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密相气力输送颗粒静电波动信号多尺度分析

许传龙 , 王式民

工程热物理学报

在加压密相气力输送实验装置上获得了不同操作条件下煤粉颗粒静电波动信号,并用Hilbert-Huang变换、功率谱进行分析.结果表明:随着表观速度的增加,静电波动信号主峰值的频率增大;静电波动信号希尔伯特-黄变换(Hilbert-Huang)揭示了气固两相流静电信号的非线性和非平稳特征,随气固两相流颗粒相浓度降低和颗粒及表观速度增加,静电波动信号特征尺度由高尺度(低频)向低尺度(高频)转移.多尺度分析有助于认识气固两相流动形态及其转变规律.

关键词: 颗粒静电 , 静电传感器 , 气-固两相流 , Hilbert-Huang变换

1998 COMPREHENSIVE TABLE OF CONTENTS

中国腐蚀与防护学报

N。1Atmospheric Corrosivlty for Steels………………………………………………… .LIANG Caideng HO[I i。-tat(6)Caustic Stress Corrosion Cr。king of Alloy 800 Part 2.The Effect of Thiosul执e……………………………………… KONG De-sheng YANG Wu ZHAO Guo-zheng HUANG De.ltL。ZHANG Yu。。he CHEN She。g-bac(13)SERS slid E16CttOCh6iniC81 Stlldy Of Illhibit1Oli M6ch&tllsth Of ThlollY68 Oil ITOll ID H....

关键词:

Shock compression of monocrystalline copper: Experiments, characterization, and analysis

Materials Science and Engineering a-Structural Materials Properties Microstructure and Processing

Monocrystalline copper samples with [001] and [221] orientations were subjected to shock/recovery experiments at 30 and 57 GPa and 90 K. The slip system activity and the microstructural evolution were investigated. Different defect structures, including dislocations, stacking faults, twins, microbands, and recrystallized grains were observed in the specimens. The residual microstructures were dependent on crystalline orientation and pressure. The differences with crystalline orientations are most likely due to different resolved shear stresses on specific crystalline planes. The geometric relationships between the shock propagation direction and crystalline orientation are presented under uniaxial strain. It is shown that the [2 2 11 orientation, by virtue of having fewer highly activated slip systems, exhibits greater concentration of deformation with more intense shear on the primary system. This, in turn leads to greater local temperature rise and full recrystallization, in spite of the thermodynamic residual temperature of similar to 500 K and rapid cooling (within 20 s) to ambient temperature. The profuse observation of microbands is interpreted in terms of the mechanism proposed by Huang and Gray [J.C. Huang, G.T. Gray III, Acta Metallurgica 37 (1989) 3335-3347]. (C) 2009 Elsevier B.V. All rights reserved.

关键词: Shock compression;Shock loading;Slip bands;Microtwins;Microbands;strain rate history;single-crystals;grain-size;constitutive;description;plastic-deformation;mechanical response;deformed metals;loaded nickel;substructure;recrystallization

BiNbO_4纳米棒的制备及光催化性能研究

赵洁 , 姚秉华 , 冯逸晨

功能材料

采用共沉淀法制备BiNbO4纳米棒。利用X射线粉末衍射仪(XRD)、透射电镜(TEM)、紫外-可见漫反射光谱(UV-Vis DRS)和热重分析(TG/DTA)对其结构、形貌和性质进行表征,并通过紫外-可见分光光度计分析BiNbO4纳米棒光降解罗丹明B来研究其光催化活性。结果表明以五氧化二铌和五水硝酸铋为原料制备得到正交相结构的BiNbO4纳米棒;BiN-bO4纳米棒具有较高的光催化活性,在紫外光下,pH值=3.05,催化剂用量为2g/L时能够有效地降解罗丹明B,降解率受到光源、催化剂浓度和溶液pH值的影响较大。

关键词: 共沉淀法 , BiNbO4纳米棒 , 光催化

基于稀疏随机投影的SIFT医学图像配准算法

杨飒 , 郑志硕

量子电子学报 doi:10.3969/j.issn.1007-5461.2015.03.005

针对尺度不变特征变换(Scale-invariant feature transform,SIFT)算法在关键点特征描述向量阶段计算复杂并且维数较高的现象,提出了一种基于压缩感知理论的SIFT算法.通过压缩感知理论的稀疏特征表示方法,对SIFT关键点特征向量进行提取,将高维梯度导数向量降到低维稀疏特征向量,降低了关键点描述向量维度.采用欧式距离作为关键点的相似性度量, Best-Bin-First(BBF)数据结构避免穷举,使数据的运算量大为减少.实验结果表明,新算法对存在仿射变换的医学图像配准性能优于传统SIFT算法,与当前改进型的SIFT算法相比,本文算法的实时性明显增强.

