采用脉冲激光沉积法在LaAlO3（LAO）衬底上生长了YBa2Cu3O7/La0.7Ca0.3MnO3（YBCO/LC-MO）和La0.7Ca0.3MnO3/YBa2Cu3O7（LCMO/YBCO）两种外延薄膜,利用高分辨电子显微镜研究了其微观结构。在YBCO/LCMO/LAO薄膜中,LCMO以层-岛模式生长,并形成层状取向畴结构。YBCO层均由c轴取向晶粒组成,其中含有c/3平移畴界、额外CuO层及Y2O3第二相等缺陷结构。在LCMO/YBCO/LAO薄膜中,LAO衬底上初始生长的YBCO为c轴取向,至一定厚度（几个纳米）转为c与a轴混合生长。LCMO层在YBCO上外延生长并具有[100]m与[011]m混合取向畴结构。在LCMO/YBCO界面未观察到失配位错,因此二者界面属应变型界面。
Epitaxial YBa2 Cu3O/La0.7 Ca0.3 MnO3 （YBCO/LCMO） and La0.7 Ca0.3 MnO3/YBa2 Cu3 07 （ LCMO/YB-CO） bi-layers were fabricated on LaA103 （LAO） substrate by pulsed laser deposition, and their microstructures were investigated by using high resolution electron microscopy. In YBCO/LCMO/LAO bi-layer, LCMO layer growed on LAO substrate with a layer-island mode, and developed a layered oriented domain structure. YBCO layers consisted of c-axis oriented domain. Some defects such as c/3 translational boundary, extra CuO layer and Y203 second phase were observed in YBCO film. In LCMO/YBCO/LAO hi-layer, the initial YBCO layer on LAO showed c-axis orientation, and switched to a mixed domain structure containing both c-axis and a-axis when the film thickness reached several nanometers. LCMO layer, which comprises a mixed domain of [100]m and [011]m orientation, epitaxially growed on YBCO film. No misfit dislocation was observed between LCMO and YBCO interface, which was characterized by a strain interface.
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