Jingxiao LIU
,
Fei SHI
,
Dazhi YANG
材料科学技术（英文）
In order to improve the corrosion resistance and biocompatibility of NiTi surgical alloy, TiO2 and TiO2-SiO2 thin films were prepared by sol-gel method. The surface characteristics of the film, which include surface composition, microstructure and surface morphology, were studied by X-ray diffraction (XRD), atomic force microscopy (AFM) and X-ray photoelectron spectra (XPS), respectively. A scratching test was used to assess the interface adhesive strength between the film and substrate. The corrosion resistances of NiTi alloy coated with oxide films were studied by anodic polarization curves measurement in biological solution. Additionally, a preliminary study of the in vitro bioactivity of the films was conducted. The results indicated that TiO2 and TiO2-SiO2 (Ti/Si=4:1) films have higher electrochemical corrosion resistance and can be used as protective layers on NiTi alloy. In addition, TiO2-SiO2 composite films have better bioactivity than TiO2 film.
关键词:
TiO2
,
null
,
null
,
null
,
null
Haihua LIU
金属学报(英文版)
doi:10.1016/S1006-7191(08)60120-9
A novel method was reported to measure the remnant magnetic field in Lorentz mode in a FEI Tecnai F20 transmission electron microscope equipped with a Lorentz lens. The movement of the circle Bloch line of the cross-tie wall in Permalloy is used to measure the remnant magnetic field by tilting the specimen and adjusting the objective lens current. The remnant magnetic field is estimated to be about 17 Oe, in a direction opposite to that of the objective lens magnetic field. The remnant magnetic field can be compensated by adjusting the value of the objective lens current.
关键词:
Lorentz electron microscopy
,
Lorentz lens
,
remnant magnetic field
,
Permalloy
,
cross-tie walls
Journal of Materials Research
Based on the best bulk metallic glass (BMG) forming alloy in the Mg-Cu-Y ternary system, we introduced Ag (or Ni) to partially substitute for Cu to improve the glass-forming ability (GFA). The objective of this paper is twofold. First, we illustrate in detail a recently developed search strategy, which was proposed but only briefly outlined in our previous publication [H. Ma, L.L. Shi, J. Xu, Y. Li, and E. Ma: Discovering inch-diameter metallic glasses in three-dimensional composition space. Appl. Phys. Lett. 87, 181915 (2005)]. The protocol to navigate in three-dimensional composition space to land large BMGs is spelled out step-by-step using the pseudo-ternary Mg-(Cu,Ag)-Y as the model system. Second, our ability to locate the best BMG former in the composition tetrahedron allows us to systematically examine, and conclude on, the effects of a given alloying element. The large improvement in glass-forming ability in the Mg-(Cu,Ag)-Y system relative to the based ternary will be contrasted with the reduced glass-forming ability in the Mg-(Cu,Ni)-Y pseudo ternary system. It is demonstrated that the improvement of glass-forming ability requires judicious choice of substitutional alloying elements and concentrations, rather than simple additions of multiple elements assuming the "confusion principle."
关键词:
bulk metallic-glass;shaped copper mold;amorphous-alloys;thermal-stability;ternary-system;casting method;p system;diameter;zr;mm
刘天成
,
卢志超
,
李德仁
,
孙克
,
周少雄
,
卢燕平
功能材料
采用电沉积方法从硫酸盐体系镀液中沉积得到Fe18Ni82合金薄膜.运用扫描电子显微镜(SEM),原子力显微镜(AFM),透射电子显微镜(TEM)和X射线衍射分析(XRD)以及磁测量设备分别对薄膜的表面形貌、显微结构和磁性能进行表征和测量.同时利用万能材料试验机和显微硬度计测量了薄膜的力学性能.结果表明:电沉积制备的Fe18Ni82合金薄膜成分均匀,表面平整、光亮、致密,晶粒大小为40～50 nm.薄膜是以Ni为溶剂原子,Fe为溶质原子的置换型固溶体,只存在单一的fcc相,Fei8Ni82合金薄膜沿(111)面有较强的择优取向.镀态Fei8Ni82合金薄膜在50 Hz交流磁场下,测得其饱和磁感应强度为1.08 T,最低矫顽力为20 A/m.19 μm厚的纳米晶薄膜的断裂应力达到785MPa,显微硬度达到605Hv.
