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Effect of austenization temperature on the microstructure evolution of the medium manganese steel (0.2C-5Mn) during ART-annealing

Jie SHI

金属学报(英文版)

Microstructure evolution during ART-annealing (austenite reverted transformation annealing) of 0.2C-5Mn steel processed by austenitation at different temperatures was examined by SEM, TEM and XRD. It was demonstrated that the initial microstructures resulted from austenization at different temperatures strongly affect the microstructure evolution during followed ART-annealing, even the ultrafine grained ferrite/austenite duplex structure with about 30% austenite could be obtained after long time ART-annealing in all cases. Austenization in the intercritical region (between Ac1 and Ac3) gave a duplex structure after quenching, which was nearly not affected by followed annealing process. However, high temperature austenization (above Ac3) resulted in a full martensite structure after quenching, which gradually transformed into a ferrite/austenite duplex structure during the following annealing process. Based on the analysis of austenite fraction and carbon concentrate, it was found that not only carbon partitioning but also manganese partitioning in the austenite affected the stability of austenite and even dominated the development of lamellar ferrite and austenite duplex structure during intercritical annealing with different times. At last an austenite lath nucleation and thickening model was proposed to describe the microstructure evolution of medium mangenese steel during ART-annealing.

关键词: Austenization temperature

Comparison of Inconel 625 and Inconel 600 in resistance to cavitation erosion and jet impingement erosion

Nuclear Engineering and Design

Liquid droplet erosion (LDE), which often occurs in bellows made of nickel-based alloys, threatens the security operation of the nuclear power plant. As the candidate materials of the bellows, Inconel 600 and Inconel 625 were both tested for resistance to cavitation erosion (CE) and jet impingement erosion (JIE) through vibratory cavitation equipment and a jet apparatus for erosion-corrosion. Cumulative mass loss vs. exposure time was used to evaluate the erosion rate of the two alloys. The surface and cross-sectional morphologies before and after the erosion tests were observed by scanning electron microscopy (SEM), the inclusions were analyzed by an energy dispersive spectroscopy (EDS), and the surface roughness was also measured by surface roughness tester to illustrate the evolution of erosion process. The results show that the cumulative mass loss of CE of Inconel 625 is about 1/6 that of Inconel 600 and the CE incubation period of the Inconel 625 is 4 times as long as that of the Inconel 600. The micro-morphology evolution of CE process illustrates that the twinning and hardness of the Inconel 625 plays a significant role in CE. In addition, the cumulative mass loss of JIE of Inconel 625 is about 2/3 that of Inconel 600 at impacting angle of 90 degrees, and almost equal to that of the Inconel 600 at impacting angle of 30 degrees. Overall, the resistance to CE and JIE of Inconel 625 is much superior to that of Inconel 600. (C) 2010 Elsevier By. All rights reserved.

关键词: stress-corrosion cracking;aluminide intermetallic alloys;high-purity;water;mechanical-properties;crevice corrosion;solid particles;wear;behavior;microstructure;deformation;steam

Cavitation erosion and jet impingement erosion mechanism of cold sprayed Ni-Al(2)O(3) coating

Nuclear Engineering and Design

A composite coating was deposited on Inconel 600 substrate by cold spray method using pure Ni powder (60 wt.%) blended with alpha-Al(2)O(3) (40 wt.%) as feedstock. It is expected to be applied to repair the bellows eroded by the liquid droplet erosion (LDE). Microstructure of the coating was observed using optical microscope (OM) and scanning electron microscopy (SEM). Microhardness of the coating was determined by Vickers hardness tester. Cavitation erosion (CE) experiments were carried out in the distilled water. Jet impingement erosion (JIE) experiments were performed in slurry containing 1 wt.% quartz particle with the flow velocity of 15 m/s at impingement angles of 30 degrees, 60 degrees and 90 degrees, respectively. Cumulative mass loss vs. testing time was used to evaluate the erosion rate of the coating. The erosion mechanism was analyzed by OM, SEM, X-ray diffraction (XRD) and the microhardness measurement. The results show that the composite coating has compact microstructure and relatively high hardness. The resistance to CE of the coating is not as good as that of Inconel 600 substrate due to the weak bonds of the Al(2)O(3) particles. However, the results of the JIE test indicate that the slurry erosion resistance of the coating is better than that of Inconel 600 at the impact angles of 30 degrees and 60 degrees, but not at the normal impact angle. (C) 2011 Elsevier B.V. All rights reserved.

