采用弧辉等离子沉积工艺在镁合金AZ91表面涂覆了TiN薄膜.研究了沉积温度对膜层的厚度、结合力及硬度的影响.用扫描电镜(SEM)、X射线衍射(XRD)和辉光放电光谱(GDS)分析了涂层的成分和微观结构.结果表明,随着控制温度的升高,膜层厚度呈缓慢增加的趋势,但温度过高或过低结合力明显下降,以160~180℃最佳.180℃时的硬度HK0.01最高,达14 630 MPa.
参考文献
[1] | Gray J E;Luan B .[J].Journal of Alloys and Compounds,2002,336:113. |
[2] | Rajan Ambat;Naing Aung;Zhou W .[J].Corrosion Science,2000,42:1433. |
[3] | 刘正,王越,王中光,李锋,申志勇.镁基轻质材料的研究与应用[J].材料研究学报,2000(05):449-456. |
[4] | Dutta Majumdar J;Ramesh Chandra B;Galun R et al.[J].Composites Science and Technology,2003,63:771. |
[5] | El-Baradie Z M .[J].Materials Letters,2003,57:3269. |
[6] | Stippich F.;Wolf GK.;Berg G.;Friedrich C.;Vera E. .Enhanced corrosion protection of magnesium oxide coatings on magnesium deposited by ion beam-assisted evaporation[J].Surface & Coatings Technology,1998(0):29-35. |
[7] | Mathieu S;Rapin C;Steinmetz J et al.[J].Corrosion Science,2003,45:2741. |
[8] | 曾荣昌,柯伟,徐永波,韩恩厚,朱自勇.Mg合金的最新发展及应用前景[J].金属学报,2001(07):673-685. |
[9] | Dutta Majumdar J;Galun R;Mordike B L et al.[J].Materials Science and Engineering,2003,A361:119. |
[10] | Hoche H.;Scheerer H.;Probst D.;Broszeit E.;Berger C. .Plasma anodisation as an environmental harmless method for the corrosion protection of magnesium alloys[J].Surface & Coatings Technology,2003(0):1002-1007. |
[11] | Lee MH.;Bae IY.;Kim KJ.;Moon KM.;Oki I. .Formation mechanism of new corrosion resistance magnesium thin films by PVD method[J].Surface & Coatings Technology,2003(0):670-674. |
[12] | 潘俊德;徐重;唐宾 et al.[P].CN 1390975A,2003. |
[13] | ASTMD 3359-1978.ASTMD 3359-1978.Evaluating Standard for Adhesion Strength of Coatings[S].,1978. |
[14] | 刘正;张奎;曾小勤.镁基轻合金理论和应用[M].北京:机械工业出版社,2002 |
[15] | 唐伟忠.薄膜材料生产的原理、技术及应用[M].北京:冶金工业出版社,1998 |
[16] | 王福贞;闻立时.表面沉积技术[M].北京:机械工业出版社,1989 |
[17] | Georg Reiners;Michael Griepentrog .[J].Surface and Coatings Technology,1995,76-77:809. |
[18] | 谢致薇 .[J].金属热处理,1998,23(09):3. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%