采用简单的水热法,以氯化锌(AR)和氢氧化钠(AR)为原料制备了花簇形氧化锌纳米棒.通过改变溶液的pH值、水热温度、水热时间等因素研究对样品结构和成貌的影响,并利用X射线衍射仪(XRD)、扫描电镜(SEM)、紫外-可见光谱仪(UV)对氧化锌纳米棒的结构、形貌及光催化性能进行研究,结果表明在温度为80℃,反应时间为18h、锌碱比为1∶7.5时,氧化锌成貌最佳,且光催化性能较好.
参考文献
[1] | Goldberger J;Sirbuly DJ;Law M;Yang P.ZnO nanowire transistors[J].The journal of physical chemistry, B. Condensed matter, materials, surfaces, interfaces & biophysical,20051(1):9-14. |
[2] | Wang ZL;Song J.Piezoelectric nanogenerators based on zinc oxide nanowire arrays.[J].Science,20065771(5771):242-246. |
[3] | Maria D. Hernandez-Alonso;Fernando Fresno;Silvia Suarez;Juan M. Coronado.Development of alternative photocatalysts to TiO_2: Challenges and opportunities[J].Energy & environmental science: EES,200912(12):1231-1257. |
[4] | Huanjun Zhang;Guohua Chen;Detlef W. Hahnemann.Photoelectrocatalytic materials for environmental applications[J].Journal of Materials Chemistry: An Interdisciplinary Journal dealing with Synthesis, Structures, Properties and Applications of Materials, Particulary Those Associated with Advanced Technology,200929(29):5089-5121. |
[5] | Pengrong Ren;Huiqing Fan;Xin Wang.Electrospun nanofibers of ZnO/BaTiO_3 heterostructures with enhanced photocatalytic activity[J].Catalysis Communications,2012:32-35. |
[6] | Cai, Y.;Fan, H.;Xu, M.;Li, Q..Rapid photocatalytic activity and honeycomb Ag/ZnO heterostructures via solution combustion synthesis[J].Colloids and Surfaces, A. Physicochemical and Engineering Aspects,2013:787-795. |
[7] | Jiawen Fang;Huiqing Fan;Guangzhi Dong.A facile way to synthesize cost-effective ZnO nanorods with enhanced photocatalytic activity[J].Materials Letters,2014Apr.1(Apr.1):147-150. |
[8] | Jones N;Ray B;Ranjit KT;Manna AC.Antibacterial activity of ZnO nanoparticle suspensions on a broad spectrum of microorganisms[J].FEMS Microbiology Letters,20081(1):71-76. |
[9] | Xia, T.;Kovochich, M.;Liong, M.;M?dler, L.;Gilbert, B.;Shi, H.;Yeh, J.I.;Zink, J.I.;Nel, A.E..Comparison of the mechanism of toxicity of zinc oxide and cerium oxide nanoparticles based on dissolution and oxidative stress properties[J].ACS nano,200810(10):2121-2134. |
[10] | G. Colon;M.C. Hidalgo;J.A. Navio.Highly photoactive ZnO by amine capping-assisted hydrothermal treatment[J].Applied Catalysis, B. Environmental: An International Journal Devoted to Catalytic Science and Its Applications,20081/2(1/2):30-38. |
[11] | Cristian Lizama;Juanita Freer;Jaime Baeza;Hector D.Mansilla.Optimized photodegradation of Reactive Blue 19 on TiO_2 and ZnO suspensions[J].Catalysis Today,20022/4(2/4):235-246. |
[12] | Lu F;Cai WP;Zhang YG.ZnO hierarchical micro/nanoarchitectures: Solvothermal synthesis and structurally enhanced photocatalytic performance[J].Advanced functional materials,20087(7):1047-1056. |
[13] | Template-free fabrication of porous zinc oxide hollow spheres and their enhanced photocatalytic performance[J].Journal of porous materials,20101(1):79. |
[14] | Yuxin Wang;Xinyong Li;Ning Wang.Controllable synthesis of ZnO nanoflowers and their morphology-dependent photocatalytic activities[J].Separation and Purification Technology,20083(3):727-732. |
[15] | E.Yassitepe;H.C.Yatmaz;C.Ozturk.Photocatalytic efficiency of ZnO plates in degradation of azo dye solutions[J].Journal of Photochemistry and Photobiology, A. Chemistry,20081(1):1-6. |
[16] | Giuseppe Marci;Vincenzo Auguliaro;Maria J. Lopez-Munoz;Cristina Martin;Leonardo Palmisano;Vicente Rives;Mario Schiavello;Richard J. D. Tilley;Anna Maria Venezia.Preparation Characterization and Photocatalytic Activity of Polycrystalline ZnO/TiO_2 System. 1. Surface and Bulk Characterization[J].The journal of physical chemistry, B. Condensed matter, materials, surfaces, interfaces & biophysical,20015(5):1026-1032. |
[17] | Yong-Hong Ni;Xian-Wen Wei;Xiang Ma;Jian-Ming Hong.CTAB assisted one-pot hydrothermal synthesis of columnar hexagonal-shaped ZnO crystals[J].Journal of Crystal Growth,20051/2(1/2):48-56. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%