{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"为改进常规晶型和非晶型磷化膜性能的不足,以常温磷化液为基础,通过改变磷化操作工艺,利用波段操作将浸泡磷化与空气中氧化磷化相结合,将晶型磷化膜与非晶型磷化膜有机地结合为一体,制备了混晶型磷化膜,并用硫酸铜点滴试验检测了磷化膜的耐蚀性能.结果表明,混晶型磷化膜硫酸铜点滴变色时间延长了1倍左右,大大提高了磷化膜的耐蚀性能.","authors":[{"authorName":"张丕俭","id":"a2d4ce82-57ad-4626-a90e-50a34559e836","originalAuthorName":"张丕俭"},{"authorName":"胡玉才","id":"d200b0a9-cd08-4026-975e-a8f911fa9522","originalAuthorName":"胡玉才"},{"authorName":"殷平","id":"5d7db1ab-faf5-4d96-8ffd-1d9239cfb866","originalAuthorName":"殷平"},{"authorName":"刘冰","id":"719e271a-4ea6-4021-8168-be71f7275755","originalAuthorName":"刘冰"}],"doi":"","fpage":"57","id":"8f8e232a-25ad-4a9c-a50b-081e9a6fbe62","issue":"12","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"4ee31880-1834-4983-9825-0efdc209a367","keyword":"常温磷化","originalKeyword":"常温磷化"},{"id":"73cb1d9e-5ab2-44d0-a7c8-e72fcc483705","keyword":"混晶型磷化膜","originalKeyword":"混晶型磷化膜"},{"id":"4e5f8f69-44e9-438d-875a-4330d559ddb3","keyword":"氧化磷化","originalKeyword":"氧化磷化"},{"id":"c8c1f188-8a7b-40ed-99c5-c39455132d1a","keyword":"耐蚀性能","originalKeyword":"耐蚀性能"}],"language":"zh","publisherId":"clbh200812018","title":"混晶型磷化膜的制备及其耐蚀性能","volume":"41","year":"2008"},{"abstractinfo":"根据磷化工艺中各项指标的相互关系,确定了低温磷化基础液配方,并研制出稳定、无氯积累,在低温下具有高加速性能的加速性以及晶粒细化剂、磷化液稳定剂.","authors":[{"authorName":"曾伟珍","id":"ab6cabd1-bda3-48ff-8cdc-16de2090abb7","originalAuthorName":"曾伟珍"}],"doi":"10.3969/j.issn.1001-3660.2001.04.015","fpage":"41","id":"e500852d-ac61-4ef1-b7a8-fd635cdef387","issue":"4","journal":{"abbrevTitle":"BMJS","coverImgSrc":"journal/img/cover/BMJS.jpg","id":"3","issnPpub":"1001-3660","publisherId":"BMJS","title":"表面技术 "},"keywords":[{"id":"d2ac2330-6edb-48b0-86d5-4569e28c807f","keyword":"低温","originalKeyword":"低温"},{"id":"739d9c8f-e5e4-4e02-9fbe-7a0e18d50ed9","keyword":"磷化","originalKeyword":"磷化"},{"id":"c42de111-296f-43de-a156-2460accc6682","keyword":"基础配方","originalKeyword":"基础配方"},{"id":"9e4c5fe6-c839-4ed2-af9e-01fb9ee4bb07","keyword":"促进剂","originalKeyword":"促进剂"},{"id":"33f30606-88a5-4baa-9f5c-964086ce6a90","keyword":"稳定剂","originalKeyword":"稳定剂"},{"id":"80f16bc0-88e5-4249-9722-ddc9f1b32c65","keyword":"细化剂","originalKeyword":"细化剂"}],"language":"zh","publisherId":"bmjs200104015","title":"低温微晶薄膜型磷化液研究","volume":"30","year":"2001"},{"abstractinfo":"有关高酸度磷化液的成膜机理目前尚无定论,作者通过对高酸度磷化液进行反复的实验,主要从时间、温度、促进剂等因素对高酸度磷化液所形成的磷化膜的耐蚀性的影响进行了讨论,并在此基础上初步探讨了高酸度磷化液的成膜机理, 