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TEM OBSERVATION OF ION-PLATED Al FILM ON Ni SUBSTRATE

WAN Lijun Dalian Maritime University , Dalian , Liaoning , China CHEN Baoqing Dalian Institute of Technology , Dalian , Liaoning , China GUO Kexin(K.H.KUO) Institute of Metal Research , Academia Sinica , Shenyang , China Institute of Metal and Technology , Dalian Maritime University , Dalian , Liaoning , China

金属学报(英文版)

A new phase was found at the interface between Al film and Ni substrate when the time of ion-plating reaches 5 min.It was identified to be body centered tetragonal lattice with the constants a=b=0.588 nm,c=0.480 nm.The variation of microstructure and phases with the ion-plating time were observed.Based on these results,the ion-plating film formation mech- anism has been also discussed.

关键词: magnetron sputtering , null , null , null

EFFECT OF MAGNETIC FIELD ON MARTENSITIC TRANSFORMATION IN Fe-21Ni-4Mn ALLOY

SUN Enxi Dalian Railway College , Dalian , ChinaYANG Dazhi Dalian University of Technology , Dalian , ChinaXU Zuyao (T.Y.Hsu) Shanghai Jiaotong University , Shanghai , ChinaYANG Fuming ZHAO Ruwen Institute of Physics , Academia Sinica , Beijing , China YANG Dazhi , Professor , Dalian University of Technology , Dalian 116024 , China

金属学报(英文版)

The pulsed magnetic field induced martensitic transformation with isothermal and athermal kinetics in Fe-2Ni-4Mn(wt-%)alloy has been studied by means of magnetization measurements,optical microscopy and thermodymical analyses.It is shown that there exits a critical magnetic intensity for induing martensitic transformation at a given temperature above Ms.The critical magnetic field increases linearly with increasing ΔT= T-M_S.The magnetic field strongly promotes the athermal martensitic transforamtion and restrains the isothermal one.The entropy change ΔS for athermal transformation at Ms is 4.13 J/mol· K.The effect of magnetic field on martensitic transformation in Fe-21Ni-4Mn alloy is main- ly due to Zeeman effect.Lath,plate and butterfly martensities were observed under magnetic field.

关键词: magnetic field-induced martensitic transformation , null , null

Isothermal Aging Kinetics in CuZnAl Shape Memory Alloy

Zengqi ZHAO Lab.of Physics , Baotou Research Institute of Rare Earth , Baotou , 014010 , ChinaFeixia CHEN Dazhi YANG Dept.of Mater.Eng. , Dalian University of Technology , Dalian , 116024 , ChinaEr BAO Dept.of Mater.Eng. , Yanshan University , Qinhuangdao , 066004 , China

材料科学技术(英文)

Isothermal aging behaviours of a CuZnAl shape memory alloy have been investigated by means of dilatometry.The length of the specimens during isothermal aging from 190 to 280℃ increases with the aging time at each temperature.The isothermal aging kinetics fits in Avrami equation and the time exponent n decreases with the increase in aging temperature.The apparent activation energy for the isothermal aging process was measured to be 109.0kJ/mol,which is about equal to that of a relaxation internal friction peak at about 200℃ (f≈1 Hz) in the alloy.

关键词: isothermal aging kinetics , null , null , null , null

GROWTH OF ISOTHERMAL MARTENSITE IN AN Fe-Ni-Mn ALLOY

YANG Dazhi ZHU Min Dalian Institute of Technology , Dalian , Liaoning , China. YANG Dazhi , Professor , Dept.of Mater.Sci.and Eng. , Dalian Institute of Technology , Dalian , Liaoning , China

金属学报(英文版)

The substructural development of martensite plates at different stage of the transformation for an Fe-21Ni-4Mn alloy has been investigated by using transmission electron microscope. Twinning was found in small thin platelets at the initial stage.Fine twins extend to the whole platelet.The dislocations and twins were found in the thick platelets at a later stage.Bending of the twins was also observed frequently at this stage.Finally,several platelets coalesce with each other to form a macroscopic(252)_f martensite“plate”.The original habit plane of the individual platelet was measured to be close to(121)_f.

关键词: Fe-Ni-Mn alloy , null , null

EFFECTS OF DEFORMATION ON MICROSTRUCTURE AND σ-PHASE FORMATION IN Cr_(25)Ni_(20) STAINLESS STEEL

GAO Yan LI Dejun CAO Zhiben Dalian University of Science and Technology , Dalian , Liaoning , China LI Dejun , Lecturer , Department of Materials Engineering , Dalian University of Science and Technology , Dalian , Liaoning , China

金属学报(英文版)

The microstructure of Cr_(25)Ni_(20)stainless steel under plastic deformation up to 50% has re- vealed an even distributed twins,micro-twins and deformation bands.The σ-phase formation in 800℃ aged specimens is accelerated by its nucleation at either deformation twins or recrystallized grain boundaries under less or more deformation respectively.In the recrystallized zone,the recrystallization is prior to the precipitation of σ-phase.Although recrystallization may accelerate the formation of σ-phase,it is not essential.The twins and micro-twins produced by deformation may also provide the additional nucleation sites.

