采用二甘醇为鳌合剂和反应液制备钛的醇酸盐前驱体球,然后180℃水热处理得到高度晶化的复合分级结构的TiO2球。用X射线衍射仪（XRD）、场发射扫描电子显微镜（FESEM）、傅里叶转换红外光谱仪（FT-IR）以及同步热分析仪（TGA-DSC）对样品进行表征,并探讨了TiO2复合分级球的形成机理。
The diethylene glycol（DEG） was used as chelating agent as well as reaction medium to synthesize the titanium diglycolate precursor spheres.And the highly crystallized hierarchically-structured TiO2 spheres were obtained by hydrothermal treatment of the precursors at 180℃.X-ray diffraction（XRD）,field emission scanning electron microscopy（FESEM）,Fourier transform infrared spectroscopy（FT-IR） and thermogravimetry-differential scanning calorimetry（TGA-DSC） were used to characterize the precursor and TiO2 spheres.The formation mechanism of the hierarchically-structured TiO2 spheres was also investigated.
参考文献
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