{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用液相化学还原法,通过正交试验优化得到高振实密度超细银粉的制备工艺;制备的超细银粉为球形、表面光洁、无团聚,d90、d50、d10与平均粒径d分别为1.85、0.79、0.34、1.11 μm,振实密度高达4.5 g/cm3.试验结果表明,在银粉的还原生成反应中,溶剂去离子水用量与分散剂用量是其中两个主要的影响振实密度的因素.","authors":[{"authorName":"周宇松","id":"5d5a99c2-401d-4eca-9b57-82e9627d25ec","originalAuthorName":"周宇松"},{"authorName":"曹国洲","id":"05999a1c-1c4b-4849-b954-af92bc5150c7","originalAuthorName":"曹国洲"},{"authorName":"逯庆国","id":"2c8e5a8c-f47a-4c63-97e7-707a39cb9917","originalAuthorName":"逯庆国"},{"authorName":"侯小宝","id":"7df3c6eb-d36e-4aa9-b6ba-e85d6484524f","originalAuthorName":"侯小宝"},{"authorName":"龚朝辉","id":"18ac8a63-d69f-4d5d-a663-b8a2294208b0","originalAuthorName":"龚朝辉"},{"authorName":"郭红燕","id":"0ea4172d-a58d-46e5-adcd-029b10c488c5","originalAuthorName":"郭红燕"},{"authorName":"吴敏","id":"f7167409-53e2-44b8-9aef-bf5d474e1577","originalAuthorName":"吴敏"}],"doi":"10.3969/j.issn.1004-244X.2007.05.006","fpage":"22","id":"851a1377-9055-43ad-9511-670fe53c5136","issue":"5","journal":{"abbrevTitle":"BQCLKXYGC","coverImgSrc":"journal/img/cover/BQCLKXYGC.jpg","id":"4","issnPpub":"1004-244X","publisherId":"BQCLKXYGC","title":"兵器材料科学与工程 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mg/kg,实际样品分析的相对标准偏差小于4.8%,样品加权平均回收率为99.2%,能满足镀层有害物质检测的相关规定要求.","authors":[{"authorName":"朱晓艳","id":"41463c07-5c57-4a54-8f62-44c527a1d7ef","originalAuthorName":"朱晓艳"},{"authorName":"曹国洲","id":"7a47fc64-39dd-41c8-b344-1817c5e89ad9","originalAuthorName":"曹国洲"},{"authorName":"黄振华","id":"71dd61c6-0710-4c41-a9a7-6e571c64d7af","originalAuthorName":"黄振华"},{"authorName":"旷亚非","id":"c12008ae-9e03-40b0-909b-ab57e37e5ca5","originalAuthorName":"旷亚非"},{"authorName":"朱丽辉","id":"af0cd70f-f69b-4d5f-b011-f9cb2c8abeea","originalAuthorName":"朱丽辉"}],"doi":"","fpage":"35","id":"3e125cac-0443-4b24-82e6-d3abf6f0d092","issue":"1","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"dc470d46-34c4-4fd7-84c3-d1ac9de24ce5","keyword":"铜基镀银","originalKeyword":"铜基镀银"},{"id":"bf11fc7e-99a4-4bc0-9e69-f32ca52a9be9","keyword":"镉","originalKeyword":"镉"},{"id":"b7311dd0-f6c0-4995-b848-2276b8e5fff6","keyword":"退镀","originalKeyword":"退镀"},{"id":"30fa21d4-5e1c-4c6c-b972-f50fc89c636b","keyword":"电感耦合等离子质谱","originalKeyword":"电感耦合等离子质谱"},{"id":"c88ddce5-d0fd-48de-9a3f-c44dc6192662","keyword":"检测","originalKeyword":"检测"}],"language":"zh","publisherId":"ddyts201001012","title":"铜基镀银层中镉含量的测定","volume":"29","year":"2010"},{"abstractinfo":"将金属镀镍材料在210 ℃、10%(体积分数)的HCI中退镀15 min,然后用电感耦合等离子体质谱仪(ICP-MS)测定退镀液中铅和镉含量.根据退镀量及所测含量,计算出镀层中铅和镉的含量.