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本文利用液相前驱体法制备二硼化锆(ZrB2)陶瓷纤维前驱体溶液.分别用转矩流变仪及自制干法纺丝设备研究固含量对流变性能及可纺性的影响,结果表明:前驱体溶液保持聚合物溶液的性质;随着固含量的提升,前驱体纺丝液的粘性区逐渐变窄,但总的来说较宽,适宜纺丝.另外,固含量在27.4%~31.3%之间的前驱体溶液可以纺丝,含30.8%固含量的溶液在纺丝压力0.6MPa,纺丝温度50℃,卷绕速度3m/min条件下,可以制得连续纤维.

参考文献

[1] Monteverde F.;Guicciardi S.;Bellosi A. .Advances in microstructure and mechanical properties of zirconium diboride based ceramics[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2003(1/2):310-319.
[2] William G. Fahrenholtz;Gregory E. Hilmas;Inna G. Talmy;James A. Zaykoski .Refractory Diborides of Zirconium and Hafnium[J].Journal of the American Ceramic Society,2007(5):1347-1364.
[3] Ruixing Li;Yun Zhang;Haijie Lou .Synthesis of ZrB2 nanoparticles by sol-gel method[J].Journal of Sol-Gel Science and Technology,2011(2):580-585.
[4] Jia She;Yongzhong Zhan;Mingjun Pang .In situ synthesized (ZrB_2 + ZrC) hybrid short fibers reinforced Zr matrix composites for nuclear applications[J].International Journal of Refractory Metals & Hard Materials,2011(3):401-404.
[5] Z.Y.Sun;K.Q.Han;X.F.Wang;Y.Q.Peng,M.H.Yu.Preparation of zirconium boride(ZrB2) ceramic nanofibers by electrospinning[A].,2011:264-266.
[6] Laura Silvestroni;Diletta Sciti .Oxidation of ZrB_2 Ceramics Containing SiC as Particles, Whiskers, or Short Fibers[J].Journal of the American Ceramic Society,2011(9):2796-2799.
[7] Li-Juan YANG,Shi-Zhen ZHU,Qiang XU,Zhen-Yu YAN,Ling LIU.Synthesis of ultrafine ZrB2 powders by sol-gel process[J].中国高等学校学术文摘·材料科学,2010(03):285-290.
[8] R.X.Li;Y.Zhang;H.J.Lou;J.P.Li,Z.H.Feng.Synthesis of ZrB2 nanoparticles by sol-gel method[J].J Sol-Gel Sci Technol
[9] Yongjie Yan;Zhengren Huang;Shaoming Dong .New Route to Synthesize Ultra-Fine Zirconium Diboride Powders Using Inorganic-Organic Hybrid Precursors[J].Journal of the American Ceramic Society,2006(11):3585-3588.
[10] Ilican S;Caglar Y;Caglar M .Preparation and characterization of ZnO thin films deposited by sol-gel spin coating method[J].Journal of optoelectronics and advanced materials,2008(10):2578-2583.
[11] P.P.Xu;X.F.Wang;S.D.Fu;J.F.Xu.Preparation of zirconia-yttrium fibres from steady precursor by sol-gel technique[J].Adv Mater Res,2012(535-537):2087-2091.
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