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Process Simulation and Microstructure Analysis of Low Carbon SiMn Quenched and Partitioned Steel

ZHAO Cai , TANG Di , JIANG Haitao , ZHAO Songshan , LI Hui

钢铁研究学报(英文版)

The quenching and partitioning (Q&P) process was experimentally investigated on the thermomechanical simulator (Gleeble3800). The microstructure and fracture mechanism of the sheets were investigated by means of TEM. It was found that the microstructure of quenched and partitioned steel consists of fine lath martensite and thin interlath austenite films. The optimum quenching temperature of producing the maximum amount of retained austenite after final quenching at room temperature was predicted by Matlab software package. It was found that the calculations by Matlab software can provide guidance for experimental processing design reliably. The volume fraction of retained austenite at room temperature was approximately 8%, which was measured easily by the software VC60++ programming. The results verified that quenched and partitioned steel possesses a good combination of strength and plasticity due to its fine microstructure. This steel exhibited high ultimate tensile strength (exceeding 1 000 MPa) and good elongation of 25%. The results showed that the fracture mechanism of the sheets is typical tough fracture under the condition of tensile failure.

关键词: Q&P;Matlab software;microstructure;mechanical property

Heredity Characteristic From Hot Rolled Microstructure to Annealed Microstructure in High Strength TRIP Steels

XIONG Ziliu , CAI Qingwu , JIANG Haitao

钢铁研究学报(英文版)

The influence of hot-rolled process on microstructure in TRIP steel and the heredity characteristic from the hot-rolled microstructure to annealed microstructure are investigated. The results show there are two kind of hot-rolled microstructures under different coiling temperatures. One is composed of coarse grains of ferrite, pearlite and bainite, and the other is composed of small grains of ferrite, bainite and austenite. After annealing, the first kind of hot-rolled microstructure is greatly refined, and volume fraction, carbon content of austenite increase significantly. However, it have little changes in grain size, volume fraction and carbon content of austenite after the second kind of hot-rolled sheet is annealed. There are also differences in distribution of retained austenite between the two annealed microstructures observed by EBSD and TEM technology. Retained austenite in the first annealed microstructure distributes mainly inside of the polygonal ferrite in the form of spot, only little retained austenite on bainte ferrite boundary, however retained austenite in the second annealing microstructure allocates several places, such as inside of polygonal ferrite, on polygonal ferrite boundary, on bainte ferrite boundary.

关键词: TRIP steel;hot-rolled;heredity;microstructure;annealing

CSD-La3TaO7薄膜外延生长行为

王耀 , 李成山 , 于泽铭 , 冯建情 , 金利华 , 王辉 , 张平祥

稀有金属

研究CSD技术制备La3TaO7 (LTO)缓冲层过程中前驱液的热分解行为以及热处理工艺对薄膜取向生长的影响,通过选取恰当的LTO前驱液以及快速升温热处理的方法最终获得了良好c轴织构的LTO薄膜.

关键词: 涂层导体 , 缓冲层 , 化学溶液沉积

Bi3+,Eu3+,Tb3+掺杂Lu3TaO7的发光性能研究

刘文鹏 , 张庆礼 , 杨华军 , 周鹏宇 , 孙敦陆 , 高进云 , 谷长江 , 罗建乔 , 王迪 , 殷绍唐

量子电子学报 doi:10.3969/j.issn.1007-5461.2011.02.018

采用固相反应法制备了Bi3+、Eu3+、Tb3+掺杂的Lu3TaO7.测量了样品的X射线衍射谱、激发和发射光谱及荧光衰减曲线.三种离子掺杂的Lu3TaO7均呈现出强的荧光发射,其中Bi3+具有峰位在431 nm处的一强发射宽带,衰减寿命为16.8μs,Eu3+、Tb3+则表现出稀土离子的特征锐发射峰,衰减寿命分别为1.26 ms和1.20 ms.因此,它们均是具有潜在应用前景的重闪烁体材料.

关键词: 材料 , 闪烁体 , Lu3TaO7 , 发光

一种基于锡锑氧化物的透明PN结及整流特性

季振国 , 周荣福 , 毛启楠 , 霍丽娟 , 曹虹

无机材料学报 doi:10.3724/SP.J.1077.2009.09217

利用反应磁控溅射法制备了半导体锡锑氧化物薄膜 (TAO). 根据霍尔效应测试结果,当Sn/Sb 原子比处于0.22~0.33范围内时,TAO薄膜是p型导电的,在此范围之外,TAO薄膜是n型导电的. 光学带隙测量结果表明,不同Sn/Sb比的TAO薄膜的禁带宽度基本相同(~3.9eV).构造了一个全透明的PN结,其中n区为Sn/Sb原子比为0.5的TAO薄膜, p区为Sn/Sb原子比为0.33的TAO薄膜.n区TAO的电极用铟锡氧化物(ITO),p区TAO的电极用Cu薄膜.实验结果表明,由于两种导电类型的TAO薄膜具有相同的禁带宽度,上述透明PN结构具有典型的准同质PN结的整流特性.