形成的磷化膜为非晶型的磷酸铁盐.","authors":[{"authorName":"张圣麟","id":"169f7485-7864-475d-8ade-100a27a8fae7","originalAuthorName":"张圣麟"},{"authorName":"李红玲","id":"e5b49b5b-e6d4-40e1-b31d-91cec1d765dd","originalAuthorName":"李红玲"},{"authorName":"郑洪河","id":"70037abe-ac14-4b7c-b9c2-5bf8477d20e9","originalAuthorName":"郑洪河"},{"authorName":"常照荣","id":"fe2e0ac9-19e4-4ac4-bad2-8b5ee1d38481","originalAuthorName":"常照荣"}],"doi":"10.3969/j.issn.1001-3660.2005.05.022","fpage":"70","id":"08d50ca4-4ee5-44f4-8f77-28b12777c552","issue":"5","journal":{"abbrevTitle":"BMJS","coverImgSrc":"journal/img/cover/BMJS.jpg","id":"3","issnPpub":"1001-3660","publisherId":"BMJS","title":"表面技术 "},"keywords":[{"id":"bfa5d1c9-8c2f-4d34-8b6b-5097b6db8707","keyword":"磷化处理","originalKeyword":"磷化处理"},{"id":"b8b1a3da-79ea-4aa5-8597-7a450fdebb43","keyword":"高酸度处理","originalKeyword":"高酸度处理"},{"id":"0a36764e-8a4d-4972-b1ad-c9ef472a3971","keyword":"机理","originalKeyword":"机理"},{"id":"6cac4dd8-1a7f-4742-8962-8c3cf734ddea","keyword":"促进剂","originalKeyword":"促进剂"},{"id":"b6ee623e-fcc6-4863-8bcb-d7a9f5a7c741","keyword":"耐蚀性","originalKeyword":"耐蚀性"},{"id":"0a1ad709-0abf-471d-aa9f-c3f42bd987c2","keyword":"磷化液","originalKeyword":"磷化液"},{"id":"5669425a-f1e4-493a-b7c7-78fd7a5dd788","keyword":"磷化膜","originalKeyword":"磷化膜"},{"id":"5da3e804-068b-4edf-bc00-ddd2dc23deb2","keyword":"成膜","originalKeyword":"成膜"}],"language":"zh","publisherId":"bmjs200505022","title":"高酸度磷化液成膜机理探讨","volume":"34","year":"2005"},{"abstractinfo":"采用均相沉淀法在95℃、常压条件下制备了金红石/锐钛混晶型纳米TiO2混悬液.研究了pH对产物晶型和晶化时间对混悬液光催化能力的影响,以及混悬液的贮存稳定性.用X射线衍射仪(XRD)测试了混晶的晶相组成;用透射电子显微镜(TEM)分析了混晶的形貌;用激光粒度仪测定了混晶的粒径.结果表明,加盐酸至pH=0.5,晶化5h制得的混悬液光催化活性良好,贮存稳定.混晶中含锐钛型72.7%,金红石型27.3%,形貌为15nm×5nm左右的长条形.","authors":[{"authorName":"季金苟","id":"a639d301-004c-41f3-b6c8-ab7e62e018f5","originalAuthorName":"季金苟"},{"authorName":"石朝辉","id":"4e90549d-658d-4590-9a99-d1d478a37aca","originalAuthorName":"石朝辉"},{"authorName":"郭静","id":"2bd5f588-d003-4724-91f8-1c0b3e4abf87","originalAuthorName":"郭静"},{"authorName":"楚莎莎","id":"2d00b3f2-947d-4ee2-bc72-8f6eb028bb19","originalAuthorName":"楚莎莎"},{"authorName":"于凯","id":"7bdcce46-ae7d-4ecc-b275-90e6e6b4f56f","originalAuthorName":"于凯"}],"doi":"","fpage":"29","id":"a5a5cac0-62b3-453c-a343-16c85b1599a8","issue":"14","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"be585663-b4d8-461b-8a95-a82c6e12aebf","keyword":"均相沉淀法","originalKeyword":"均相沉淀法"},{"id":"e9672f04-ebf3-4fbe-b41a-62521da02765","keyword":"混晶型","originalKeyword":"混晶型"},{"id":"5104f73c-87a8-45d8-9882-6e46bdf46920","keyword":"纳米二氧化钛","originalKeyword":"纳米二氧化钛"},{"id":"b8f94764-bded-4cbe-8a26-e94e6c6304c9","keyword":"光催化","originalKeyword":"光催化"}],"language":"zh","publisherId":"cldb201214008","title":"混晶型纳米二氧化钛混悬液的制备及其光催化性能","volume":"26","year":"2012"},{"abstractinfo":"Q235钢铁试片在以磷酸、钼酸铵等组成的铁系磷化液中常温快速磷化后,自然干燥8 h以上,生成了免水洗的彩色磷化膜.