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Selection of Heat Treatment Process and Wear Mechanism of High Wear Resistant Cast Hot-Forging Die Steel

WEI Min-xian , WANG Shu-qi , WANG Lan , CUI Xiang-hong , CHEN Kang-min

钢铁研究学报(英文版)

Dry sliding wear tests of a Cr-Mo-V cast hot-forging die steel was carried out within a load range of 50-300 N at 400 ℃ by a pin-on-disc high-temperature wear machine. The effect of heat treatment process on wear resistance was systematically studied in order to select heat treatment processes of the steel with high wear resistance. The morphology, structure and composition were analyzed using scanning electron microscopy (SEM), X-ray diffraction (XRD) and energy dispersive spectroscopy (EDS); wear mechanism was also discussed. Tribo-oxide layer was found to form on worn surfaces to reduce wear under low loads, but appear inside the matrix to increase wear under high loads. The tribo-oxides were mainly consisted of Fe3O4 and Fe2O3, FeO only appeared under a high load. Oxidative mild wear, transition of mild-severe wear in oxidative wear and extrusive wear took turns to operate with increasing the load. The wear resistance strongly depended on the selection of heat treatment processes or microstructures. It was found that bainite presented a better wear resistance than martensite plus bainite duplex structure, martensite structure was of the poorest wear resistance. The wear resistance increased with increasing austenizing temperature in the range of 920 to 1120 ℃, then decreased at up to 1220 ℃. As for tempering temperature and microstructure, the wear resistance increased in following order: 700 ℃ (tempered sorbite), 200 ℃ (tempered martensite), 440 to 650 ℃ (tempered troostite). An appropriate combination of hardness, toughness, microstructural thermal stability was required for a good wear resistance in high-temperature wear. The optimized heat treatment process was suggested for the cast hot-forging steel to be austenized at 1020 to 1120 ℃, quenched in oil, then tempered at 440 to 650 ℃ for 2 h.

关键词: cast hot-forging die steel , heat treatment process , high-temperature wear mechanism , wear behavior , microstructure

Effect of Microstructures on Elevated-Temperature Wear Resistance of a Hot Working Die Steel

WEI Min-xian , WANG Shu-qi , WANG Lan , CHEN Kang-min

钢铁研究学报(英文版)

Elevated-temperature wear tests under atmospheric conditions at 400 ℃ were performed for a hot working die steel H21 on a pin-on-disk wear tester. The phase and morphology of worn surfaces were examined using XRD and SEM, and the relation of wear resistance to tempered microstructures was studied for H21 steel. XRD patterns exhibit that oxidative wear is a predominated wear mechanism with Fe3O4 and Fe2O3 on worn surfaces. It is found that with increasing normal load, obvious plastic deformation of substrate appears on worn surfaces. Microstructures start to affect apparently wear resistance of the steel with an increase of load. Under loads of 50-100 N, wear losses of steel retain low values and relatively approach for steels with various microstructures. As loads are increased to 150-200 N, wear losses of steel start to increase obviously and present apparent difference for steel with various microstructures. Wear resistance is found to increase in the sequence as follows: tempered sorbite, tempered martensite, tempered troostite without secondary hardening and tempered troostite with secondary hardening or upcoming one. Higher strength and microstructural stability are required for steels with excellent wear resistance.

关键词: steel , heat treatment , microstructure , wear , wear resistance

Chen系统的状态变量周期性反馈控制

李开明 , 李亚洲 , 冯维贵 , 林长

量子电子学报 doi:10.3969/j.issn.1007-5461.2007.05.014

采用非线性反馈控制,用附加了带参数的正弦项对Chen系统进行了有效的控制.随着参数k的逐渐增大,系统的动力学行为呈现出一系列的变化.数值研究结果表明:随控制参数的增大,驱动信号的强度渐大,混沌系统由混沌运动到周期轨道,最终到一相点.

