欢迎登录材料期刊网

材料期刊网

高级检索

采用超声-脉冲电铸工艺在覆铜板表面的微区域内制备了镍铸层,用扫描电镜观察镍铸层的表面形貌,并采用Image Tool软件测量了镍铸层的平均晶粒尺寸,研究了超声波功率及方向、脉冲平均电流密度、脉冲占空比等对镍铸层晶粒尺寸的影响。结果表明:其他条件相同时,双向(y向和z向)超声波制备镍铸层的晶粒尺寸小于相同功率单向(y向或z向)超声制备的;随着超声波功率、脉冲平均电流密度的增大,镍铸层的晶粒尺寸先减小后增大;当脉冲占空比由10%增大到30%时,晶粒尺寸由0.97μm增大到3.32μm。

The nickel electroforming layer was prepared by ultrasonic-pulse electroforming process in the micro-region on employed copper clad laminate(CCL) surface.The surface morphology of nickel electroforming layer was observed by scanning electron microscopy and the average grain size was measured by Image Tool software,and the effects of ultrasonic power and direction,pulse average current density and pulse duty ratio on the grains size of nickel electroforming layer were studied.The results show that when other conditions were remained unchanged,the grain size of nickel electroforming layer prepared under double-direction ultrasonic(y direction and z direction) was less than that under single-direction ultrasonic(y direction or z direction).And the grain size of nickel eletroforming layer decreased first and then increased with the increase of ultrasonic power and the pulse average current density.The grain size of nickel electroforming layer increased from 0.97 μm to 3.32 μm when the pulse duty ratio increased from 10% to 30%.

参考文献

[1] 范爱玲,贺怀堂,田文怀,孙起.电铸超细晶材料的微观组织研究[J].太原重型机械学院学报,2003(02):88-91.
[2] 赵阳培,黄因慧,张君伟,刘志东,田宗军,赵剑峰,花国然.脉冲射流电铸纳米晶铜的组织与性能[J].机械工程材料,2006(06):87-90.
[3] 吴蒙华,傅欣欣,李智,夏法锋.超声电沉积镍/纳米碳化硅复合镀层组织结构研究[J].机械工程材料,2004(12):46-48.
[4] 夏法锋,吴蒙华,贾振元,李智.超声波对纳米Ni-TiN复合镀层的影响[J].功能材料,2008(04):690-691,694.
[5] 明平美,朱荻,胡洋洋,曾永彬.超声微细电铸试验研究[J].中国机械工程,2008(06):644-647.
[6] 肖日松 .微电铸工艺参数对模具质量影响研究[D].大连理工大学,2006.
[7] 吴蒙华,李智,夏法锋,陈丽燕.超声电沉积制备纳米金属陶瓷复合镀层工艺[J].机械工程材料,2005(08):58-61.
[8] 方小红.超声波电镀镍及镍基复合镀层的研究进展[J].材料保护,2008(05):58-61.
[9] 杨艳玲,申勇峰,陈进耿,王沿东.超声波搅拌-脉冲电沉积法制备纳米镍[J].金属学报,2007(08):883-888.
[10] 张俊,裴和中,张国亮.超细晶镍钴合金的电铸工艺[J].材料保护,2010(01):36-37.
[11] 解西锋,朱荻.高频脉冲电铸的试验研究[J].航空精密制造技术,2003(02):10-13,33.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%