表面技术 , 2012, 41(4): 80-83.
表面机械活化粉煤灰提取氧化铝及其动力学研究
吉涛 1, , 方莹 2, , 李镇 3, , 耿秋菊","id":"1b7b85bd-e515-4d72-8626-77f6d039dcb1","originalAuthorName":"耿秋菊"},{"authorName":"周荣明","id":"8f8ee31d-415d-4389-b562-b3c665068aea","originalAuthorName":"周荣明"},{"authorName":"印仁和","id":"9df7d98a-61c2-4d72-bf28-64269fccf438","originalAuthorName":"印仁和"},{"authorName":"郁祖湛","id":"3798c973-eed1-4ae8-a7f8-18c885a85bd6","originalAuthorName":"郁祖湛"}],"doi":"10.3969/j.issn.1001-3849.2005.02.002","fpage":"5","id":"02c6651f-643b-46ed-a3e9-d2bba3dac199","issue":"2","journal":{"abbrevTitle":"DDYJS","coverImgSrc":"journal/img/cover/DDYJS.jpg","id":"20","issnPpub":"1001-3849","publisherId":"DDYJS","title":"电镀与精饰 "},"keywords":[{"id":"4121e28d-9d43-494f-97cd-50751f89a365","keyword":"电解涂硅","originalKeyword":"电解涂硅"},{"id":"786707e6-ae3c-4caf-9a54-de3b9d6a37b7","keyword":"薄层二氧化硅","originalKeyword":"薄层二氧化硅"},{"id":"c0de9726-634b-4353-b97b-e003f597d8cf","keyword":"纳米","originalKeyword":"纳米"}],"language":"zh","publisherId":"ddjs200502002","title":"冷轧钢板表面电解涂覆薄层二氧化硅过程研究Ⅰ电解工艺参数对表面涂硅量的影响","volume":"27","year":"2005"},{"abstractinfo":"结合偏压磁控溅射铜(铜靶,本底真空度6.6 mPa,工作压力0.4 Pa,电流0.3 A,电压450 V,负偏压50 V,溅射时间10min)及脉冲焦磷酸盐电镀铜(60～70 g/L焦磷酸铜,280～320 g/L,焦磷酸钾,20～25 g/L柠檬酸铵,温度45～50℃,pH4.2～4.5)工艺对以聚酰亚胺薄膜为基材的挠性印制线路板微孔进行金属化处理,讨论了正向脉冲平均电流密度对镀层质量,以及正向脉冲占空比对镀层金相显微组织和电阻的影响.结果表明:金属化后孔壁镀层连续,平整光滑,结合力较好;随着正向脉冲电流密度的增大,镀层粗糙度减小;随着正向脉冲占空比的增大,镀层电阻急剧增大并最终达到稳定状态.","authors":[{"authorName":"余凤斌","id":"c3caab93-0069-450b-b136-4eb360935879","originalAuthorName":"余凤斌"},{"authorName":"冯立明","id":"469a6658-bd4f-45ab-b838-97b6917b3b4b","originalAuthorName":"冯立明"},{"authorName":"夏祥华","id":"5f365ede-b2b6-4dff-b9d0-5de48a51af95","originalAuthorName":"夏祥华"},{"authorName":"耿秋菊","id":"429ce43e-1e2e-448b-88f2-ff486bdeee0f","originalAuthorName":"耿秋菊"}],"doi":"","fpage":"30","id":"5bc619e0-7cf7-4a94-93db-774bf55597b1","issue":"1","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"0d2d2951-028b-4072-9ba0-9a3837a5c260","keyword":"聚酰亚胺","originalKeyword":"聚酰亚胺"},{"id":"a1659d19-dc29-47f2-a8c8-934cd4840ec4","keyword":"挠性印制线路板","originalKeyword":"挠性印制线路板"},{"id":"12fff980-a517-4e62-b6f2-1c051c0d51c1","keyword":"孔金属化","originalKeyword":"孔金属化"},{"id":"a78ad14e-102d-4550-994b-1d3b30d80899","keyword":"脉冲电镀","originalKeyword":"脉冲电镀"},{"id":"ee06da38-d800-49f5-b9dc-92e8caf656e9","keyword":"磁控溅射","originalKeyword":"磁控溅射"},{"id":"2fd3d9dc-e469-4836-9855-b0bf49433267","keyword":"占空比","originalKeyword":"占空比"},{"id":"d752ddd5-6277-458c-83d2-31c56955be28","keyword":"形貌","originalKeyword":"形貌"},{"id":"4ab435bf-6988-4a28-af40-4c4ef8fdb4d6","keyword":"电阻","originalKeyword":"电阻"}],"language":"zh","publisherId":"ddyts200901010","title":"挠性印制线路板孔金属化研究","volume":"28","year":"2009"},{"abstractinfo":"采用真空磁控溅射在涤纶织物上镀上金属镍,然后电镀上金属铜和镍.