用SEM和EDS对磷化膜进行形貌和元素含量分析.结果表明:免水洗的磷化膜由Fe3+的氧化物、磷酸盐及少量的钼酸盐等组成,膜晶粒尺寸≤3μm,膜连续、致密,膜重约O.8 g/m2,耐3%的NaCl溶液腐蚀约2 h以上,喷涂铁红环氧底漆后附着力达1级.","authors":[{"authorName":"黎成勇","id":"c6c60cfb-c37b-47d6-aade-adc0495402bf","originalAuthorName":"黎成勇"},{"authorName":"余取民","id":"69dfc853-bb59-4048-9b87-e878122aa46d","originalAuthorName":"余取民"},{"authorName":"刘琳琪","id":"85387fbf-5aa9-4443-ba78-de477b9ba8fa","originalAuthorName":"刘琳琪"}],"doi":"10.3969/j.issn.1001-3660.2010.02.021","fpage":"67","id":"8eeaab8a-1d28-4a80-9d98-d9b2543f8435","issue":"2","journal":{"abbrevTitle":"BMJS","coverImgSrc":"journal/img/cover/BMJS.jpg","id":"3","issnPpub":"1001-3660","publisherId":"BMJS","title":"表面技术 "},"keywords":[{"id":"c0778d0a-1678-4cb0-a656-d8a16e797ecb","keyword":"铁系磷化膜","originalKeyword":"铁系磷化膜"},{"id":"4de76153-d311-42a8-b486-119a574324d3","keyword":"表面处理","originalKeyword":"表面处理"},{"id":"334c849e-7523-4241-8aa8-0fb8412cac8f","keyword":"常温","originalKeyword":"常温"}],"language":"zh","publisherId":"bmjs201002021","title":"清洁型铁系磷化膜的常温制备与表征","volume":"39","year":"2010"},{"abstractinfo":"用DSC法研究了聚甲醛(POM)和聚醚型聚氨酯(PEU)共混体系的溶混性,WAXD分析表明,PEU未能进入POM的晶胞及晶粒中,两者仅在POM的无定形区域形成可溶混结构,且POM的(110)晶面法向微晶粒尺寸110是随组分的增加而增大的.","authors":[{"authorName":"姚日生","id":"82336542-63b8-4bc8-8370-d381f570121f","originalAuthorName":"姚日生"},{"authorName":"边侠玲","id":"0231e825-69f5-41a5-9f17-17995528f6f7","originalAuthorName":"边侠玲"}],"doi":"","fpage":"100","id":"6c262a3e-d76e-4a9e-9725-50b52df6d47e","issue":"1","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"0a879b62-b6b1-4238-b42c-b2a14d6dbb34","keyword":"聚甲醛","originalKeyword":"聚甲醛"},{"id":"b4eda56a-ea78-4e20-9f45-0e6c5e5e7150","keyword":"聚醚型聚氨酯","originalKeyword":"聚醚型聚氨酯"},{"id":"e7cdf82d-0a41-4e7b-b881-7c3ddb867a6f","keyword":"溶混性","originalKeyword":"溶混性"},{"id":"8a916357-4a6b-4b74-a9f6-f7eaad3b8960","keyword":"微晶","originalKeyword":"微晶"}],"language":"zh","publisherId":"gfzclkxygc199901027","title":"聚甲醛/聚醚型聚氨酯共混体系的溶混性及微晶结构","volume":"","year":"1999"},{"abstractinfo":"0前言\n不锈钢在自然状态下表面会生成一层薄而致密、附着牢而透明的钝化膜,起不到长时间的防腐蚀作用,磷化前必须除去。去除这层自然钝化膜,费工费时,又会增加生产成本。本工作找到了一种能有效去除其自然钝化膜的方法,且又不损害基体;对其改进磷化后磷化膜由大小不等的片状或针状晶体组成,","authors":[{"authorName":"杨改航","id":"ca482451-ceb2-4ccc-ab8e-0261b18c70b8","originalAuthorName":"杨改航"}],"doi":"","fpage":"63","id":"c937570f-6ee0-4688-9dad-786cc4fbe34a","issue":"10","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"a829dbf0-4e05-4ccc-9715-77549d2be832","keyword":"自然状态","originalKeyword":"自然状态"},{"id":"7799