材料期刊网

THERMAL FATIGUE CRACKING IN STEEL 5CrMnMo

HE Shiyu LI Ying LIU Jianhong Harbin Institute of Technology , Harbin , China HE Shiyu , Faculty of Metal , Harbin Institute of Technology , Harbin , 150006 , China

金属学报(英文版)

The thermal fatigue behaviour of steel 5CrMnMo after various heat treatments has been examined by means of Coffin-model and self-strained thermal fatigue testing machines.The thermal fatigue crack initiation and propagation have been observed under SEM and TEM. The majority of thermal fatigue cracks of the quenched samples initiated firstly at the grain boundaries and that of the quenched-tempered samples at the breakage interface of the car- bide and matrix.The thermal fatigue cracks of either quenched or quenched-tempered steel propagated mainly along the breakage interface of carbide and grain boundaries.

关键词: thermal fatigue crack , null , null

Brief Outline of the Metallurgy Department of Kunming Institute of Technology

LIU Chunpeng Kunming Institute of Technology , Kunming 650093 , China.

材料科学技术（英文）

关键词:

THERMAL NUCLEATION AND GROWTH OF He BUBBLES IN He IMPLANTED STAINLESS STEELS

ZHANG Lei WANG Peixuan TAO Rong MA Ruzhang ZHANG Guoguang University of Science and Technology Beijing , Beijing , China professor , Department of Materials Physics.University of Science and Technology Beijing.Beijing 100083 , China

金属学报(英文版)

Nucleation and growth of He bubbles at different annealing temperatures T≤1023 K in stain- less steels HR-2 and SS321,implanted with He~+(40-70 keV.1×10~(16)-6× 10~(17) He~+/cm~2),were ohserved under TEM.T=0.45T_m seems to be a transition temperature.The He bubbles continue mainly their nucleation at 0.3T_m< T<0.45T_m,and grow predominantly at T≥0.45T_m,due probably to migration and coalescence by surface diffusion of metal atoms around the bubbles.The apparent activation energies for the growth are found to he 0.41 and 0.31 eV for HR-2 and SS321 respectively.The bubble density in HR-2 is greater than that in SS321 within whole measuring temperature range,and the onset temperature of rapid swelling is also higher.It is believed that the resistance of HR-2 to He is superior to that fo SS321.

关键词: stainless steel , null , null , null , null

Microstructures and Dielectric Properties of Ba_1-xSr_xTiO₃ Ceramics Doped with B₂O₃-Li₂O Glasses for LTCC Technology Applications

Xiujian Chou

材料科学技术（英文）

Ba_1-xSr_xTiO₃ ceramics, doped with B₂O₃-Li₂O glasses have been fabricated via a traditional ceramic process at a low sintering temperature of 900 °C using liquid-phase sintering aids. The microstructures and dielectric properties of B₂O₃-Li₂O glasses doped Ba_1-xSr_xTiO₃ ceramics have been investigated systematically. The temperature dependence dielectric constant and loss reveals that B2O3-Li₂O glasses doped Ba_1-xSr_xTiO₃ ceramics have diffusion phase transformation characteristics. For 5 wt% B₂O₃-Li₂O glasses doped Ba0:55Sr0:45TiO₃ composites, the tunability is 15.4% under a dcpplied electric field of 30 kV/cm at 10 kHz; the dielectric loss can be controlled about 0.0025; and the Q value is 286. These composite ceramics sintered at low temperature with suitable dielectric constant, low dielectric loss, relatively high tunability and high Q value are promising candidates for multilayer low-temperature co-fired ceramics (LTCC) and potential microwave tunable devices applications.

关键词: Sintering

Titanium technology in the USA - an overview

D.Eylon , S.R.Seagle

材料科学技术（英文）

The state of Ti research, development and industry is reviewed in this article. The fifty-year anniversary of Ti technology commercialization in the USA provides an opportunity for a historical perspective. Incorporation of "information-age" tools into alloy development, processing, and production invigorates the technology. Consolidation, diversification and globalization have been transforming the Ti industry in the recent years.

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NUMERICAL ANALYSIS OF THREE-DIMENSIONAL FLUID FLOW AND HEAT TRANSFER IN TIG WELD POOL WITH FULL PENETRATION

WU Chuansong , CAO Zhenning , WU Lin Harbin Institute of Technology , Harbin , China

金属学报(英文版)

A model is established to analyze three-dimensional fluid flow and heat transfer in TICweld pools with full penetration.It considers the deformation of the molten pool surfaceat the condition of full penetrated workpieees,takes the are pressure as the drivingforce of the pool surface deformation,and determines the surface configuration of weldpool based on the dynamic balance of arc pressure,pool gravity and surface tension atdeformed weld pool surface. The SIMPLER algorithm is used to calculate the fluid flowfield and temperature distribution in TIG weld pools of stainless steel workpieces.TIGwelding experiments are made to verify the validity of the model.It shows the calculatedresults by the model are in good agreement with experimental measurements. professor,Dept of Welding Engineering,Harbin Institute of Technology,Harbin 150006,China

