{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用氧化还原-盐酸常压搅拌浸出法对钛铁矿进行选择性浸出,研究了氧化还原预处理对钛铁矿粒度、结构、表面形貌的影响,并考察了不同浸出条件对钛铁矿中Fe、Ti浸出率及浸出渣中TiO2品位的影响.结果表明,钛铁矿经过氧化还原后颗粒表面粗糙程度增加,粒径有所增大.采用1000℃氧化1h,800℃H2还原1h的改性矿浸出,优化浸出条件为:液固比5∶1,盐酸浓度4 mol/L,反应温度90℃,浸出时间5h.优化条件下Fe和Ti的浸出率分别为93.89%和3.28%,最终获得TiO2品位87.51%的富钛料,同时很好地保持了原矿的粒度.","authors":[{"authorName":"吕斌","id":"69660388-10d5-42d0-87f0-387d21c1e659","originalAuthorName":"吕斌"},{"authorName":"丁伟中","id":"7073c77c-024d-484d-9f0d-9587e78992f5","originalAuthorName":"丁伟中"},{"authorName":"尚兴付","id":"484a9b96-7530-4080-a689-8ae704672576","originalAuthorName":"尚兴付"},{"authorName":"谈定生","id":"35b024d2-be24-4650-9ebe-7e64894858ff","originalAuthorName":"谈定生"},{"authorName":"郭曙强","id":"60c142fd-510a-4f11-a870-c4903211ab96","originalAuthorName":"郭曙强"}],"doi":"10.7513/j.issn.1004-7638.2016.03.001","fpage":"1","id":"ae33c35f-9390-4b31-ae6a-771370a68765","issue":"3","journal":{"abbrevTitle":"GTFT","coverImgSrc":"journal/img/cover/gtft1.jpg","id":"28","issnPpub":"1004-7638","publisherId":"GTFT","title":"钢铁钒钛"},"keywords":[{"id":"bc3bf88a-d5fa-4bd9-898a-8c671c32f803","keyword":"钛铁矿","originalKeyword":"钛铁矿"},{"id":"01f15ee2-2cff-4cb3-904a-4c98e1a137bd","keyword":"氧化还原","originalKeyword":"氧化还原"},{"id":"262e8cd8-53b0-485a-b421-b215dcbc3d27","keyword":"盐酸浸出","originalKeyword":"盐酸浸出"},{"id":"5bdc4754-e523-4eb5-8b27-8a3d8db86f39","keyword":"浸出率","originalKeyword":"浸出率"},{"id":"31b14bc4-e195-4cbf-937b-e997d1b803ac","keyword":"富钛料品位","originalKeyword":"富钛料品位"}],"language":"zh","publisherId":"gtft201603001","title":"氧化还原-盐酸浸出钛铁矿制备富钛料工艺研究","volume":"37","year":"2016"},{"abstractinfo":"由NiCl2、NaBH4等组成的微乳液体系发生氧化还原反应制备NiO纳米棒前驱物,在熔融盐环境中860℃焙烧2.5h前驱体发生氧化反应,成功地制备了NiO纳米棒,用透射电子显微镜、X射线衍射对NiO纳米棒进行了表征.","authors":[{"authorName":"赵鹤云","id":"0f3f26be-7604-49b9-bb06-e606d6de7c97","originalAuthorName":"赵鹤云"},{"authorName":"杨留方","id":"54f02a65-157c-48b0-a546-85259a6f26c9","originalAuthorName":"杨留方"},{"authorName":"朱文杰","id":"935bf3aa-36fc-4cbd-b237-1d1c98c6e894","originalAuthorName":"朱文杰"},{"authorName":"柳清菊","id":"8b7d48ca-01c0-4bd0-9fad-fa08535559ae","originalAuthorName":"柳清菊"},{"authorName":"吴兴惠","id":"9433802a-6aad-453e-8dc7-d1a42207890b","originalAuthorName":"吴兴惠"}],"doi":"","fpage":"2694","id":"2095b8d3-e4f1-4aae-b631-1b1d8cf50cc3","issue":"z1","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"97d806ed-d412-441b-82ff-2519a32d6ff8","keyword":"微乳液","originalKeyword":"微乳液"},{"id":"d58f1a01-4b8b-4bf4-9d7d-3b980dc66059","keyword":"NiO纳米棒","originalKeyword":"NiO纳米棒"},{"id":"889f76b3-1961-4325-ae1a-670a81aabe55","keyword":"熔盐","originalKeyword":"熔盐"},{"id":"5e38c8af-5429-4c50-b8d9-5d0173b682b7","keyword":"氧化还原","originalKeyword":"氧化还原"}],"language":"zh","publisherId":"gncl2004z1753","title":"氧化还原法制备NiO纳米棒一维材料的研究","volume":"35","year":"2004"},{"abstractinfo":"在聚氧乙烯五醚(NP5)、聚氧乙烯九醚(NP9)和环己烷组成的微乳体系中用氧化还原法制备SnO2前驱物,然后在熔盐中再经800℃、860℃焙烧2.5h,成功地制备了金红石结构的SnO2纳米棒,并用透射电子显微镜,X射线衍射对SnO2纳米棒的结构进行了表征.","authors":[{"authorName":"赵鹤云","id":"35c7ab71-cd77-4b40-85bb-c87602a82d11","originalAuthorName":"赵鹤云"},{"authorName":"杨留方","id":"b33eceeb-52e9-447a-b3c5-65540c2f3818","originalAuthorName":"杨留方"},{"authorName":"朱文杰","id":"3815c689-1f97-4ca4-9747-229cae98fae9","originalAuthorName":"朱文杰"},{"authorName":"柳清菊","id":"d1f94e39-7db8-4d5a-84b7-65e016494085","originalAuthorName":"柳清菊"},{"authorName":"吴兴惠","id":"cfc9709c-2dbe-46e7-90f2-e9c02d17a1b8","originalAuthorName":"吴兴惠"}],"doi":"","fpage":"96","id":"e8487b64-5f1e-4f13-8384-7339f4bbbd73","issue":"4","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"c2c6160d-cc83-4f5a-996b-ced4e36fdacd","keyword":"氧化还原","originalKeyword":"氧化还原"},{"id":"4c4a662c-fbcf-4977-87d4-ba1fdf610133","keyword":"纳米棒","originalKeyword":"纳米棒"},{"id":"c6dd3ea3-8cca-4fe1-bba0-66e88832e8ff","keyword":"微乳液","originalKeyword":"微乳液"},{"id":"676b0617-22d4-4e79-a488-e8bada538cb2","keyword":"熔盐","originalKeyword":"熔盐"}],"language":"zh","publisherId":"cldb200404028","title":"氧化还原法制备SnO2纳米棒的研究","volume":"18","year":"2004"},{"abstractinfo":"研究了钨晶须的制备工艺,并分析了其生长机理.采用X射线衍射、扫描电镜、能谱分析、透射电镜对制备的钨晶须进行物相、形貌、成分、微观结构的分析和表征.研究表明:钨晶须长度大致在1~10μm,直径在1μm以下,部分达到纳米级;晶须为单晶bcc结构,生长方向为〈110〉;钨晶须形成过程为钨粉及其氧化产物与水汽反应生成气相水合物WO2(OH)2,遇氢气还原后形核并沉积,进而定向生长为晶须结构,钨晶须的生成遵循VS机理.","authors":[{"authorName":"马运柱","id":"e8a24ed1-db7a-412b-8809-fc1d7d09735e","originalAuthorName":"马运柱"},{"authorName":"石玉斌","id":"0513ef2c-2e44-41be-a16c-c078cda45854","originalAuthorName":"石玉斌"},{"authorName":"刘文胜","id":"0ee96ada-8ad4-4176-8c47-7e6d7ebb93b8","originalAuthorName":"刘文胜"},{"authorName":"李静","id":"3f15f2df-c281-4656-9107-74a74aaad379","originalAuthorName":"李静"}],"doi":"","fpage":"117","id":"6d6970d3-6e89-4095-92a3-0ab14a180b81","issue":"3","journal":{"abbrevTitle":"CLKXYGY","coverImgSrc":"journal/img/cover/CLKXYGY.jpg","id":"14","issnPpub":"1005-0299","publisherId":"CLKXYGY","title":"材料科学与工艺"},"keywords":[{"id":"aeaf9f10-75b0-461d-acd9-98e4adb6998a","keyword":"钨晶须","originalKeyword":"钨晶须"},{"id":"168f058d-f230-4aa7-bf49-97bbfed3e690","keyword":"氧化还原","originalKeyword":"氧化还原"},{"id":"daf71272-7982-4846-bf48-4c5485f22de3","keyword":"化学气相迁移","originalKeyword":"化学气相迁移"},{"id":"96024fcc-cbd5-42a3-82bc-1de50fa40ece","keyword":"VS机理","originalKeyword":"VS机理"}],"language":"zh","publisherId":"clkxygy201203023","title":"氧化还原法制备钨晶须及其生长机理研究","volume":"20","year":"2012"},{"abstractinfo":"应用热重和高温X射线衍射技术,研究了Pd/PdO的高温循环氧化还原过程,并考察了添加少量Mn对其高温热稳定性的影响.