关键词: 透明半导体薄膜 , antimony-tin oxide , PN junction

一种基于锡锑氧化物的透明PN结及整流特性

季振国 , 周荣福 , 毛启楠 , 霍丽娟 , 曹虹

无机材料学报 doi:10.3724/SP.J.1077.2009.09217

利用反应磁控溅射法制备了半导体锡锑氧化物薄膜 (TAO). 根据霍尔效应测试结果,当Sn/Sb 原子比处于0.22~0.33范围内时,TAO薄膜是p型导电的,在此范围之外,TAO薄膜是n型导电的. 光学带隙测量结果表明,不同Sn/Sb比的TAO薄膜的禁带宽度基本相同(~3.9eV).构造了一个全透明的PN结,其中n区为Sn/Sb原子比为0.5的TAO薄膜, p区为Sn/Sb原子比为0.33的TAO薄膜.n区TAO的电极用铟锡氧化物(ITO),p区TAO的电极用Cu薄膜.实验结果表明,由于两种导电类型的TAO薄膜具有相同的禁带宽度,上述透明PN结构具有典型的准同质PN结的整流特性.

关键词: 透明半导体薄膜 , 锡锑氧化物 , PN结

Ion sputter erosion in metallic glass-A response to "Comment on: Homogeneity of Zr(64.13)Cu(15.75)Ni(10.12)Al(10) bulk metallic glass" by L-Y. Chen, Y-W. Zeng, Q-P. Cao, B-J. Park, Y-M. Chen, K. Hono, U. Vainio, Z-L. Zhang, U. Kaiser, X-D. Wang, and J-Z Jiang J. Mater. Res. 24, 3116 (2009)

Journal of Materials Research

The morphology of the dark and bright regions observed by transmission electron microscopy for the Zr(64.13)Cu(15.75)Ni(10.12)Al(10) bulk metallic glass strongly depends on the ion beam parameters used for ion milling. This indicates that the ion beam could introduce surface fluctuation to metallic glasses during ion milling.

关键词: room-temperature

Improved Nonlinear Equation Method for Numerical Prediction of Jominy EndQuench Curves

SONG Yuepeng , LIU Guoquan , LIU Shengxin , LIU Jiantao , FENG Chengming

钢铁研究学报(英文版)

Without considering the effects of alloying interaction on the Jominy endquench curves, the prediction results obtained by YU Baihai′s nonlinear equation method for multialloying steels were different from those experimental ones reported in literature. Some alloying elements have marked influence on Jominy endquench curves of steels. An improved mathematical model for simulating the Jominy endquench curves is proposed by introducing a parameter named alloying interactions equivalent (Le). With the improved model, the Jominy endquench curves of steels so obtained agree very well with the experimental ones.

关键词: Jominy endquench curve;nonlinear equation method;alloying interaction parameter;computer simulation

基于粒子群和有限元的材料本构模型参数的确定

倪永中 , 徐鸿

材料科学与工程学报

本文提出了一种基于粒子群算法和有限元方法的弹塑性本构方程参数的确定方法,并在此基础上开发了参数自动优化系统CMPI(Constitutive Material Parameter Identification).通过使最小二乘形式的目标函数达到极小值,实现参数的动态寻优;模型参数作为粒子群优化模块的输入,采用应变(应力)控制方法,调用材料非线性有限元模块计算特定参数时的应力(应变)响应,并计算与实验数据的误差,从而实现优化过程.CMPI目前适用于A-F类模型(Chaboehe、Ohno-Wang、Jiang-Sehitoglu)的参数优化,以此为基础,不难扩展到其他材料模型.

关键词: 粒子群 , 材料非线性 , 有限元 , Ohno-Wang 模型

不同烷基酰亚胺的合成及对镥的萃取

刘峙嵘 , 周利民 , 李传茂 , 江小昌

稀有金属 doi:10.3969/j.issn.0258-7076.2006.03.021

合成了7种同一系列新型酰亚胺类萃取剂,并运用元素分析、核磁共振、红外光谱、紫外光谱等测试手段对其物化指标进行了表征.萃取性能表明,烷基酰亚胺萃取稀土镥的能力与骨架空间结构有关.直链烷基酰亚胺萃取镥的能力大于相应的支链烷基酰亚胺,而且随链长的增长萃取能力不断增强.利用斜率法,采取直线线性回归求得镥(Ⅲ)与萃取剂基本上以1:2交换.相同条件下,7种酰亚胺类萃取剂分配比的大小顺序为DOI>DDI>DHI>HAI>HIBI>DBI>BIBI.

关键词: 烷基酰亚胺 , 合成 , , 萃取

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