该方法的铅、镉检出限分别为0.10 mg/kg和0.18 mg/kg,实际样品分析的相对标准偏差分别为3.33%和4.07%,加标平均回收率为94.5%~107%,能满足镀层有害物质检测相关规定的要求.","authors":[{"authorName":"朱晓艳","id":"e8fe8588-5646-4b0b-8d28-7a2143f5f197","originalAuthorName":"朱晓艳"},{"authorName":"曹国洲","id":"bb24383b-d6d9-4067-9a0b-a73574944d60","originalAuthorName":"曹国洲"},{"authorName":"黄振华","id":"7d501f5d-12c0-43a3-ae88-a7b041363265","originalAuthorName":"黄振华"},{"authorName":"旷亚非","id":"48f1d28d-16b0-42ce-a09d-b0bc83e808a8","originalAuthorName":"旷亚非"},{"authorName":"朱丽辉","id":"8880fab4-9e4b-484a-a4e2-a529ed1e47f7","originalAuthorName":"朱丽辉"}],"doi":"","fpage":"35","id":"511a44ec-5a7c-480d-b1c4-623ea21afcb0","issue":"7","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 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mm钢板的抗拉强度和延伸率不符合该船级社的技术要求,通过对材料化学成分、力学性能和金相组织的检验,认为,材料存在带状组织是导致钢板力学性能不合格的主要原因.","authors":[{"authorName":"曹国洲","id":"6dd5a08f-acc1-4dbe-96d3-0b664d160e47","originalAuthorName":"曹国洲"},{"authorName":"王谦","id":"b0c4756f-5d47-47ba-900d-2619dcc6219e","originalAuthorName":"王谦"}],"doi":"10.3969/j.issn.1004-244X.2009.03.024","fpage":"77","id":"5fa7b5eb-975a-4c74-abf8-3599fea2926f","issue":"3","journal":{"abbrevTitle":"BQCLKXYGC","coverImgSrc":"journal/img/cover/BQCLKXYGC.jpg","id":"4","issnPpub":"1004-244X","publisherId":"BQCLKXYGC","title":"兵器材料科学与工程 "},"keywords":[{"id":"c74458d9-9493-45d7-85b2-ce98582f5c42","keyword":"AH36钢","originalKeyword":"AH36钢"},{"id":"adca2856-5a8f-4d6b-aa52-27a59357fe92","keyword":"带状组织","originalKeyword":"带状组织"},{"id":"9f5a835a-b0d9-48e6-af1e-32d63ef0c77f","keyword":"不合格分析","originalKeyword":"不合格分析"}],"language":"zh","publisherId":"bqclkxygc200903024","title":"高强度船用钢板AH36力学性能不合格原因分析","volume":"32","year":"2009"},{"abstractinfo":"对炼油厂典型的恶臭、有毒有害气体硫化氢、甲硫醇与乙硫醇进行了纳米光催化净化分解模拟试验,在此基础上研制出纳米光催化空气净化样机,并对样机进行了初步测试.","authors":[{"authorName":"周宇松","id":"0c721d9f-6e15-4e2a-b8dc-64ac55b47e0e","originalAuthorName":"周宇松"},{"authorName":"聂通元","id":"1fa6542c-410b-4be6-b466-9e49ea344548","originalAuthorName":"聂通元"},{"authorName":"曹国洲","id":"8bb912f9-ed09-4aa4-95ff-45f1e58c83e6","originalAuthorName":"曹国洲"},{"authorName":"王铭","id":"b9d3955b-bd81-4817-ac02-b7cef39370df","originalAuthorName":"王铭"},{"authorName":"檀革江","id":"ec3d902d-bc92-4bdd-953a-910984dc459e","originalAuthorName":"檀革江"},{"authorName":"陈良灯","id":"d3560969-dc11-4573-a83c-3b779793b478","originalAuthorName":"陈良灯"}],"doi":"","fpage":"66","id":"8faf64ea-dc53-46fc-a8b6-8be979bd629d","issue":"7","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"63ebe181-4e72-4231-a5c5-52f9cce81523","keyword":"纳米光催化剂","originalKeyword":"纳米光催化剂"},{"id":"10ef5e63-c16a-48f0-b7b3-8d84f519d4d0","keyword":"光催化分解","originalKeyword":"光催化分解"},{"id":"9d389b98-be6a-45fc-9738-216