E;Ding X;Gao JM;Qi SR .Template-free preparation of bunches of aligned boehmite nanowires[J].The journal of physical chemistry, B. Condensed matter, materials, surfaces, interfaces & biophysical,2006(43):21680-21683.
[2] Xiaoxiao Yu;Jiaguo Yu;Bei Cheng .Synthesis of Hierarchical Flower-like AlOOH and TiO2/AlOOH Superstructures and their Enhanced Photocatalytic Properties[J].The journal of physical chemistry, C. Nanomaterials and interfaces,2009(40):17527-17535.
[3] 汤睿,张昭,杨晓娇,王寅.溶剂热合成分级叶片簇状纳米氧化铝[J].无机化学学报,2011(02):251-258.
[4] Ye Liu;Ding Ma;Xiuwen Han;Xinhe Bao;Wiebke Frandsen;Di Wang;Dangsheng Su .Hydrothermal synthesis of microscale boehmite and gamma nanoleaves alumina[J].Materials Letters,2008(8/9):1297-1301.
[5] Weiquan Cai;Shuanggui Chen;Jiaguo Yu;Yuzhen Hu;Chengxiong Dang;Shuhua Ma .Template-free solvothermal synthesis of hierarchical boehmite hollow microspheres with strong affinity toward organic pollutants in water[J].Materials Chemistry and Physics,2013(1):167-173.
[6] Zhang J;Liu SJ;Lin J;Song HS;Luo JJ;Elssfah EM;Ammar E;Huang Y;Ding XX;Gao JM .Self-assembly of flowerlike AlOOH (boehmite) 3D nanoarchitectures[J].The journal of physical chemistry, B. Condensed matter, materials, surfaces, interfaces & biophysical,2006(29):14249-14252.
[7] 孟范成,张晓磊,任海深,卢思颖,黄伟九,洪学鹍.核桃状3D分级结构γ-AlOOH无模板水热合成及对刚果红吸附性能研究[J].人工晶体学报,2014(05):1274-1279.
[8] Feng YL;Lu WC;Zhang LM;Bao XH;Yue BH;Iv Y;Shang XF .One-step synthesis of hierarchical cantaloupe-like AlOOH superstructures via a hydrothermal route[J].Crystal growth & design,2008(4):1426-1429.
[9] Fei JB;Cui Y;Yan XH;Qi W;Yang Y;Wang KW;He Q;Li JB .Controlled preparation of MnO2 hierarchical hollow nanostructures and their application in water treatment[J].Advanced Materials,2008(3):452-456.
[10] Chichao Yu;Xiaoping Dong;Limin Guo .Template-Free Preparation of Mesoporous Fe2O3 and Its Application as Absorbents[J].The journal of physical chemistry, C. Nanomaterials and interfaces,2008(35):13378-13382.
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