欢迎登录材料期刊网

材料期刊网

高级检索

纳米压痕测试结果是材料微观力学性能本质属性的体现.本文简述了水泥基材料中应用纳米压痕技术的测试要求,揭示了水化浆体中各物相的微观结构与力学性能,尤其对水化硅酸钙(C-S-H)凝胶在纳米尺度的结构特征与力学性能进行了重点分析.同时利用纳米压痕在界面区微结构特征测试方面的优势,介绍了不同组分水泥基材料界面区的微观力学性能差异.另外概述了水泥基材料中加入矿物细掺料、纳米材料后C-S-H的变化规律,这为后续纳米压痕在水泥基材料微观力学性能研究、宏观性能优化等方面提供参考和依据.

参考文献

[1] W.C. Oliver;G.M. Pharr.Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology[J].Journal of Materials Research,20041(1):3-20.
[2] I.Zyganitidis;M. Stefanidou;N. Kalfagiannis.Nanomechanical characterization of cement-based pastes enriched with SiO_2 nanoparticles[J].Materials Science & Engineering, B. Solid-State Materials for Advanced Technology,201119(19):1580-1584.
[3] Jin Nemecek.Creep effects in nanoindentation of hydrated phases of cement pastes[J].Materials Characterization,20099(9):1028-1034.
[4] Pavel Trtik;Beat Munch;Pietro Lura.A critical examination of statistical nanoindentation on model materials and hardened cement pastes based on virtual experiments[J].Cement & concrete composites,200910(10):705-714.
[5] G. Constantinides;K.S. Ravi Chandran;F.-J. Ulm;K.J. Van Vliet.Grid indentation analysis of composite microstructure and mechanics: Principles and validation[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,20061/2(1/2):189-202.
[6] Randall, NX;Vandamme, M;Ulm, FJ.Nanoindentation analysis as a two-dimensional tool for mapping the mechanical properties of complex surfaces[J].Journal of Materials Research,20093(3):679-690.
[7] Christopher A. Jones;Zachary C. Grasley;James A. Ohlhausen.Measurement of elastic properties of calcium silicate hydrate with atomic force microscopy[J].Cement & concrete composites,20124(4):468-477.
[8] Paramita Mondal;Surendra P. Shah;Laurence Marks.A reliable technique to determine the local mechanical properties at the nanoscale for cementitious materials[J].Cement and Concrete Research,200710(10):1440-1444.
[9] Georgios Constantinides;Franz-Josef Ulm.The effect of two types of C-S-H on the elasticity of cement-based materials: Results from nanoindentation and micromechanical modeling[J].Cement and Concrete Research,20041(1):67-80.
[10] Ju-Young Kim;Jung-Jun Lee;Yun-Hee Lee.Surface roughness effect in instrumented indentation: A simple contact depth model and its verification[J].Journal of Materials Research,200612(12):2975-2978.
[11] 姚武;何莉;梁慷.应用纳米压痕技术表征水化硅酸钙凝胶[J].建筑材料学报,2010(3):277-280.
[12] D. Davydov;M. Jirasek;L. Kopecky.Critical aspects of nano-indentation technique in application to hardened cement paste[J].Cement and Concrete Research,20111(1):20-29.
[13] 姚武;梁慷;何莉.水化硅酸钙凝胶的弹塑性和徐变特性[J].材料研究学报,2010(2):123-128.
[14] 姚武;何莉.水化硅酸钙纳米结构研究进展[J].硅酸盐学报,2010(4):754-761.
[15] Ch. Pichler;R. Lackner.Identification of Logarithmic-Type Creep of Calcium-Silicate-Hydrates by Means of Nanoindentation[J].Strain,20091(1):17-25.
[16] Wenzhong Zhu;John J. Hughes;Nenad Bicanic.Nanoindentation mapping of mechanical properties of cement paste and natural rocks[J].Materials Characterization,200711/12(11/12):1189-1198.
[17] Matthieu Vandamme;Franz-Josef Ulm;Philip Fonollosa.Nanogranular packing of C-S-H at substochiometric conditions[J].Cement and Concrete Research,20101(1):14-26.
[18] Paramita Mondal;Surendra P. Shah;Laurence D. Marks.Nanoscale Characterization of Cementitious Materials[J].ACI materials journal,20082(2):174-179.
[19] Xiao Hui Wang;Stefan Jacobsen;Jian Ying He.Application of nanoindentation testing to study of the interfacial transition zone in steel fiber reinforced mortar[J].Cement and Concrete Research,20098(8):701-715.
[20] Shiho Kawashima;Pengkun Hou;David J. Corr.Modification of cement-based materials with nanoparticles[J].Cement & concrete composites,2013:8-15.
[21] 周伟玲;孙伟;陈翠翠;缪昌文.纳米压痕技术研究磨细矿渣对水泥基材料微观力学性能的影响[J].硅酸盐学报,2011(4):718-725.
[22] 刘仍光;韩方晖;阎培渝.纳米压痕研究含矿渣硬化浆体C-S-H凝胶的特性[J].中国科学(技术科学),2013(8):912-920.
[23] 周伟玲;孙伟;陈翠翠;缪昌文.应用纳米压痕技术表征水泥基材料微观力学性能[J].东南大学学报(自然科学版),2011(2):370-375.
[24] 郑克仁;孙伟;林玮;赵庆新;张云升.界面过渡区微力学性质对高周疲劳性能的影响[J].三峡大学学报(自然科学版),2006(4):305-308.
[25] Maria S. Konsta-Gdoutos;Zoi S. Metaxa;Surendra P. Shah.Highly dispersed carbon nanotube reinforced cement based materials[J].Cement and Concrete Research,20107(7):1052-1059.
[26] Maria S. Konsta-Gdoutos;Zoi S. Metaxa;Surendra P. Shah.Multi-scale mechanical and fracture characteristics and early-age strain capacity of high performance carbon nanotube/cement nanocomposites[J].Cement & concrete composites,20102(2):110-115.
[27] Y. Saez de Ibarra;J. J. Gaitero;E. Erkizia;I. Campillo.Atomic force microscopy and nanoindentation of cement pastes with nanotube dispersions[J].Physica Status Solidi, A. Applied Research,20066(6):1076-1081.
[28] 戎志丹;姜广;孙伟.纳米SiO和CaCO3对超高性能水泥基复合材料的影响[J].东南大学学报(自然科学版),2015(2):393-398.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%