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以钨酸钠和硝酸钙为原料,加以表面活性剂聚乙二醇200,配制出钨酸钙混浊液,将得到的沉淀物在100 ℃烘干后,制备出钨酸钙纳米晶.对样品进行了XRD分析、红外光谱分析及TEM观察.结果表明,制备的钨酸钙样品结晶良好,纳米晶颗粒间分散性良好,无团聚;在钨酸钙纳米晶的形成过程中,聚乙二醇200对钨酸钙纳米晶颗粒间的分散起着决定性作用;在265 nm波长光的激发下,钨酸钙的光致发光谱中显示一宽化的蓝色发光带.

参考文献

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