测试了样品的表面电阻、耐磨性、附着力及其在1kHz～40GHz频率范围内的电磁屏蔽性能.结果表明,样品具有良好的导电性、耐磨性和附着力,在30MHz～1.5GHz内的屏蔽效能大于70dB,在1.5GHz～40GHz内的屏蔽效能大于60dB,可以满足各种条件下的电磁屏蔽要求.","authors":[{"authorName":"余凤斌","id":"9611e36f-797e-4b6a-868b-84098514502f","originalAuthorName":"余凤斌"},{"authorName":"夏祥华","id":"3b75f23b-a350-4ee5-b0ca-01573be1fd1d","originalAuthorName":"夏祥华"},{"authorName":"耿秋菊","id":"17ff1b65-3258-451f-8335-40d1a36ed17c","originalAuthorName":"耿秋菊"},{"authorName":"方莉","id":"5e7472c6-0e73-4a1e-9947-97f8330dceb8","originalAuthorName":"方莉"},{"authorName":"刘贞","id":"8f365462-81f9-40bd-b781-2f9b12a34deb","originalAuthorName":"刘贞"}],"doi":"","fpage":"34","id":"641f8665-98d4-4e63-9b4e-cbfa6c4568d7","issue":"6","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"ecf60e55-7feb-4e21-b65e-4e0d30e3d59e","keyword":"导电布","originalKeyword":"导电布"},{"id":"fe353955-6c46-4768-8e51-57c061fa9c00","keyword":"涤纶","originalKeyword":"涤纶"},{"id":"bc317104-0d53-458f-98a6-2f98cfc33743","keyword":"镍","originalKeyword":"镍"},{"id":"5c992a14-b08c-465e-88e2-2b92edae88f7","keyword":"铜","originalKeyword":"铜"},{"id":"39c1d803-72c9-4137-b9a1-0bce8ed1e221","keyword":"磁控溅射","originalKeyword":"磁控溅射"},{"id":"587e5858-8f1f-4586-9f99-33a84bd41ebe","keyword":"电镀","originalKeyword":"电镀"},{"id":"474dcce2-dd82-42a2-b9be-e65d489a30d4","keyword":"电磁屏蔽","originalKeyword":"电磁屏蔽"}],"language":"zh","publisherId":"ddyts200806011","title":"电磁屏蔽织物的制备及性能表征","volume":"27","year":"2008"},{"abstractinfo":"在已有各种工艺因素对电解涂硅量影响研究的基础上,对在高电流密度(100～200 A/dm2)及短时间(0.1 s)电解条件下电解涂覆薄层(纳米量级)SiO2机理进行了初步研究,实验模拟了实际生产中采用的中间导体法,并运用多种测试方法对电解涂硅的机理进行了分析探讨,揭示了高电流密度下电解脱脂涂硅的吸附本质及SiO2在钢板表面的空间分布,并就钢板阴阳极两面涂硅量的不同原因进行了解释.","authors":[{"authorName":"耿秋菊","id":"40acf5b2-ba8d-407a-96d6-06bf2b55dd2c","originalAuthorName":"耿秋菊"},{"authorName":"周荣明","id":"e35d60c7-875b-45fd-8e0b-2d6646a5dcee","originalAuthorName":"周荣明"},{"authorName":"印仁和","id":"11075cf3-7eb1-45f9-bb46-538b274f2fe0","originalAuthorName":"印仁和"},{"authorName":"郁祖湛","id":"9d5fbf47-37e6-4414-a33c-3b4d3994fbf4","originalAuthorName":"郁祖湛"}],"doi":"10.3969/j.issn.1001-3849.2005.03.002","fpage":"5","id":"6a2fc597-2474-4bcd-9418-406c8e4fa361","issue":"3","journal":{"abbrevTitle":"DDYJS","coverImgSrc":"journal/img/cover/DDYJS.jpg","id":"20","issnPpub":"1001-3849","publisherId":"DDYJS","title":"电镀与精饰 "},"keywords":[{"id":"6b7fbb38-5b9f-41f1-bc43-6cdfde82d85d","keyword":"中间导体法","originalKeyword":"中间导体法"},{"id":"c813f5de-3432-40df-9bc3-17dccf29199e","keyword":"电解涂覆二氧化硅","originalKeyword":"电解涂覆二氧化硅"},{"id":"f264dedd-5e3d-450b-9311-6f269b5e7202","keyword":"纳米","originalKeyword":"纳米"}],"language":"zh","publisherId":"ddjs200503002","title":"冷轧钢板表面电解涂覆薄层二氧化硅过程的研究Ⅱ.机理研究","volume":"27","year":"2005"},{"abstractinfo":"采用IGp-AES法测定冷轧钢板表面涂覆的硅量.钢板尺寸为5 cm×5 cm或直径4 cm,在60℃恒温、体积分数为25%的盐酸溶液中浸渍处理30 s将表面涂层剥离,定容后IGp-AES测定.扣除空白后计算钢板表面涂覆硅量.讨论了酸的种类、酸的浓度、温度对剥离的影响,空白的影响,以及fE对Si分析线的光谱干扰.测定结果准确,与辉光-光谱法测定一致,可用于冷轧钢板表面涂硅量的测定.","authors":[{"authorName":"耿秋菊","id":"53574682-fe30-46b4-b20f-de1786d2f9bd","originalAuthorName":"耿秋菊"},{"authorName":"周荣明","id":"3e17ee02-dab7-4354-bbdd-1fbc55c44459","originalAuthorName":"周荣明"},{"authorName":"印仁和","id":"77c7bd90-bcb2-4b24-93c9-e4976d276f7e","originalAuthorName":"印仁和"},{"authorName":"李慧莉","id":"f11647ff-879e-42d3-896d-08523dcf760c","originalAuthorName":"李慧莉"},{"authorName":"郁祖湛","id":"9591f9f5-9ae7-494c-8ed0-e3dbc5ec1657","originalAuthorName":"郁祖湛"}],"doi":"10.3969/j.issn.1004-227X.2004.04.012","fpage":"42","id":"7b751c3a-a1c1-4ac1-b0b4-81288d3f3489","issue":"4","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"5ca6887c-d6aa-4986-a0b9-4726dbf57844","keyword":"表面涂覆硅量","originalKeyword":"表面涂覆硅量"},{"id":"34d374e2-2559-4710-89be-aa0a25d37de1","keyword":"冷轧钢板","originalKeyword":"冷轧钢板"},{"id":"9c9cd69e-a719-471f-a4b7-1f2de50a0ceb","keyword":"IGp-AES","originalKeyword":"IGp-AES"}],"language":"zh","publisherId":"ddyts200404012","title":"冷轧钢板表面涂硅量的测定","volume":"23","year":"2004"},{"abstractinfo":"采用磁控溅射法在聚对苯二甲酸乙二醇酯(PET)基材上制备了镍薄膜.用扫描电子显微镜(SEM)分析溅射功率、溅射真空室气压等工艺参数对镍薄膜表面形貌的影响;研究了溅射工艺参数与薄膜性能之间的关系.实验结果表明,在室温下,随着溅射气压的增加,沉积速率和粒径都是先增加后又逐渐变小,而薄膜的电阻则随着压强的增大先减小后逐步增大;薄膜的表面粗糙度随着溅射功率的增加而增大;膜层与基材的剥离强度较大且均匀,膜层结合较为牢固,薄膜的耐摩擦性能较为优良.","authors":[{"authorName":"余凤斌","id":"d7764b1d-4d59-4cc0-8644-d8553c5966df","originalAuthorName":"余凤斌"},{"authorName":"夏祥华","id":"ec622951-05a5-48da-80e8-70bc807c4c66","originalAuthorName":"夏祥华"},{"authorName":"于子龙","id":"1cffb73e-e53f-440d-b5a1-f0a0cabc11ea","originalAuthorName":"于子龙"},{"authorName":"耿秋菊","id":"b02fb6dd-d996-4112-8fa4-9327a2996a02","originalAuthorName":"耿秋菊"}],"doi":"10.3969/j.issn.1009-9239.2008.02.016","fpage":"57","id":"c131eb65-df55-4a75-9c0d-2d715843eef6","issue":"2","journal":{"abbrevTitle":"JYCL","coverImgSrc":"journal/img/cover