关键词: 图像处理 , 图像配准 , 尺度不变特征变换 , 特征提取 , 稀疏随机投影

DTPA及其衍生物与乳酸脱氢酶的酶学研究及光谱测定

李伟国 , 祁超 , 刘立岩 , 赵大庆

应用化学 doi:10.3969/j.issn.1000-0518.2005.11.003

分别研究了二乙三胺五乙酸(DTPA)及2种衍生物二乙三胺五乙酸-双二甲酰胺(DTPA-BDMA)和二乙三胺五乙酸-双(异烟肼)(DTPA-BIN)对乳酸脱氢酶活性及酶促反应动力学的影响.结果表明,它们均可以抑制脱氢酶的活性,其抑制类型为竞争性的抑制作用,抑制常数分别为3.37、7.41、8.52μmol/L.紫外差谱结果表明,DTPA及其衍生物可以和酶分子作用,其羧基部分被包埋到分子内部,在酶分子的结合部位存在芳香族的氨基酸残基.DTPA与脱氢酶作用后使酶分子中的色氨酸荧光强度减弱,对酪氨酸的荧光没有明显影响.

关键词: 二乙三胺五乙酸 , 乳酸脱氢酶 , 酶学动力学 , 紫外差谱 , 荧光光谱

Mean-field theory for ferroelectricity in Ca(3)CoMnO(6)

Physical Review B

An elastic Ising model for CoMnO(6) chain is proposed to explain the ferroelectricity induced by collinear magnetic order in Ca(3)CoMnO(6), and then a mean-field theory with interchain spin interactions based on this model is developed. With inclusion of the dynamics of polarization domains at finite temperature, we address the rationality of our theory by the good agreement of the calculated electric polarization and dielectric susceptibility with the reported data on Ca(3)Co(2-x)Mn(x)O(6) (x approximate to 0.96) [Y. J. Choi, H. T. Yi, S. Lee, Q. Huang, V. Kiryukhin, and S.-W. Cheong, Phys. Rev. Lett. 100, 047601 (2008)], a typical diatomic Ising spin chain system, while the predicted magnetic susceptibility shows some difference from experiment, the reason of which is discussed.

关键词: calcium compounds;cobalt compounds;dielectric polarisation;ferroelectricity;Ising model;magnetic susceptibility;multiferroics;optical susceptibility;one-dimensional oxides;magnetic-properties;multiferroics;ca3co1+xmn1-xo6

Lu-induced orthorhombic phase in polycrystalline La0.7Sr0.3MnO3

Physica B-Condensed Matter

Polycrystalline La0.5Lu0.2Sr0.3MnO3 samples prepared by thermal decomposition are investigated by means of electron diffraction and high-resolution transmission electron microscopy. Besides rhombohedral La0.7Sr0.3MnO3 phase (R-phase) and hexagonal LuMnO3 phase (H-phase) reported by Huang, unexpectedly, an orthorhombic lattice (O-phase) with space group Pnma is observed in the interior of R-phase grain. The lattice parameters of the orthorhombic unit cell are a(o) = 5.44 angstrom, b(o) = 7.65 angstrom and c(o) = 5.48 angstrom The formation of O-phase results from a(-)b(+)a(-) type orthorhombic distortion of MnO6 octahedra induced by partial substitution of Lu3+ for La3+. Meanwhile, based on image simulation of the interface between R and O-phases, the atomic bonding on the interface is particularly discussed. (c) 2005 Elsevier B.V. All rights reserved.

关键词: orthorhombic lattice;octahedral;substitution;atomic bonding;la0.7-xluxsr0.3mno3 perovskites;transport-properties;magnetoresistance;films

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