关键词:
铁镍合金
,
薄膜
,
电沉积
,
纳米结构
,
性能
邓联文
,
周亮
,
李慧敏
,
黄生祥
,
丁丽
,
周克省
材料导报
利用ZnFeO4铁氧体材料居里温度对Zn含量敏感的特点,将其作为主成分,通过Cu、Ti离子掺杂技术调整居里温度并提高材料的温度稳定性.采用传统氧化物工艺制备CuTiZn尖晶石铁氧体材料;采用测量起始磁导率的温变曲线间接测量居里温度的方法,获得了CuTiZn磁热铁氧体材料的居里温度.结果表明,Zn含量增加将使居里温度快速下降;材料成分为Cu.0.45Zn0.55Ti0.03Fei.97O4时居里温度为44.9℃,起始磁导率达852.5,且居里温度点磁导率的变化率达50.3/℃,该组分的CuZnTi铁氧体具有良好的自控温灵敏度,可以用作温热疗法磁热材料.
关键词:
CuTiZn铁氧体
,
居里温度
,
磁热效应
,
温热疗法
马建勋
,
严密
,
赵传礼
,
肖洪博
,
文玉华
,
杨德仁
材料科学与工程学报
doi:10.3969/j.issn.1673-2812.2005.02.023
本文研究了Sm含量,凝固速度及Nb和Zr元素的添加对Sm-Fe合金微观组织及氮化后Sm2Fei7Nx合金磁性能的影响.研究结果表明:采用真空感应炉熔炼Sm-Fe合金,当Sm的补偿量大于10wt%时,合金铸锭组织中出现大量的富Sm相,这将导致氮化后磁体磁性能的恶化;提高铸锭的冷却速度及添加Nb和Zr等元素可以有效地细化铸锭中α-Fe相的晶粒,减少均匀化退火后α-Fe相的数量,提高磁性能.
关键词:
微观组织
,
Sm2Fei7Nx
,
磁性能
孙保基
,
张葆
,
宋策
,
龙思源
液晶与显示
doi:10.3788/YJYXS20163109.0921
针对TLD算法的特征点无法有效表述目标问题，提出了一种基于角点增强改进的TLD目标跟踪算法。改进算法在跟踪模块加入了对目标表述能力更强，具有光照不敏感性和旋转不变性的 Shi-Tomas 角点作为跟踪特征点。跟踪器运行时，在角点经光流法跟踪和双向误差检测后，利用剩余的稳定角点定位目标窗口。对照结果表明，改进算法在面对目标抖动和形变时可以稳定跟踪；有效抑制因跟踪平滑点造成的漂移现象；提高了跟踪的稳定性。针对 TLD算法跟踪过程中因在线模板积累造成的计算量持续增大、实时性持续降低的问题，提出了一种依据相似度中值的模板判断删除机制。该删除机制在模板积累到设定阈值时运行，根据模板与当前目标的相似度，删除不再具备代表性的模板；调整模板空间并更新模板数目。实验表明，该删除机制在应对模板更新快、持续时间长的跟踪情景时有效降低算法计算量，实时性可提高约20％。
关键词:
目标跟踪
,
TLD
,
角点特征
,
在线模板
李晓红
,
关颖
,
李伟
,
张静武
,
张湘义
功能材料
采用X射线衍射分析(XRD)技术,研究了NdprFeCoB熔体快淬所制备的α-Fee/Nd2Fe14B纳米晶的织构形成过程.结果表明,Nd2Fe14B纳米晶具有较强的(001)织构,而α-Fe纳米晶具有(110)织构,这些织构垂直于薄带表面,且从自由面到激冷面逐渐减弱.从自由面到激冷面,Nd2Fe14B相在(001)晶面法线方向的尺寸和α-Fe相在(220)晶面法线方向的尺寸逐渐减小.在激冷面各晶面法线方向的尺寸相近,表明纳米晶的形状近似于等轴晶.α-Fe/Nd2Fei4B纳米晶织构的形成和生长受合金薄带在凝固过程中热流梯度的控制.
关键词:
复合纳米永磁体
,
晶体织构
,
控制
,
凝固