关键词: large powder particles;composite coatings;slurry erosion;kinetic;spray;liquid impact;alloy;microstructure;steels;deposition;resistance

Improving glass-forming ability of Mg-Cu-Y via substitutional alloying: Effects of Ag versus Ni

Journal of Materials Research

Based on the best bulk metallic glass (BMG) forming alloy in the Mg-Cu-Y ternary system, we introduced Ag (or Ni) to partially substitute for Cu to improve the glass-forming ability (GFA). The objective of this paper is twofold. First, we illustrate in detail a recently developed search strategy, which was proposed but only briefly outlined in our previous publication [H. Ma, L.L. Shi, J. Xu, Y. Li, and E. Ma: Discovering inch-diameter metallic glasses in three-dimensional composition space. Appl. Phys. Lett. 87, 181915 (2005)]. The protocol to navigate in three-dimensional composition space to land large BMGs is spelled out step-by-step using the pseudo-ternary Mg-(Cu,Ag)-Y as the model system. Second, our ability to locate the best BMG former in the composition tetrahedron allows us to systematically examine, and conclude on, the effects of a given alloying element. The large improvement in glass-forming ability in the Mg-(Cu,Ag)-Y system relative to the based ternary will be contrasted with the reduced glass-forming ability in the Mg-(Cu,Ni)-Y pseudo ternary system. It is demonstrated that the improvement of glass-forming ability requires judicious choice of substitutional alloying elements and concentrations, rather than simple additions of multiple elements assuming the "confusion principle."

关键词: bulk metallic-glass;shaped copper mold;amorphous-alloys;thermal-stability;ternary-system;casting method;p system;diameter;zr;mm

(1-x)Bi4Ti3O12-xSrBi2Nb2O9铋层状铁电陶瓷结构与性能研究

涂娜 , 江向平 , 李小红 , 傅小龙 , 杨帆

人工晶体学报

采用传统固相法制备了(1-x)Bi4Ti3 O12-xSrBi2 Nb2 O9(BIT-SBN,x=0,0.025,0.050,0.100,0.150,0.200)铋层状无铅压电陶瓷.系统研究了SrBi2 Nb2 O9掺杂对Bi4Ti3 O12基陶瓷物相结构、微观结构以及jie电性能的影响.结果表明:所有陶瓷样品均为单一的铋层状结构;当SBN掺量为0.100时,样品具有最佳的电性能:d33=21 pC/N,相对密度ρ =98.1%,机电耦合系数kp=8.26%,εr=220,介电损耗tanδ =0.29%,剩余极化强度Pr=9.128 μC/cm2,Tc=594℃.同时,SBN的引入增强了样品的抗老化性和热稳定性.

关键词: Bi4Ti3O12 , SrBi2Nb2O9 , 铋层状 , 铁电陶瓷 , 介电性能

基于角点增强改进的TL D目标跟踪算法

孙保基 , 张葆 , 宋策 , 龙思源

液晶与显示 doi:10.3788/YJYXS20163109.0921

针对TLD算法的特征点无法有效表述目标问题,提出了一种基于角点增强改进的TLD目标跟踪算法。改进算法在跟踪模块加入了对目标表述能力更强,具有光照不敏感性和旋转不变性的 Shi-Tomas 角点作为跟踪特征点。跟踪器运行时,在角点经光流法跟踪和双向误差检测后,利用剩余的稳定角点定位目标窗口。对照结果表明,改进算法在面对目标抖动和形变时可以稳定跟踪;有效抑制因跟踪平滑点造成的漂移现象;提高了跟踪的稳定性。针对 TLD算法跟踪过程中因在线模板积累造成的计算量持续增大、实时性持续降低的问题,提出了一种依据相似度中值的模板判断删除机制。该删除机制在模板积累到设定阈值时运行,根据模板与当前目标的相似度,删除不再具备代表性的模板;调整模板空间并更新模板数目。实验表明,该删除机制在应对模板更新快、持续时间长的跟踪情景时有效降低算法计算量,实时性可提高约20%。

关键词: 目标跟踪 , TLD , 角点特征 , 在线模板

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