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Microstructure Evolution during Friction Stir Welding of Aluminum Alloy AA2219

K.S. Arora S. Pandey M. Schaper R. Kumar

材料科学技术(英文)

The characterization of microstructure evolution in friction stir welded aluminum alloy was carried out by optical microscopy (OM) and transmission electron microscopy (TEM) and electron backscatter diffraction (EBSD). The weld nugget consisted of very fine equiaxed grains and experienced dissolution of nearly half of metastable precipitates into the matrix during welding. Thermomechanically affected zone (TMAZ) also experienced dissolution of precipitates but to a lesser extent whereas coarsening of precipitates was observed in heat affected zone (HAZ). Grain boundary misorientation measurements using EBSD indicated continuous dynamic recrystallization as the underlying mechanism for the fine equiaxed nugget grains. The yield and tensile strength of the weld decreased with comparison to base material. But due to the decrease of grain size and the dissolution of second phase precipitates, an increased Charpy energy value was observed in the weld nugget.

关键词: Friction stir welding

Secondary M6C precipitation in K40S cobalt-base alloy

Materials Letters

Secondary M,C precipitation was investigated in K40S cobalt-base alloy after 100 h aging at 950 degreesC. The results showed that it was closely related to the tungsten-rich zones inherited from the as-cast condition and the degeneration of the primary M7C3 carbide. A direct element reaction, 6M + C --> M6C, in which C comes from the decomposition of the M7C3 carbides, is suggested as the mechanism of secondary M6C precipitation in K40S alloy. (C) 2001 Elsevier Science B.V. All rights reserved.

关键词: M6C precipitation;aging;M7C3 carbide;superalloy

R. erythropolis对赤铁矿和石英的吸附?捕收作用

杨慧芬 , 唐琼瑶 , 王传龙 , 张露 , 李甜

中国有色金属学报

为考察红城红球菌(Rhodococcus erythropolis,R. erythropolis)作为赤铁矿捕收剂使用的可能性及效果,对R. erythropolis形貌、细胞壁成分及其吸附前后赤铁矿、石英表面电性、疏水性进行分析,对赤铁矿、石英单矿物以及赤铁矿与石英矿1:1(质量比)混合矿进行浮选实验,对其在赤铁矿表面的吸附状况及吸附机理进行研究.结果表明,杆状R. erythropolis表面既含有非极性基团,又含有极性基团,使得其表面具有较高的负电性和较强的疏水性,因而对赤铁矿的吸附作用明显大于对石英的吸附作用.当以此细菌为捕收剂、在溶液 pH 值为6、R. erythropolis用量为75 mg/L时,赤铁矿的回收率为89.68%,而石英的回收率仅为26.25%.混合矿经过一次浮选,可获得铁品位和回收率分别为50.08%和76.41%的铁精矿.R. erythropolis在赤铁矿表面发生复杂的化学吸附且使赤铁矿颗粒形成疏水絮团,从而证实R. erythropolis可作为赤铁矿的捕收剂使用.

关键词: R. erythropolis , 微生物 , 赤铁矿 , 石英 , 吸附 , 絮团 , 捕收剂

Creep rupture Behavior of K40S alloy at elevated temperatures

材料科学技术(英文)

Creep testing was conducted on K40S alloy. The detailed creep deformation and fracture mechanisms under constant load were studied. The results show that the stress exponent ranges between 7 and 14.4 at elevated temperature 973similar to1173 K, and that the activation energy is approximately 449.1 kJ/mol. During creep, the grain boundary sliding cut off primary carbides at the boundary, generating the "O" model cracks. The creep failure mode of K40S alloy is transgranular ductile and cracks originate at the primary carbides. A long carbide and matrix interface is often a preferential path for crack propagation. The creep mechanism is discussed in light of the creep microstructure, the stress exponent and the activation energy.

关键词: K40S alloy;creep;fracture;crack propagation;activation-energies;superalloy;term

Bain对应和K-S模型的数学描述

王宝奇 , 谷南驹 , 郭素珍 , 马晓莉

金属学报

利用Bain点阵对应对K-S模型的晶格改建过程进行了严密的数学描述.对于不同的马氏体正方度,提出了计算第一切变、第二切变及晶格调整的计算依据,并给出了普遍的计算公式.以Fe-1.4C和纯铁为例,计算了马氏体相变的点阵畸变.进一步分析表明,K-S模型实质是Bain模型的旋转.计算的结果与实测的取向关系相符合.