结果表明:PdO在一个确定的温度将会急剧分解为金属Pd,其分解温度与粉体粒度无关.Pd/PdO是否出现循环氧化特征将取决于Pd粉的分散状态,加入适量的Mn将会改变Pd/PdO的高温热稳定性和循环氧化特征.","authors":[{"authorName":"蒲健","id":"181fde33-fdaf-4cce-a4af-d4c528d471e7","originalAuthorName":"蒲健"},{"authorName":"梁凤丽","id":"4b551fde-62e9-40f6-9e77-5a486065374e","originalAuthorName":"梁凤丽"},{"authorName":"华斌","id":"5dcf0bb3-5cf6-4b18-96bb-97c76006318b","originalAuthorName":"华斌"},{"authorName":"颜冬","id":"be9c3c44-8914-482f-8df2-d24317324999","originalAuthorName":"颜冬"},{"authorName":"池波","id":"e54c8890-2535-49b7-9979-0452652007aa","originalAuthorName":"池波"},{"authorName":"李箭","id":"eaabd01c-4499-4ecd-9a6c-151c7af0301d","originalAuthorName":"李箭"}],"doi":"","fpage":"1395","id":"d3985290-3a02-4454-91c5-af7001ba8510","issue":"8","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"baaeccb0-6008-4819-97d8-e0e4b55101a8","keyword":"Pd","originalKeyword":"Pd"},{"id":"2097235f-ef1d-4012-9b4b-2dae3fa98391","keyword":"热稳定性","originalKeyword":"热稳定性"},{"id":"230a6dad-59fc-4991-b678-fc371f52e8a2","keyword":"氧化还原","originalKeyword":"氧化还原"}],"language":"zh","publisherId":"xyjsclygc201008016","title":"Pd/PdO循环氧化还原过程特性研究","volume":"39","year":"2010"},{"abstractinfo":"用电导率电池测量了钠铁磷熔体的电阻率,并分析了相应玻璃的穆斯堡尔谱,计算了铁离子的价态和氧化还原比,分析了温度、时间和氧化钠含量对熔体电阻率和玻璃氧化还原比的影响.发现在Na2O含量低的熔体中,升温和降温过程的电阻率的变化是不可逆的,随着Na2O含量增加,不可逆性消失,熔体的电阻率随时间轻微下降.同时发现Na2O含量低的铁磷熔体的导电机理是电子性的,并用氧化还原比解释了其电阻率-温度曲线的不可逆性.","authors":[{"authorName":"刘艺","id":"62d8ff35-e646-4a48-b748-ed19d8b5376b","originalAuthorName":"刘艺"},{"authorName":"陈福义","id":"2ffe50a4-94b6-4f7d-9384-5c761d0dcb82","originalAuthorName":"陈福义"}],"doi":"10.3969/j.issn.1673-2812.2001.04.009","fpage":"37","id":"eb176505-834e-4534-9323-402b6d2c5887","issue":"4","journal":{"abbrevTitle":"CLKXYGCXB","coverImgSrc":"journal/img/cover/CLKXYGCXB.jpg","id":"13","issnPpub":"1673-2812","publisherId":"CLKXYGCXB","title":"材料科学与工程学报"},"keywords":[{"id":"afa86b13-afe6-4d79-b6c3-b5fb1da92e16","keyword":"铁磷熔体","originalKeyword":"铁磷熔体"},{"id":"c10957ff-4fdb-4a36-8242-940752cd4a6c","keyword":"电阻率","originalKeyword":"电阻率"},{"id":"b1579212-1f4d-40f8-80eb-bad80bcba4aa","keyword":"氧化还原","originalKeyword":"氧化还原"}],"language":"zh","publisherId":"clkxygc200104009","title":"氧化还原比对钠铁磷熔体电阻率的影响","volume":"19","year":"2001"},{"abstractinfo":"首次在微波场作用下,采用直接法和间接法快速合成了氟化铈(Ⅲ),通过XRD、TG-DTG及场发射扫描电镜(FE-SEM)等方法对样品的组成、结构进行了分析表征,并讨论了两种合成方法以及微波合成条件对产物的影响.