关键词: 混沌 , Chen系统 , 不动点 , Lyapunov指数 , 反馈控制

THEREVERSSE TRANSFOR MATION OF THE STERSS INDUCEDεMIN FE 17MN 10CR 5SI 4NIALLOY

Q.S. Liu1 , 2 , 3) , L.C. Zhao3) , G.X. Dong2) and N.J. Gu1) 1) Heibei University of Technology , Tianjin 300130 , China 2) Tianjin Institute of Technology , Tianjin 300191 , China 3) Harbin University of Technology , Harbin 150001 , China

金属学报(英文版)

Theconstruction changinginthereversetransformation ofthestress induced εMin Fe 17 Mn 10 Cr 5 Si 4 Ni alloy is carefully inspected in transmission electron microscope, and then stress induced εM procedure of reverse transformation is analyzed. The behavior of reverse transformationisdissimilar when the organization of εMis different. The reversetransfor mation ofεM withtheshapeofsingle plateandstripisrelativelyeasy,anditsreversibilityincrystallographiciseasilytocarryout,fortheεM with multilayerstructure,thereversetrans formationtakes placein isolatedlayers, fortheεMthat grows well,thereversetransforma tion isrelatively difficult becauseofthe ductile harmonization between itsinternalorganiza tion structures.

关键词: stress induced εM , null , null

[C16min]Br修饰的多壁碳纳米管及其与低密度聚乙烯复合材料的制备及介电性能

徐佩 , 卢旭鑫 , 汪传斌 , 杨善中 , 孙晓红 , 丁运生

高分子材料科学与工程

为改善多壁碳纳米管(MWNT)在低密度聚乙烯(LDPE)中的分散性及复合材料的界面特性,采用溴化-1-十六烷基-3-甲基咪唑基离子液体([C16min]Br)对MWNT进行表面改性,并用Raman光谱对改性效果进行了表征.将经过修饰的碳纳米管(MIL)与LDPE熔融共混得到MIL/LDPE复合材料,采用场发射扫描电子显微镜(FESEM)和阻抗分析仪(LCR)对复合材料的结构与介电性能进行了分析.结果表明,相比与MWNT/LDPE(渗流阈值为5.2%,介电常数为82,介电损耗为0.93),MIL/LDPE(渗流阈值为9.1%,介电常数为169,介电损耗为0.51)介电常数增大,介电损耗降低.并且在低温时,MIL/LDPE介电常数随温度的变化甚小,显示出良好的温度-介电常数特性.

关键词: 咪唑基离子液体 , 碳纳米管 , 低密度聚乙烯 , 介电性能

Ion sputter erosion in metallic glass-A response to "Comment on: Homogeneity of Zr(64.13)Cu(15.75)Ni(10.12)Al(10) bulk metallic glass" by L-Y. Chen, Y-W. Zeng, Q-P. Cao, B-J. Park, Y-M. Chen, K. Hono, U. Vainio, Z-L. Zhang, U. Kaiser, X-D. Wang, and J-Z Jiang J. Mater. Res. 24, 3116 (2009)

Journal of Materials Research

The morphology of the dark and bright regions observed by transmission electron microscopy for the Zr(64.13)Cu(15.75)Ni(10.12)Al(10) bulk metallic glass strongly depends on the ion beam parameters used for ion milling. This indicates that the ion beam could introduce surface fluctuation to metallic glasses during ion milling.

关键词: room-temperature

第27卷B辑作者索引

金属学报

Volu扣ne 27SeriesB1991AUTHOR INDEX CCAO Guanghan(曹光旱)············……6一B科6CAo weijie(曹卫恋)..················……5一B32oCAO Yilin(曹益林)··················……6一B443CHANG Xin(常听)···············……1一B48CHE Guang邻n(车广灿)·············一6一B科0CHEN Erbao(陈二保)···············……6一B410CHEN Jia....

关键词:

基于二氧化碳封存的超临界两相流动的数值研究

高诚 , 胥蕊娜 , 陈黎 , 姜培学

工程热物理学报

格子Boltzmann方法(LBM)在计算复杂结构物理模型时具有独特优势并在模拟两相流动过程中能够高效清晰捕捉相界面.本文介绍了基于Shan-Chen多相模型的格子Boltzmann方法的理论成果以及基于二氧化碳封存的超临界两相流的模拟研究.结果表明,Shan-Chen模型在模拟两相流时符合Laplace定律,且两相层流时的速度分布和相渗曲线均与理论值吻合.二氧化碳封存过程中,较大的注入速率在提高二氧化碳残余俘获量的同时会降低其化学俘获量.

关键词: 二氧化碳封存 , 超临界两相流 , Shan-Chen模型

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