/JYCL.jpg","id":"50","issnPpub":"1009-9239","publisherId":"JYCL","title":"绝缘材料"},"keywords":[{"id":"7cba1119-803c-491d-99c7-0e2dee0218de","keyword":"磁控溅射","originalKeyword":"磁控溅射"},{"id":"6b1ed1e1-51ce-40ec-97c3-3fc07b58b551","keyword":"薄膜","originalKeyword":"薄膜"},{"id":"a2cbc0fe-b1d6-48d1-ba5d-cdb8c1c2cd3f","keyword":"Ni","originalKeyword":"Ni"}],"language":"zh","publisherId":"jycltx200802016","title":"磁控溅射镍膜及其性能的研究","volume":"41","year":"2008"},{"abstractinfo":"随着施镀的进行,化学镀镍液中的硫酸钠和亚磷酸钠的积累越来越多,从而影响镀液的使用寿命.提出了镀液中硫酸钠和亚磷酸钠的处理方法.对于硫酸镍体系,首先将镀液冷却至室温除去过量的硫酸钠晶体,接着在常温下添加Ca(OH)2沉淀除去亚磷酸根离子;对于次磷酸镍体系,直接采用常温下Ca(OH)2沉淀除去亚磷酸根离子的方法.分别测试和对比了2种体系镀液处理前后,镀液和镀层的性能,如镀液各组分浓度、镀液的密度、镀速、镀层应力等.采用化学沉淀法延长化学镀镍液寿命是切实可行的.","authors":[{"authorName":"耿秋菊","id":"78c4ae68-d1c6-469e-aefa-3b56010e4b33","originalAuthorName":"耿秋菊"},{"authorName":"周荣明","id":"7cdb2552-23b4-498b-b93a-7c9362ca8a68","originalAuthorName":"周荣明"},{"authorName":"印仁和","id":"404949fe-c8f1-4561-9dd7-f9060ff2c672","originalAuthorName":"印仁和"},{"authorName":"贺延峰","id":"f2467c88-229d-4028-8105-5ae7297922a3","originalAuthorName":"贺延峰"},{"authorName":"孙江燕","id":"37b3968d-ab8d-43c4-979a-af4a81855e26","originalAuthorName":"孙江燕"},{"authorName":"郁祖湛","id":"beb27e50-3777-40ea-8e74-96e899697f10","originalAuthorName":"郁祖湛"}],"doi":"10.3969/j.issn.1004-227X.2006.01.003","fpage":"11","id":"cb162e96-bcc5-458a-9ae1-173374054d2e","issue":"1","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"2b6faf19-d451-4f98-ac28-b08338fe5123","keyword":"化学镀镍","originalKeyword":"化学镀镍"},{"id":"c403129f-8167-4e74-92ac-373e0569a53e","keyword":"镀液寿命","originalKeyword":"镀液寿命"},{"id":"a607c252-51d3-4760-b640-83afb4423714","keyword":"硫酸钠","originalKeyword":"硫酸钠"},{"id":"d41c1185-e48d-4f3c-85d9-ca217d54e2dc","keyword":"亚磷酸钠","originalKeyword":"亚磷酸钠"},{"id":"1e7085ee-d607-43c4-9f4d-b7804c1248e0","keyword":"化学沉淀法","originalKeyword":"化学沉淀法"},{"id":"f2929095-4d8a-457b-9005-3af68a1fd8ab","keyword":"Ca(OH)2","originalKeyword":"Ca(OH)2"}],"language":"zh","publisherId":"ddyts200601003","title":"延长化学镀镍液寿命的研究","volume":"25","year":"2006"},{"abstractinfo":"为提高低温氯化物电镀铁溶液的稳定性,采用赫尔槽试验和阴极极化曲线测量方法,研究了5种稳定剂对镀层光亮区、阴极极化过程以及镀铁液稳定性的影响.