Wen WANG
,
Yu ZHOU
,
Sheng CHEN
,
Feng Y
,
Dechang JIA
材料科学技术（英文）
Strontium bismuth tantalum (SBT) fine power was prepared by Sol-Gel method. Pentaethoxy tantalum, strontium acetate and bismuth subnitrate were used as raw materials, and were dissolved in proper order in ethylene glycol to form transparent sol. The mixed precursor was dried at 80℃ and annealed at 800℃ for 1 h. Crystallized nanometer sized SBT fine powder was obtained and characterized by XRD.
关键词:
Junbao ZHANG
,
Guangwu WEN
,
Tingquan LEI
,
Dechang JIA
,
Jiancun RAO
材料科学技术（英文）
Si-B-O-N powder without B-O bonds synthesized by polymeric precursor were hot-pressed into ceramics at different temperatures. The variations of microstructure and mechanical properties of Si-B-O-N ceramics have been investigated. Crystallization of Si-B-O-N ceramics occurred at about 1400°C. Density, elastic modulus, and flexural strength of the ceramics increased with the increasing sintering temperatures, and reached to their maximum values at 1600°C. By contrast,hardness and fracture toughness of the ceramics monotonically changed with increasing sintering temperatures. Hardness decreased, while the fracture toughness increased. The principal toughening mechanisms including crack deflection, crack bridging and plate grain pulling-out effects are discussed
关键词:
Si-B-O-N ceramics
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null
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null
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null
Dianran YAN
,
Jining HE
,
XiangZhi LI
,
Yangai LIU
,
Yu ZHOU
,
Dechang JIA
材料科学技术（英文）
The corrosion resistance of SiO2/A12O3, TiO2/Al2O3 and (SiO2+TiO2)/Al2O3 ceramic composite coatings on Q235 substrate fabricated by means of plasma spraying was investigated. The results show that A12O3+13 wt pct TiO2 ceramic coating has the highest density, the lowest connected porosity and the best corrosion resistance. The corrosion mechanism of Q235 with ceramic coating has also been studied.
关键词:
金属学报
Volu扣ne 27SeriesB1991AUTHOR INDEX CCAO Guanghan(曹光旱)············……6一B科6CAo weijie(曹卫恋)..················……5一B32oCAO Yilin(曹益林)··················……6一B443CHANG Xin(常听)···············……1一B48CHE Guang邻n(车广灿)·············一6一B科0CHEN Erbao(陈二保)···············……6一B410CHEN Jia....
关键词:
Materials Research Bulletin
Through analysis of the latest experimental results reported in the literature and obtained in our laboratory, we have extended our previous quantum confinement/luminescence center model for the photoluminescence mechanism of porous Si and of nanometer-silicon-particle-embedded Si oxide films (G.G. Qin and Y.Q. Jia, Solid State Commun. 86, 559 (1993)). We consider that there are three main types of competitive photoexcitation/photoemission processes and that the process in which photoexcitation occurs in the nanometer silicon particles (NSPs) while photoemission occurs in the luminescence centers (LCs) in the SiOx layers very close to the NSPs is usually the major one. We discuss under what conditions the other two types of processes will dominate. We believe that the extended quantum confinement/luminescence center model is a physical model that is suitable for the photoluminescence from silicon oxide films embedded with NSPs or nanometer Ge particles (NGPs), as well as from oxidized porous Si. (C) 1999 Elsevier Science Ltd.
关键词:
oxides;luminescence;defects;blue-light emission;visible luminescence;optical-properties;nanocrystals;mechanism;dependence;sio2-films;absorption;spectra;defects
刘守平
,
周上祺
,
王佳眉
,
任勤
腐蚀学报（英文）
用金相显微镜、扫描电镜、X射线衍射仪和X射线能谱仪对天然气井油管悬挂器腐蚀失效进行了检测分析，并对天然气井油管悬挂器用35CrMo钢进行了盐雾试验，结果表明，天然气中的水和CO2是引起腐蚀的主要介质，腐蚀产物主要是FeCO3，高速天然气冲刷和钢中的非金属夹杂加剧了腐蚀的速度.
CORROSION FAILURE ANALYSIS OF AN OIL TUBE USED IN NATURAL GAS WELL
LIU Shou-ping,ZHOU Shang-qi,WANG Jia-mei,REN Qin
Chongqing University
A failed oil tube used in natural gas well was examined by optical microscope,scanning electron microscope ,X-ray diffractometer and X-ray spectrometer.Corrosion behavior of 35CrMo steel samples of the oil tube were investigated by means of salt spray tests in the laboratory.The results show that CO2 and H2O are primary factors in the corrosion of oil tube.The corrosion product is FeCO3,non-metallic inclusions in the steel and erosion of natural gas fluid played an important role in accelerating the corrosion.
oil tube;
natural gas well；
35CrMo steel；
failure analysis；
corrosion
关键词:
悬挂器
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null
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null
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