采用单辊甩带法制备了ZK60镁合金薄带,研究了不同条件热处理薄带的组织和显微硬度.结果表明,薄带由晶粒尺寸<8 μm的等轴α-Mg、球状β'2相和少量杆状β',相组成;热处理温度<300℃时,晶粒无长大;温度>300℃时,晶粒显著长大.原始薄带显微硬度约为50 HV,300℃×2 h热处理后显微硬度值最大约为80 HV;β'1和β'2相的弥散强化作用是薄带硬度提高的内在原因.
The rapidly solidified(RS)ZK60 magnesium alloy ribbons were prepared by a single roller apparatus.Microstructure and microhardness of the ribbons with and without heat treatment were investigated by menas of optical microscope,TEM,XRD and microhardness test.The results show that the ribbons are composed of equiaxed α-Mg matrix with grain size 8 μm,spherical β'2 and a few rods β'1 phases.No growth of the α-Mg matrix grains is observed for the RS ZK60 alloy after annealing at temperature below 300 ℃.However,the grains grow significantly after annealing at temperatures higher than 300 ℃.The average microhardness of the RS ribbons of ZK60 alloy is about SO HV.Microhardness of the annealed RS ribbons increases firstly to a maximum value of 80 HV at 300 ℃ for 2 h and then decreases with increasing annealing temperature or prolonging annealing time at 300 ℃.The TEM observation suggests show that β'1 and β'2 phases are considered to be the main strengthening phases.
参考文献
[1] | Ma CJ.;Liu MP.;Wu GH.;Ding WJ.;Zhu YP. .Tensile properties of extruded ZK60-RE alloys[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2003(1/2):207-212. |
[2] | Hiroyuki Watanabe;Toshiji Mukai;Koichi Ishikawa;Kenji Higashi .Low temperature superplasticity of a fine-grained ZK60 magnesium alloy processed by equal-channel-angular extrusion[J].Scripta materialia,2002(12):851-856. |
[3] | A. Bussiba;A. Ben Artzy;A. Shtechman;S. Ifergan;M. Kupiec .Grain refinement of AZ31 and ZK60 Mg alloys — towards superplasticity studies[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2001(1):56-62. |
[4] | 王成全,于艳,方园,李廷举.亚快速凝固技术的研究进展[J].钢铁研究学报,2005(05):11-15. |
[5] | Maeng D.Y.;Kim T.S. .MICROSTRUCTURE AND STRENGTH OF RAPIDLY SOLIDIFIED AND EXTRUDED Mg-Zn ALLOYS[J].Scripta materialia,2000(5):358-389. |
[6] | 黄正华,郭学锋,张忠明.快速凝固AZ91D镁合金组织的研究[J].材料热处理学报,2005(01):32-35. |
[7] | Yoshihito Kawamura;Kentaro Hayashi;Akihisa Inoue .Rapidly Solidified Powder Metallurgy Mg_(97)Zn_1Y_2 Alloys with Excellent Tensile Yield Strength above 600 MPa[J].Materials transactions,2001(7):1172-1176. |
[8] | X. Gao;J.F. Nie .Structure and thermal stability of primary intermetallic particles in an Mg-Zn casting alloy[J].Scripta materialia,2007(7):655-658. |
[9] | J. Buha .The effect of Ba on the microstructure and age hardening of an Mg-Zn alloy[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2008(1/2):70-79. |
[10] | J. Buha .Grain refinement and improved age hardening of Mg-Zn alloy by a trace amount of V[J].Acta materialia,2008(14):3533-3542. |
[11] | L.Y. WEI;G.L. DUNLOP;H. WESTENGEN .The Intergranular Microstructure of Cast Mg-Zn and Mg-Zn-Rare Earth Alloys[J].Metallurgical and Materials Transactions, A. Physical Metallurgy and Materials Science,1995(8):1947-1955. |
[12] | Govind.;Mittal MC.;Lal K.;Mahanti RK.;Sivaramakrishnan CS.;Nair KS. .Development of rapidly solidified (RS) magnesium-aluminium-zinc alloy[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2001(0):520-523. |
[13] | Buha J .Reduced temperature (22-100 degrees C) ageing of an Mg-Zn alloy[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2008(1/2):11-19. |
[14] | Gao X;Nie J F .Characterization of strengthening precipitate phase in a Mg-Zn alloy[J].Scripta Materialia,2007,56(08):645-648. |
[15] | J. BUHA;T. OHKUBO .Natural Aging in Mg-Zn(-Cu) Alloys[J].Metallurgical and materials transactions. A, physical metallurgy and materials science,2008(9):2259-2273. |
- 下载量()
- 访问量()
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%