关键词: K-S模型 , null , null

Bain对应和K-S模型的数学描述

王宝奇 , 谷南驹 , 郭素珍 , 马晓莉

金属学报 doi:10.3321/j.issn:0412-1961.2002.05.006

利用Bain点阵对应对K-S模型的晶格改建过程进行了严密的数学描述.对于不同的马氏体正方度,提出了计算第一切变、第二切变及晶格调整的计算依据,并给出了普遍的计算公式.以Fe-1.4C和纯铁为例,计算了马氏体相变的点阵畸变.进一步分析表明,K-S模型实质是Bain模型的旋转.计算的结果与实测的取向关系相符合.

关键词: K-S模型 , 马氏体相变 , 点阵畸变

KⅧ-TbLⅣ离子3s3p 3P1-3s2 1S0 的自旋禁戒跃迁

牟致栋 , 魏琦瑛

原子核物理评论 doi:10.3969/j.issn.1007-4627.2004.01.015

在对KⅧ-TbLⅣ离子3s3p 3P1能级结构的多组态相互作用理论HXR方法计算的基础上, 分析了各种效应对等电子序列离子能级结构的影响, 找出了能级沿等电子序列变化的规律性. 预测计算了K Ⅷ-Tb LⅣ离子3s3p 3P1的能级. 由此进一步计算了KⅧ-TbL Ⅳ离子自旋禁戒跃迁3s3p 3P1-3s2 1S0的谱线波长、振子强度和跃迁概率.

关键词: KⅧ-TbLⅣ离子 , 自旋禁戒跃迁 , 波长 , 振子强度和跃迁概率

Fatigue crack propagation behavior of K40S cobalt-base superalloy at elevated temperature

Transactions of Nonferrous Metals Society of China

Fatigue crack propagation behavior of K40S cobalt-base superalloy under ambient atmosphere at 700 degreesC and 900 degreesC was investigated. The detailed fatigue crack propagation and fracture mechanism under the alternating loads were studied. The results show that, there is a defined threshold for K40S alloy at elevated temperatures. The fatigue threshold is 23. 9 MPa . m(1/2) at 700 degreesC and 12 MPa . m(1/2) at 900 V. The significant decrease of the threshold with increasing temperature is associated with the oxidation induced embrittlement at crack tip. Observation on the fatigue fracture surfaces indicates a ductile fracture mechanism related to the fatigue crack growth.

关键词: cobalt-base superalloy;fatigue crack propagation;fatigue threshold;ductility;growth-behavior;alloy;steel

On the low cycle fatigue deformation of K40S cobalt-base superalloy at elevated temperature

Materials Letters

Low cycle isothermal mechanical fatigue testing K40S cobalt-base superalloy was carried out at 700 and 900degreesC with total strain amplitude from +/-0.1 to +/-1.0 pct. Correlations between microscopic cyclic deformation and cycle stress response with various microstructural phenomena were enabled through scanning electron microscopy (SEM) and transmission electron microscopy (TEM), detailing the deformation substructure and carbide precipitation. The results show that K40S superalloy exhibited cyclic stress response of cyclic hardening at 700degreesC, and of initial hardening followed by softening at 900degreesC. In addition, at both temperatures, cyclic hardening during cycle deformation increased with increasing strain amplitude, while the fatigue lifetime decreased. The cyclic stress response behavior can be rationalized based on the mechanisms associated with dislocation-dislocation interactions, dislocation-precipitate (M23C6) interactions and interactions between solute atoms and dislocations. (C) 2002 Elsevier Science B.V. All rights reserved.

关键词: K40S cobalt-base alloy;isothermal cyclic deformation;cyclic stress;response;room-temperature;behavior;alloy;mechanisms

Cs-K混合蒸气中Cs(8D)+K(4S)碰撞能量转移

沈异凡 , 沈晓燕

量子电子学报 doi:10.3969/j.issn.1007-5461.2004.01.003

在Cs-K混合蒸气中,两步激发Cs原子到8D态,观察了Cs(8D)+K(4S)→Cs(5D)+K(4P)碰撞能量合并逆过程(REP,reverse energy pooling).应用双调制技术探测K(4P)原子发射的荧光,基态K原子密度用光学吸收方法测量.得到了REP速率系数,讨论了其它过程对速率系数的影响.

关键词: 光谱学 , 激发态原子 , 能量合并逆过程 , 速率系数

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