fa1e91a91","keyword":"硫化氢","originalKeyword":"硫化氢"},{"id":"789ab28e-80d6-4a63-be5b-dcccb8111b87","keyword":"甲硫醇","originalKeyword":"甲硫醇"},{"id":"d2d5219b-4326-41f9-9979-35074e0426ca","keyword":"乙硫醇","originalKeyword":"乙硫醇"}],"language":"zh","publisherId":"cldb200207021","title":"纳米光催化净化分解炼化厂恶臭有毒气体研究","volume":"16","year":"2002"},{"abstractinfo":"在150℃下,先用50g/L的氢氧化钠溶液使铜基镀锡材料退镀,再用体积分数为10%的盐酸二次退镀,将两次退镀液分别定容到100 mL,稀释5倍后,用电感耦合等离子体质谱测定退镀液中的铅含量.此方法检出限为1 mg/kg,实际样品分析的相对标准偏差为2.7%,平均回收率为99.9%.该方法能满足欧盟RoHS指令以及食品接触材料中铅含量检测的要求.","authors":[{"authorName":"曹国洲","id":"9d828235-cbd1-47db-980e-8cd2ab5c7922","originalAuthorName":"曹国洲"},{"authorName":"朱晓艳","id":"8eb556f3-d6ec-4d32-a654-49481c38a9a2","originalAuthorName":"朱晓艳"},{"authorName":"朱丽辉","id":"43b5fe3d-0ce2-49ef-9cab-67d07b41ebcc","originalAuthorName":"朱丽辉"},{"authorName":"金献忠","id":"92eb9ec0-1156-407e-bc4a-af8bfbbcc725","originalAuthorName":"金献忠"},{"authorName":"王谦","id":"f6aa749d-f1b3-4ead-973d-97befba93744","originalAuthorName":"王谦"}],"doi":"","fpage":"29","id":"fa79e38e-f172-45ad-9f86-9c014aab474e","issue":"10","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 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"},"keywords":[{"id":"6bd47d99-21c7-4c41-b557-8cc8332aa638","keyword":"硅","originalKeyword":"硅"},{"id":"14954a7f-4668-4c22-a980-a18292f2dd95","keyword":"铝合金","originalKeyword":"铝合金"},{"id":"9e69c220-52ce-4dd8-9725-3d410791a137","keyword":"微波消解","originalKeyword":"微波消解"},{"id":"fae76201-1a53-4350-95a2-169b280e9218","keyword":"ICP-AES","originalKeyword":"ICP-AES"}],"language":"zh","publisherId":"yjfx200101022","title":"微波消解ICP-AES法测定铝合金中高含量硅","volume":"21","year":"2001"},{"abstractinfo":"某公司生产的一批400HRB热轧带肋钢筋在进行出厂检验时发现屈服强度达不到要求.通过对钢筋成分、力学性能、金相组织和生产工艺等分析.结果表明,组织中晶粒粗大是导致钢筋屈服强度降低的主要原因,而轧制温度过高是引起晶粒粗大的的直接原因.从而提出控制轧制温度及采用V、Ti、Nb微合金化等方法来细化晶粒,改善钢筋的综合性能的建议.","authors":[{"authorName":"曹国洲","id":"1aa901e8-55ca-45a6-b80f-90e9f5ced8ab","originalAuthorName":"曹国洲"},{"authorName":"李国伟","id":"6edc0733-41ad-4d15-bb99-618cd7ebd6ff","originalAuthorName":"李国伟"},{"authorName":"朱晓艳","id":"6375da09-6ac7-45fb-a1e1-de1eb140fe01","originalAuthorName":"朱晓艳"}],"doi":"10.3969/j.issn.1004-244X.2008.05.012","fpage":"41","id":"f18e0771-6300-4e6e-84eb-2a03322f31de","issue":"5","journal":{"abbrevTitle":"BQCLKXYGC","coverImgSrc":"journal/img/cover/BQCLKXYGC.jpg","id":"4","issnPpub":"1004-244X","publisherId":"BQCLKXYGC","title":"兵器材料科学与工程 "},"keywords":[{"id":"cd749123-0693-4d91-8a08-46ccd3d5958e","keyword":"20MnSi","originalKeyword":"20MnSi"},{"id":"0451946b-c57e-467c-bdac-e577381f419f","keyword":"热轧钢筋","originalKeyword":"热轧钢筋"},{"id":"3e4ff7d7-6630-4298-b678-d7b94658247e","keyword":"屈服强度偏低","originalKeyword":"屈服强度偏低"}],"language":"zh","publisherId":"bqclkxygc200805012","title":"20MnSi热轧带肋钢筋强度偏低原因分析","volume":"31","year":"2008"},{"abstractinfo":"针对曹家埠金矿缓倾斜薄矿体,概述分析了其采矿方法的演变过程和存在问题;介绍了适合该类型矿体回采的小进路全面采矿法和短壁式崩落采矿法的试验应用情况,试验取得了较好的技术经济效果,为推广应用奠定了基础.","authors":[{"authorName":"滕建军","id":"926e2350-3db8-4de1-9bec-88579aaec1c2","originalAuthorName":"滕建军"},{"authorName":"何顺斌","id":"c9d2b3f7-9acb-4509-b53f-1c08b86a4ad9","originalAuthorName":"何顺斌"},{"authorName":"李威","id":"62e2065f-6216-406a-ba1a-39bc68394fc2","originalAuthorName":"李威"},{"authorName":"张益岭","id":"25c6c09b-c6ff-4ce3-8947-6438d695fc3e","originalAuthorName":"张益岭"}],"doi":"10.3969/j.issn.1001-1277.2008.02.007","fpage":"26","id":"b1531df0-7a9a-44dc-85ca-94b393bc5772","issue":"2","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"54b6c08b-d974-425d-a7cd-cb5d16eea74e","keyword":"缓倾斜","originalKeyword":"缓倾斜"},{"id":"c8a64ad9-1717-4906-8653-f83137f7d8b8","keyword":"薄矿体","originalKeyword":"薄矿体"},{"id":"20b40bca-aea4-42fa-a883-a6a106c16a50","keyword":"采矿方法","originalKeyword":"采矿方法"}],"language":"zh","publisherId":"huangj200802007","title":"曹家埠金矿缓倾斜薄矿体回采实践","volume":"29","year":"2008"},{"abstractinfo":"通过在台洲海轮上进行的实船试验,研究了压载水舱在两个浸水周期中的保护电位变化以及四年实船试验的保护度与保护电流密度的关系。","authors":[{"authorName":"吴建华","id":"fb43e3f9-1d7b-489a-93ac-8aafd1698d25","originalAuthorName":"吴建华"},{"authorName":"陈仁兴","id":"28fc9591-5cdf-4023-8968-b0c00de79bb4","originalAuthorName":"陈仁兴"},{"authorName":"刘光洲","id":"b8e9d672-64fb-47d1-b62d-29a6b8f0fb9a","originalAuthorName":"刘光洲"},{"authorName":"陈光章","id":"f6e70b99-ceb1-45cb-a0a3-4cbffce30503","originalAuthorName":"陈光章"},{"authorName":"王志学","id":"634624ff-2689-4dee-9886-488d2335af9f","originalAuthorName":"王志学"},{"authorName":"郭卫华","id":"373dce07-1814-4855-957c-c0b2091a7f65","originalAuthorName":"郭卫华"},{"authorName":"张殿平","id":"436a63be-97e4-4372-b4ca-65e659313fd2","originalAuthorName":"张殿平"},{"authorName":"运德才","id":"b6be20e0-bb0d-4ea5-9e80-2b1840949d83","originalAuthorName":"运德才"},{"authorName":"邹立卿","id":"79ece413-81a8-40ad-bb28-2c05f4f36f67","originalAuthorName":"邹立卿"}],"categoryName":"|","doi":"","fpage":"297","id":"5a2fa7b5-4171-4c33-bc8b-b95e4b572bbd","issue":"4","journal":{"abbrevTitle":"ZGFSYFHXB","coverImgSrc":"journal/img/cover/中国腐蚀封面19-3期-01.jpg","id":"81","issnPpub":"1005-4537","publisherId":"ZGFSYFHXB","title":"中国腐蚀与防护学报"},"keywords":[{"id":"a47de3b7-fbde-4757-baaf-bed8cfc850f3","keyword":"压载水舱","originalKeyword":"压载水舱"},{"id":"f14d81f0-bc88-431b-aa44-51b888f9352e","keyword":" 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