氧化还原法制备SnO2纳米棒的研究

材料导报, 2004, 18(4): 96-103.

氧化还原法制备SnO2纳米棒的研究

赵鹤云 ^1, , 杨留方 ^2, , 朱文杰 ^3, , 柳清菊 ^4, , 吴兴惠 ^5,

1.云南大学化学与材料工程学院材料科学与工程系,昆明,650091

2.云南大学化学与材料工程学院材料科学与工程系,昆明,650091

3.云南大学化学与材料工程学院材料科学与工程系,昆明,650091

4.云南大学化学与材料工程学院材料科学与工程系,昆明,650091

5.云南大学化学与材料工程学院材料科学与工程系,昆明,650091

基金项目: 云南省自然科学基金(2000E002Z) 云南省教育厅资助项目(0111164)

关键词：氧化还原 , 纳米棒 , 微乳液 , 熔盐

Study on the SnO2 Nanorods Synthesized by Oxidation-Reduction

在聚氧乙烯五醚(NP5)、聚氧乙烯九醚(NP9)和环己烷组成的微乳体系中用氧化还原法制备SnO2前驱物,然后在熔盐中再经800℃、860℃焙烧2.5h,成功地制备了金红石结构的SnO2纳米棒,并用透射电子显微镜,X射线衍射对SnO2纳米棒的结构进行了表征.

参考文献

[1]	Iijima S Helical .Microtubules of graphitic carbon[J].Nature,1991,354:56.
[2]	Trentler T J;Hickman K M;Buhro W E et al.Solution-liquid- solid growth of crystalline Ⅲ-Ⅴ semiconductors-An analogy to vapor-liquid-solid growth[J].Science,1995,270:1791.
[3]	Fasol G .Applied physics-Nanowires:Small is beautiful[J].Science,1998,280:545.
[4]	PAN Z W;Dai Z R;Wang Z L .Nanobelts of semiconducting oxides[J].Science,2001,291:1947.
[5]	Lampert C M .[J].Solar Energy Materials and Solar Cells,1991,6:1.
[6]	Nayal C;Viala C;Colliere V et al.[J].Journal of Applied Surface Science,2000,164:219.
[7]	Petit C.;Pileni M.P.;Taleb A. .Cobalt nanosized particles organized in a 2D superlattice: Synthesis, characterization, magnetic properties[J].The journal of physical chemistry, B. Condensed matter, materials, surfaces, interfaces & biophysical,1999(11):1805-1810.
[8]	麦振洪,赵永男.微乳液技术制备纳米材料[J].物理,2001(02):106-110.
[9]	Trentler T J;Hickman K M;Buhro W E et al.Solution-liquid- solid growth of crystalline Ⅲ-Ⅴ semiconductors-An analogy to vapor-liquid-solid growth[J].Science,1995,270:1791.
[10]	Morlaes A M;Lieber C M .Semiconductor nanowires[J].Science,1998,279:208.
[11]	Dingman S D;Rath N P;Markowitz P D et al.[J].Angrew Chem,2000,112:1530.
[12]	Yoon KH.;Kang DH.;Cho YS. .Molten salt synthesis of lead-based relaxors [Review][J].Journal of Materials Science,1998(12):2977-2984.
[13]	Ito Y;Shi S;Kimura T et al.[J].Journal of the American Ceramic Society,1995,78:2695.
[14]	Yoon KH.;Kang DH.;Cho YS. .Molten salt synthesis of lead-based relaxors [Review][J].Journal of Materials Science,1998(12):2977-2984.
[15]	Wada H;Sakane K;Kitamura T .[J].Journal of Materials Science Letters,1991,10:1076.
[16]	HashimotoS;Yamaguchi A .[J].Journal of the European Ceramic Society,2000,20:397.

上一张下一张

计量

下载量()
访问量()

作者相关

文章评分

您的评分：
1

0%
2

0%
3

0%
4

0%
5

0%

材料期刊网

氧化还原法制备SnO2纳米棒的研究

Study on the SnO2 Nanorods Synthesized by Oxidation-Reduction

参考文献