关键词: KEY WORDS TIG weld pool , null , null , null , null

高温退火后含He纳米晶钛膜中He相关缺陷的演化

李悦 , 邓爱红 , 刘莉 , 王康 , 谢莎

材料研究学报

利用x射线衍射(xRD)和慢正电子束分析(SPBA)技术研究高温退火后含He钛膜的微观结构和钛膜内He相关缺陷的演化.XRD分析表明,高温退火后Ti和Si在高温下发生反应形成稳定的多晶TiSi2化合物,He原子的掺入会影响TiSi2晶体的择优取向,而对TiSi2晶粒尺寸的影响较小.SPBA结果表明,室温下,钛膜内的缺陷浓度或尺寸会随着掺He浓度的增加而增大;高温退火后,当He浓度小于5％(原子分数,下同)时(除2％外),钛膜内的He相关缺陷浓度随着He浓度增加相应地增加.当He浓度增加到14％时,高温会使较高浓度的He原子、He-空位复合体以及小He泡迁移聚集形成一些尺寸较大He泡,而较大He泡周围与He相关的小尺寸缺陷的浓度则会发生相应地减少.

关键词: 金属材料 , 含He钛膜 , 直流磁控溅射 , He相关缺陷 , XRD , SPBA

直流磁控溅射沉积含He钛膜的研究

施立群 , 金钦华 , 刘超卓 , 徐世林 , 周筑颖

原子核物理评论 doi:10.3969/j.issn.1007-4627.2005.01.045

研究了用He/Ar混合溅射气体的直流磁控溅射制备钛膜中He的掺入现象.分析结果表明,大量的He原子(He/Ti原子比高达56%) 被均匀地引入到Ti膜中,He含量可由混合溅射气体的He分量精确控制.通过调节溅射参数,可实现样品中He的低损伤引入.研究还发现,溅射沉积的含氦Ti膜具有较高的He成泡剂量和高的固He能力,这可能是溅射沉积形成了纳米晶Ti膜所致.纳米晶Ti膜较粗晶材料具有很高浓度的He捕陷中心,使He泡密度增大而泡尺寸减小.随He引入量的增加,Ti膜的晶粒尺寸减小,He引起的晶体点阵参数和X射线衍射峰宽度增大,晶体的无序程度增加.

关键词: 氦 , 损伤 , 泡 , 钛膜 , 溅射沉积

Microstructure and mechanical properties of Ni(3)Al and Ni(3)Al-1B alloys fabricated by SHS/HE

Intermetallics

The well-densified Ni(3)Al alloys without and with boron addition were fabricated by self-propagation high-temperature synthesis and hot extrusion (SHS/HE) technology. Microstructure investigation showed that Ni(3)Al and Ni(3)Al-1B alloys contained fine grain structure. Analysis of X-ray spectra as well as transmission electron microscopy studies revealed that three phases present in all alloys: gamma-Ni, Ni(3)Al and dispersoids of alpha- Al(2)O(3) and gamma- Al(2)O(3). However, beta-NiAl, Ni(3)B phase and twinned Ni(3)Al crystal are observed in the Ni(3)Al-1B alloy. In addition, dislocations with high density exist in all alloys. The mechanical test showed that the B addition leads to obvious improvement in yield strength and compressive ductility, and compared with the ones synthesized by combustion, SHS/HE synthesized Ni(3)Al and Ni(3)Al-1B alloys exhibit more excellent mechanical properties. (C) 2010 Elsevier Ltd. All rights reserved.

关键词: Nickel aluminides, based on Ni(3)Al;Mechanical properties at ambient;temperature;Reaction synthesis;Microstructure;combustion synthesis;nickel;aluminides;boron

Heuristic treatments of tricritical behaviour as observed in 4He-3He mixtures and in polymeric assemblies

Physics and Chemistry of Liquids

Tricritical behaviour in three dimensions is accessible to experiment in, for example, 4He-3He mixtures and some polymeric assemblies. Here, by largely heuristic arguments, which appeal however to some specific model Hamiltonians, we indicate how one can understand the gist of the experimental results near the tricritical point in the systems cited above. We point out that the spin fluctuations at the tricritical point are much weaker than those at the critical point, which leads to the conclusion that the tricritical behaviours can be described well by the mean-field exponents with logarithmic corrections, at d = 3.

关键词: tricritical behaviour;tricritical exponents;4He-3He mixtures;polymeric assemblies;Ising model;emery-griffiths model;single-ion-anisotropy;ising-model;phase-separation;magnetic-properties;lattice statistics;crystal-field;exponents;superconductivity;transition