{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用HF-CVD法,在氩.氧等离子气氛中,将WCl6进行氧化反应,经骤冷制各出纳米级的WOx微晶.把WCl6进料温度为350℃时所得微晶用TEM、XRD、XPS进行了测试.结果表明:微晶呈近球形,粒径范围为15~65 nm,统计平均粒径为39.0 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IonPac NG1保护柱和NS1分离柱,在流速为1.00 mL/min、淋洗液为1.00 mmol/L九氟戊酸(作为离子对试剂)-7%(体积分数,下同)乙腈时等度洗脱分离,能够快速稳定出峰,且被测物与其他干扰离子充分分离.矮壮素和缩节胺的检出限分别为0.154 6和0.171 4 mg/L,在1~100 mg/L范围内具有良好的线性关系和重现性.对实际样品进行测定,矮壮素和缩节胺的回收率范围分别为96.06%~104.6%和98.53%~103.7%,相对标准偏差小于3%.该方法分析结果令人满意,可以满足矮壮素和缩节胺常规的定性、定量分析需求.","authors":[{"authorName":"周旭","id":"1d066adb-95bd-46b9-846b-07fb7efba044","originalAuthorName":"周旭"},{"authorName":"许锦钢","id":"60cd2373-d517-4198-8971-bb992a49c917","originalAuthorName":"许锦钢"},{"authorName":"陈智栋","id":"c59eb08f-4cc2-4ec8-9bdf-3aeb902fbe27","originalAuthorName":"陈智栋"},{"authorName":"朱岩","id":"0b00333a-988a-492c-ae45-13f9c48dae21","originalAuthorName":"朱岩"}],"doi":"10.3724/SP.J.1123.2011.00244","fpage":"244","id":"4de7604c-a5fd-40fe-aaec-ee6a44b6c21e","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 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m水平突水及治水过程,在查清该矿区水文地质条件及矿井突水要因的基础上,为综合防治竖井掘进期间通过特殊地质构造段突水,提出相应的主井掘进帷幕注浆防治水技术及措施,并在掘进工程中收到了良好的应用效果,对类似特殊条件下的矿山井巷掘进工程具有借鉴意义.","authors":[{"authorName":"董华兴","id":"c08faef8-222f-4269-ab57-068e213c04a0","originalAuthorName":"董华兴"},{"authorName":"郑翠敏","id":"71818941-893c-450e-8900-6d9f7dc6d4f4","originalAuthorName":"郑翠敏"},{"authorName":"董凤霞","id":"ce559c6e-5477-4acc-96d6-55cc93294757","originalAuthorName":"董凤霞"},{"authorName":"韩建国","id":"d72c3f8a-9086-4000-8209-5e6a1f371d1d","originalAuthorName":"韩建国"}],"doi":"10.11792/hj20130209","fpage":"35","id":"50da3555-9182-4c83-b8b8-7c218b723d08","issue":"2","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"c8ee1711-e9ee-4c00-a471-1354d308bfe1","keyword":"大水矿山","originalKeyword":"大水矿山"},{"id":"5da58d6c-dff5-4998-b645-b63ba8ec37c0","keyword":"主井掘进","originalKeyword":"主井掘进"},{"id":"a29b56b2-06f6-49a2-9412-0a6cbd37c8f5","keyword":"特殊地质构造","originalKeyword":"特殊地质构造"},{"id":"49c4c65b-3993-4060-b81d-5caf117fa377","keyword":"突水","originalKeyword":"突水"},{"id":"5f22c680-f6b2-4312-8b46-fe823c71eddb","keyword":"防治","originalKeyword":"防治"}],"language":"zh","publisherId":"huangj201302009","title":"南李庄矿主井施工突水防治技术","volume":"34","year":"2013"},{"abstractinfo":"","authors":[],"doi":"","fpage":"72","id":"6dc2f984-a0d4-41a2-94ff-c3ee488d47dd","issue":"4","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"3063b884-88c7-442a-ab4f-f1931c33ef5b","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"tlgy200904020","title":"壮根扎江南","volume":"39","year":"2009"},{"abstractinfo":"文中用数值模拟的方法分析了矿房倾角对蚕庄金矿倾斜试验采场稳定性的影响,找到了最佳的矿房倾角,得出了有价值的结论.","authors":[{"authorName":"安然","id":"eb59fc27-4023-4c9d-801c-ffbec5a44bbb","originalAuthorName":"安然"},{"authorName":"王保学","id":"f2767b10-4cd8-4b56-aaa9-aabd894534f5","originalAuthorName":"王保学"},{"authorName":"扬同","id":"b76378c0-3100-4303-bdbb-8b597dbc2d0d","originalAuthorName":"扬同"}],"doi":"10.3969/j.issn.1001-1277.2001.02.005","fpage":"16","id":"c4133e77-684a-4213-b763-399af8c1e760","issue":"2","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"dd846364-ba70-45c6-8b88-b010dc9d8cac","keyword":"倾斜矿房","originalKeyword":"倾斜矿房"},{"id":"f5f14367-2d0d-4054-9648-25eaa5f498e2","keyword":"数值模拟","originalKeyword":"数值模拟"},{"id":"e5b0c150-f742-485b-8af3-7d5c7007868f","keyword":"稳定性分析","originalKeyword":"稳定性分析"}],"language":"zh","publisherId":"huangj200102005","title":"蚕庄金矿倾斜矿房倾角对其稳定性的影响","volume":"22","year":"2001"},{"abstractinfo":"用反相高效液相色谱法(HPLC)和紫外分光光度法 (UV)测定了β-环糊精(β-CD)与维生素D2(VD2)包合物中VD2的质量分数,两种方法测得的结果十分吻合.