采用单辊快淬法制备Fe80Zr5Nb4B11合金,并在不同温度下对其进行退火,研究热处理对该合金的结构和磁性能的影响.利用X射线衍射(XRD)和透射电镜(TEM)表征合金的结构,利用振动样品磁强计(VSM)测量合金的磁性能.结果表明:随着退火温度的增加,α-Fe晶体相从非晶基体中析出;晶粒尺寸逐渐增大;Fe81Zr5Nb4B10合金的比饱和磁化强度(Ms)在300℃下降,之后保持持续上升的趋势;而矫顽力(Hc)的变化相对复杂,呈现先上升→下降→上升的趋势,这些特征与其微观结构密切相关.
参考文献
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