试验结果表明,取抗坏血酸13 mL/L(10%,质量分数,以下同)、氨基酸5 mL/L(10%)、氟化物8 mL/L(10%)组成的复合稳定剂,不仅能显著增大低温氯化物电镀铁镀层光亮区范围,而且当Jk在2～15 A/dm2范围内时,还提高了镀液的阴极极化能力,镀液在敞口的小烧杯中,出现沉淀的时间是305 h.","authors":[{"authorName":"耿秋菊","id":"eec94380-9ea7-493b-98c4-bc7e4d33bbbd","originalAuthorName":"耿秋菊"},{"authorName":"冯立明","id":"d9e94f2c-2d21-45f8-9e8b-017ed863855a","originalAuthorName":"冯立明"},{"authorName":"夏祥华","id":"7fe5f3d5-d710-4ea1-a29a-0c4f7a114806","originalAuthorName":"夏祥华"}],"doi":"10.3969/j.issn.1004-227X.2007.08.004","fpage":"14","id":"172dd138-0c5e-4acf-905f-b8f6f07aa3fd","issue":"8","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"2dbe7e05-9933-424b-be80-70a93803a798","keyword":"电镀铁","originalKeyword":"电镀铁"},{"id":"eb31f8f5-e833-457b-a2ef-28145dd3e3f1","keyword":"氯化物","originalKeyword":"氯化物"},{"id":"565780c1-2f5b-4a4c-a77f-762e28739577","keyword":"低温","originalKeyword":"低温"},{"id":"d1e23307-11c9-4966-8595-16b05c28e5cf","keyword":"稳定剂","originalKeyword":"稳定剂"},{"id":"6cdf8f51-5edd-440c-b377-13c1639cbf3b","keyword":"光亮区","originalKeyword":"光亮区"},{"id":"77ee7edc-91ef-41c0-a629-1bca08d96c6f","keyword":"阴极极化","originalKeyword":"阴极极化"}],"language":"zh","publisherId":"ddyts200708004","title":"低温氯化物电镀铁溶液的稳定剂研究","volume":"26","year":"2007"},{"abstractinfo":"为更好地评价变压器油的绝缘性能，对不同水分含量下的变压器油进行了工频击穿测试，分别利用正态分布、耿贝尔分布和威布尔分布等统计方法对变压器油的击穿电压进行对比分析，研究不同的统计方法对评估变压器油绝缘性能的适用性。结果表明：大量的重复击穿试验会使变压器油中水分的形态发生变化，从而使得变压器油的击穿电压升高；三参数的威布尔分布能够较好地拟合不同水分含量下变压器油的击穿电压结果，并且位置参数为评价变压器油的绝缘性能提供了直观的依据。","authors":[{"authorName":"周游","id":"546d55fa-a46a-4871-82fa-10f81b6407cc","originalAuthorName":"周游"},{"authorName":"江军","id":"54dc15af-d231-4475-92f9-715105c0ab0a","originalAuthorName":"江军"},{"authorName":"罗颖婷","id":"67a8b652-4355-4c25-995c-732e7d19568f","originalAuthorName":"罗颖婷"},{"authorName":"吴昊","id":"101068ca-f1b9-414b-929d-8bcb4385e0fa","originalAuthorName":"吴昊"},{"authorName":"吕玉珍","id":"8d69239f-7157-4ada-b0f6-0d345ea8cb70","originalAuthorName":"吕玉珍"},{"authorName":"李成榕","id":"0f77a118-ddc8-4099-84e5-42aed1a3b7e3","originalAuthorName":"李成榕"}],"doi":"","fpage":"73","id":"511974c9-821e-4e96-b394-4b9d3961d4a3","issue":"3","journal":{"abbrevTitle":"JYCL","coverImgSrc":"journal/img/cover/JYCL.jpg","id":"50","issnPpub":"1009-9239","publisherId":"JYCL","title":"绝缘材料"},"keywords":[{"id":"5b2fd2df-da30-416b-8abe-5325b9f73c0c","keyword":"变压器油","originalKeyword":"变压器油"},{"id":"911ce951-7066-4372-954d-25daa99a5bb6","keyword":"击穿电压","originalKeyword":"击穿电压"},{"id":"c01f29b4-732f-4aa7-a312-a70a80ff8b70","keyword":"水分","originalKeyword":"水分"},{"id":"16eba297-5157-4a5d-90e0-8db21e41203f","keyword":"统计学","originalKeyword":"统计学"},{"id":"e16d2930-042e-4a44-94b1-fa6d1d01eac9","keyword":"威布尔分布","originalKeyword":"威布尔分布"}],"language":"zh","publisherId":"jycltx201503015","title":"变压器油工频电压击穿特性的统计研究","volume":"","year":"2015"}],"totalpage":1,"totalrecord":9}