研究表明:采用本方法合成的CeF3,晶型为类球形,平均粒径约为100nm.","authors":[{"authorName":"张秀凤","id":"fc95c1b8-25ef-4abc-bb37-f21103bce835","originalAuthorName":"张秀凤"},{"authorName":"涂华民","id":"97d1e376-c757-4258-b5c0-e59f49fc1cec","originalAuthorName":"涂华民"},{"authorName":"张迈生","id":"b8bc6001-df65-4fe7-b21e-a38bd187fe7c","originalAuthorName":"张迈生"},{"authorName":"林木良","id":"f2160c53-58e0-40c9-aea9-4d5bd729c1dc","originalAuthorName":"林木良"}],"doi":"","fpage":"78","id":"67a657c9-e500-4747-a604-781111e8c767","issue":"1","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"cbb5896a-1e9f-4ce2-944a-95836d4dd690","keyword":"氟化铈(Ⅲ)","originalKeyword":"氟化铈(Ⅲ)"},{"id":"5298fcaf-554c-4e1f-8345-dfab2696f09e","keyword":"微波合成","originalKeyword":"微波合成"},{"id":"bf25b385-0bd3-46c9-ae1d-0a0261ef68d3","keyword":"氧化还原","originalKeyword":"氧化还原"},{"id":"fd335d74-303d-4fc7-92c6-ceb1f103aabe","keyword":"纳米级","originalKeyword":"纳米级"}],"language":"zh","publisherId":"cldb200301025","title":"纳米氟化铈(Ⅲ)的微波固相氧化还原合成法","volume":"17","year":"2003"},{"abstractinfo":"铋的蒸气压小,熔点低,用直接蒸发冷凝的方法制备铋粉体较困难.采用先将铋蒸发氧化制备氧化铋纳米粉体,然后在低于铋的熔点下,用氢气还原的方法制备了超细铋粉体.XRD与SEM分析结果表明:氧化铋为β-Bi2O3,平均粒径为37nm;用氢气还原所得粉体为纯铋,平均粒径为222.1 nm.","authors":[{"authorName":"胡汉祥","id":"f64723b0-ff62-48c9-ac8e-e718dee29b6d","originalAuthorName":"胡汉祥"},{"authorName":"谢华林","id":"a0de5371-6f25-433f-8e8a-900e73d9dcf0","originalAuthorName":"谢华林"},{"authorName":"何晓梅","id":"bb2270df-0165-4385-badb-311c1c6b6281","originalAuthorName":"何晓梅"}],"doi":"","fpage":"164","id":"7a45b935-62a7-45f5-a34c-6edd3c2a9bc6","issue":"z1","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"b2b0b746-b68d-40c2-ac94-0204efe49a88","keyword":"氧化铋","originalKeyword":"氧化铋"},{"id":"c5620b0b-0216-42fb-838f-4a32a67d1fcc","keyword":"铋","originalKeyword":"铋"},{"id":"53fec21f-5b83-4d77-aebd-f0558acc7134","keyword":"氧化还原","originalKeyword":"氧化还原"},{"id":"36cbf1fd-c88b-41b0-977c-68b108115ffe","keyword":"纳米粉体","originalKeyword":"纳米粉体"}],"language":"zh","publisherId":"cldb2006z1053","title":"超细铋金属粉体的制备","volume":"20","year":"2006"},{"abstractinfo":"CeO2的催化性能不仅与粒子大小有关,而且与其形貌密切相关. 