关键词: plastic deformation , null , null

THERMAL FATIGUE AND FRACTURE MECHANICS ANALYSIS OF GREY CAST IRON

GUO Chengbi ZHOU Weisheng Dalian Institute of Technology , Dalian , Liaoning , China Professor , Dept.of Shipbuilding , Dalian Institute of Technology , Dalian , Liaoning , China

金属学报(英文版)

The in-phase and out-of-phase thermal fatigue,the C-P type and P-C type isothermal fa- tigue of grey cast iron were experimentally studied.The fatigue life was evaluated analytically by using the elastic-plastic fracture mechanics method(mainly J integral).The results of ex- periments and calculations showed that the lifes of in-phase and C-P type fatigue are longer than that of out-of-phase and P-C type fatigue respectively within the same strain range. This is in contrast to the results of other materials such as low carbon steel.On the other hand, the predicted lifes are consistent with experimental results.This suggests that J integral as a mechanics parameter for characterizing the thermal fatigue strength of grey cast iron and the mechanics model and the calculation method developed here are efficient.A parameter ΔW_1 was proposed from energy aspect to characterize the capacity of crack propagation. The isothermal fatigue life is the same as the thermal fatigue life for identical ΔW_1 values.

关键词: grey cast iron , null , null

Oxygen Relief/Absorption and Superconductivity of Bi-Pb-Sr-Ca-Cu-O Compounds

QIN Zuoxiang , ZHANG Yansheng , ZHU Naiping Department of Materials Engineering , Dalian Railway Institute , Dalian , 116022 , China.Institute of Metal Research , Academia Sinica , Shenyang , 110015 , China.

材料科学技术(英文)

The oxygen relief/absorption,superconduc— tivity and structure of(Bi_(1-x)Pb_x)_2Sr_2Ca_2— Cu_3O_y compounds have been studied by TGA, electrical resistance measurement and X-ray diffraction.The amount of oxygen which can be re- leased and superconductivity of the compounds are correlative to Pb content.The release of oxygen in- creases when x less than 0.2 and decreases when x exceeds 0.2 with increasing x.The appropriate con- tent of Pb for superconductivity is in the range of 0.1

关键词: oxygen relief/absorption , null , null , null

(α+β)Dual Phase CuZnAl Shape Memory Alloy

ZHAO Xu , QI Min , YANG Dazhi Institute of Metal Research , Academia Sinica , Shenyang , 110015 , China.Department of Materials Engineering , Dalian University of Technology , Dalian , 116012 , China.

材料科学技术(英文)

The effect of α phase on CuZnAl shape memo- ry alloy(SMA)has been systematically studied by electrical resistance method,quantitative measure- ment of micrography and transmission electron microscopy(TEM).It is found that,by controlling the amount of α phase in(α+β)-CuZnAl alloy, phase transformation temperatures can be adjusted precisely in a wide range,while the good shape memory effect of CuZnAl is kept.In a word, quenching from(α+β)dual phase region is a rea- sonable method of adjusting phase transformation temperatures for CuZnAl alloy.

关键词: (α+β)-CuZnAl alloy , null , null

GRAIN BOUNDARY FEATURE AND CREEP BEHAVIOR OF Fe-15Cr-25Ni ALLOYS

ZHANG Junshan CHEN Weixing CAO Zhiben Dalian University of Technology , Dalian , China Associate Professor , Department of Materials Engineering , Dalian University of Technology , Dalian , China

金属学报(英文版)

Creep behavior of Fe-15Cr-25Ni alloys with different grain boundary features has been in- vestigated at 850 and 950℃ and in stress range of 14.7~78.5 MPa.The single phase alloy exhibits typical recovery creep characteristics,and for the alloy in which M_(23)C_6 carbides densely precipitate at grain boundaries,the creep rate dramatically decreases and creep behav- ior is also significantly different from the single phase alloy.When the carbides precipitate at grain boundaries,the dislocation density are higher and the size of subgrains near grain boundaries are smaller than those of single phase alloy.The creep mechanisms for two grain boundary features have been discussed.

关键词: grain boundary feature , null , null

DRY SLIDING WEAR OF Cu-BASED SHAPE MEMORY ALLOY

WANG Hongwei Dalian University of Technology , Dalian , ChinaWU Wangzi Shenyang Institute of Technology , Shenyang , ChinaWANG Fengting YANG Dazhi Dalian University of Technology , Dalian , China

金属学报(英文版)

The wear of Cu-based CuZnAl shape memory alloys under dry sliding against steel was found to be plasticity-dominated,with adhesion and delamination being the two main mecha- nisms.Adhesion was found to be accompanied by metal transfer.TEM observation on tensile test of thin foil showed that the stress-induced martensitic transformation occurred from β-phase in the vicinity of pre-existing microcracks.The blunt effect of crack tips may be proposed to explain the wear of CuZnAl shape memory alloy due to preferential orientation reaction of variants in martensite and stress-induced martensitic transformation in β-phase.

关键词: CuZnAl allov shape memory alloy , null , null

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