研究了HPLC测定的精密度和回收率,其相对标准偏差分别为0.63%和1.54%,表明该法准确可靠.含有β-CD-VD2包合物的\"龙牡壮骨冲剂\"经KOH、维生素C和乙醇-水(体积比为1∶2 )于70 ℃下皂化处理,再由HPLC检测用乙醚萃取的VD2产物,得到准确的结果.","authors":[{"authorName":"张俐娜","id":"57627f4b-9b2c-4fdd-be2c-76bc8252dd7b","originalAuthorName":"张俐娜"},{"authorName":"黄进","id":"8091dc78-e25f-4c72-8aec-902d44cd5857","originalAuthorName":"黄进"},{"authorName":"杨光","id":"7d674cdf-c279-45c5-baea-b7d9bb7b1561","originalAuthorName":"杨光"},{"authorName":"张平义","id":"f8aa7f2b-4e4a-4747-9af6-cf7cc3bcad86","originalAuthorName":"张平义"},{"authorName":"彭湘红","id":"23f64e8b-6eeb-40bb-8eca-bd92f0e7b5e7","originalAuthorName":"彭湘红"},{"authorName":"王业文","id":"32588724-9ed1-4107-844d-ea6b0123a77a","originalAuthorName":"王业文"}],"doi":"10.3321/j.issn:1000-8713.2000.01.015","fpage":"52","id":"e8a828ae-0f03-479f-8d48-5c14040c6b79","issue":"1","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"0ffe98dd-47ff-420f-828d-ad04d1705a15","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"5f24d6fd-7ba2-40f7-a031-9bd5be7fcae6","keyword":"维生素D2","originalKeyword":"维生素D2"},{"id":"ec001ee3-30a3-4e86-b9a2-cab22305e1c5","keyword":"β-环糊精","originalKeyword":"β-环糊精"},{"id":"1da2ef3e-02c2-4d41-895c-23b207518cc8","keyword":"包合物","originalKeyword":"包合物"},{"id":"ef04812d-fd22-481e-9554-98a14d0ca347","keyword":"紫外光谱","originalKeyword":"紫外光谱"}],"language":"zh","publisherId":"sp200001015","title":"高效液相色谱法测定\"龙牡壮骨冲剂\"中β-环糊精包合的维生素D2","volume":"18","year":"2000"},{"abstractinfo":"针对蚕庄金矿上庄矿区深部缓倾斜中厚Ⅱ号矿体的赋存及开采技术条件,详细介绍了竖分条采矿法矿块布置及参数、回采及充填工艺,试验应用取得了较上向水平分层尾砂充填采矿法更好的回采效果.值得类似条件矿山借鉴.","authors":[{"authorName":"王兴涛","id":"036e21c0-259e-4e45-a3eb-686158c77e1f","originalAuthorName":"王兴涛"},{"authorName":"郭建军","id":"b1454f12-6dfb-4c1a-9e74-e1fb9a552a9e","originalAuthorName":"郭建军"},{"authorName":"杨玉泉","id":"22b5dc93-d30f-4f1c-b769-f5ecd4e8eae9","originalAuthorName":"杨玉泉"},{"authorName":"浦玉传","id":"7ebbbf24-5cf6-43b1-99a3-9707447e843a","originalAuthorName":"浦玉传"},{"authorName":"李昊","id":"3dd8e1ba-94be-4a20-a3a0-a56418fde666","originalAuthorName":"李昊"}],"doi":"10.3969/j.issn.1001-1277.2008.09.008","fpage":"26","id":"dac718fe-d78e-4a3e-a88b-dafc1be118bd","issue":"9","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"2302b4cd-1c80-4c36-ab83-44cff96a290c","keyword":"竖分条","originalKeyword":"竖分条"},{"id":"f84ac425-f394-4f5a-9edb-7ef107e9b5c2","keyword":"缓倾斜","originalKeyword":"缓倾斜"},{"id":"816f1eb8-8a40-4a67-8e36-fbb9e22f657c","keyword":"中厚矿体","originalKeyword":"中厚矿体"},{"id":"c0f837cb-9812-4a37-ad9b-4d53670fa614","keyword":"蚕庄金矿","originalKeyword":"蚕庄金矿"}],"language":"zh","publisherId":"huangj200809008","title":"竖分条回采工艺在蚕庄金矿缓倾斜中厚矿体的应用实践","volume":"29","year":"2008"}],"totalpage":7,"totalrecord":62}