本文分析了CeO2的纳米结构和氧化还原特性,综述了CeO2在催化反应中的形貌效应,着重介绍了CeO2的结构和形貌对CO氧化、水气变换和乙醇水蒸气重整制氢以及二元醇脱水反应活性的影响.","authors":[{"authorName":"李娟","id":"d7355d45-8009-42b3-ae32-659ff62a7b96","originalAuthorName":"李娟"},{"authorName":"塔娜","id":"7a5707b4-5888-4e67-91dd-07369da015cd","originalAuthorName":"塔娜"},{"authorName":"李勇","id":"70344787-d464-4ce4-bafa-ac847aa8fd5d","originalAuthorName":"李勇"},{"authorName":"申文杰","id":"782cf2a2-4f67-49e2-9d01-1edcfce3dc99","originalAuthorName":"申文杰"}],"doi":"","fpage":"823","id":"f3def4a0-56ea-4d61-85aa-3c7c138eec5f","issue":"9","journal":{"abbrevTitle":"CHXB","coverImgSrc":"journal/img/cover/CHXB.jpg","id":"18","issnPpub":"0253-9837","publisherId":"CHXB","title":"催化学报 "},"keywords":[{"id":"c2c0c41a-5f10-4418-b70d-1d819ba7edcb","keyword":"氧化铈","originalKeyword":"氧化铈"},{"id":"28528446-6db2-4e59-af3d-e2fb4205ff75","keyword":"纳米结构","originalKeyword":"纳米结构"},{"id":"74e794bd-b252-4b33-8b95-376150b20d71","keyword":"氧化还原","originalKeyword":"氧化还原"},{"id":"8930258d-a91c-4311-b09f-a0b3e01a6c71","keyword":"形貌效应","originalKeyword":"形貌效应"},{"id":"cf2a3c72-8605-467f-b166-49208102616f","keyword":"多相催化反应","originalKeyword":"多相催化反应"}],"language":"zh","publisherId":"cuihuaxb200809003","title":"纳米尺度CeO2在多相催化反应中的形貌效应","volume":"29","year":"2008"},{"abstractinfo":"合成了一种新的四硫富瓦烯衍生物修饰的银溶胶,并通过透射电子显微镜、红外、紫外、拉曼光谱和循环伏安法测试技术对其进行了表征. 透射电子显微镜照片显示,纳米银颗粒为球形,其直径约为70 nm,用四硫富瓦烯衍生物修饰的银纳米粒子有较好的单分散性. 将修饰后的银溶胶固着在Pt片电极上进行了电化学测定. 结果显示,修饰后的纳米银颗粒具有较好的氧化还原活性. 2组氧化-还原峰(E1/2)为0.67和0.86 V,分别对应于TTF/TTF·+和TTF·+/TTF2+ 2个单电子氧化过程.","authors":[{"authorName":"郭文娟","id":"b1deafc8-990e-4c1e-a6ac-42c3ba30c38f","originalAuthorName":"郭文娟"},{"authorName":"郭琳","id":"9832ed87-4330-4277-8657-032484e580c0","originalAuthorName":"郭琳"},{"authorName":"戴洁","id":"ad42ff7b-a6b4-4ce3-a8c8-df616432d810","originalAuthorName":"戴洁"},{"authorName":"卞国庆","id":"ef1c5847-02f5-4d0c-bcb9-0db726654c1d","originalAuthorName":"卞国庆"},{"authorName":"卢雯","id":"98ba95e8-f87d-4fa6-ab16-910bddd1f9c3","originalAuthorName":"卢雯"}],"doi":"10.3969/j.issn.1000-0518.2006.09.003","fpage":"953","id":"606ab472-0ff7-4b20-98fa-bb1cacc4bbd2","issue":"9","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"9febfaba-fa50-41ec-b4cb-9c99307b2926","keyword":"银溶胶","originalKeyword":"银溶胶"},{"id":"a3928493-f4f3-4873-9fd7-b373a832db39","keyword":"纳米粒子","originalKeyword":"纳米粒子"},{"id":"da059f0d-129c-49f1-a35f-132d66254ae8","keyword":"四硫富瓦烯","originalKeyword":"四硫富瓦烯"},{"id":"b378c766-f539-417c-a3fa-b0a662a4e09e","keyword":"氧化还原","originalKeyword":"氧化还原"},{"id":"eec9e9d4-4e48-4c5f-839e-975b3a0cf686","keyword":"表面修饰","originalKeyword":"表面修饰"}],"language":"zh","publisherId":"yyhx200609003","title":"四硫富瓦烯衍生物修饰的银溶胶","volume":"23","year":"2006"}],"totalpage":3367,"totalrecord":33661}