f3cf-417c-4e1d-b2bf-2a97498fb676","keyword":"钝化膜","originalKeyword":"钝化膜"},{"id":"6b8f31c8-278e-4b81-965d-f4b6bd4e5c0e","keyword":"磷化膜","originalKeyword":"磷化膜"},{"id":"3b0986ee-16b8-4b12-bd80-39114d1daefb","keyword":"不锈钢","originalKeyword":"不锈钢"},{"id":"df7b54dc-eac9-40c7-a586-b734e2a37d57","keyword":"改进型","originalKeyword":"改进型"},{"id":"4983c212-8541-473e-bbd6-26e9fffa81ec","keyword":"防腐蚀作用","originalKeyword":"防腐蚀作用"},{"id":"c5e16d52-4961-4a42-bf76-2c1ca146f54f","keyword":"生产成本","originalKeyword":"生产成本"},{"id":"0a92befb-ede7-48e8-bb41-3bfd2c46e887","keyword":"体组成","originalKeyword":"体组成"}],"language":"zh","publisherId":"clbh201210021","title":"不锈钢自然钝化膜的去除及改进型磷化效果","volume":"45","year":"2012"},{"abstractinfo":"为了研究一种中温黑色磷化工艺,借助金相显微镜和扫描电镜对磷化膜的结构和形貌进行表征.黑色磷化膜表调后的厚度为6μm,其厚度为表调前传统磷化膜的1/3左右.通过表调也可使磷化膜均匀、致密,耐蚀性得到明显提高.硫酸铜点滴腐蚀时间是国家标准的4倍,氯化钠浸渍达72h.结果得到了一种成本低廉、无沉渣、无毒、膜黑的工业生产型磷化液.此工艺可以满足工业化批量生产要求.","authors":[{"authorName":"王建胜","id":"440fc885-a25c-4dbf-a22e-2d9d47c0e3a9","originalAuthorName":"王建胜"},{"authorName":"刘力拓","id":"04f5bd1b-15f6-45ec-81d3-f878899f6b24","originalAuthorName":"刘力拓"}],"doi":"10.3969/j.issn.1001-3660.2008.01.023","fpage":"64","id":"bc22771a-c8bc-474c-971e-7c8e565b519f","issue":"1","journal":{"abbrevTitle":"BMJS","coverImgSrc":"journal/img/cover/BMJS.jpg","id":"3","issnPpub":"1001-3660","publisherId":"BMJS","title":"表面技术 "},"keywords":[{"id":"6a2b5844-c656-4795-a8a9-516edd0c1cfe","keyword":"磷化处理","originalKeyword":"磷化处理"},{"id":"15d8d65a-d30e-4b56-92de-45e53e8195a4","keyword":"中温","originalKeyword":"中温"},{"id":"f7f3d0e7-1970-42c9-abaf-19b547762203","keyword":"黑色,金相显微镜","originalKeyword":"黑色,金相显微镜"},{"id":"ad62e853-6993-47bb-ad45-7c595200954a","keyword":"SEM","originalKeyword":"SEM"},{"id":"c1ad12ed-e41d-4fb7-965d-547f38c52429","keyword":"发黑工艺","originalKeyword":"发黑工艺"}],"language":"zh","publisherId":"bmjs200801023","title":"中温黑色磷化膜的研究","volume":"37","year":"2008"},{"abstractinfo":"指出磷化膜的外观会受磷化喷淋设备的影响,阐明了磷化膜的点状、条状、发蓝、发黄等缺陷与磷化液流量、压力、喷淋状态诸因素的关系,提出喷淋磷化设备设计或改造时管道或喷嘴的合理分布意见,并介绍了喷淋磷化设备维护方面的几点经验.","authors":[{"authorName":"王戈","id":"f7a80d80-013c-4802-a022-b54eff9f91f4","originalAuthorName":"王戈"},{"authorName":"熊力","id":"df341518-fab0-4a14-bc9f-fa5e75cce894","originalAuthorName":"熊力"}],"doi":"10.3969/j.issn.1001-3849.2000.05.008","fpage":"27","id":"f4056807-4e34-4d46-b017-ea0b850912a1","issue":"5","journal":{"abbrevTitle":"DDYJS","coverImgSrc":"journal/img/cover/DDYJS.jpg","id":"20","issnPpub":"1001-3849","publisherId":"DDYJS","title":"电镀与精饰 "},"keywords":[{"id":"1646aec2-6a36-4dac-9056-c9d6525045bb","keyword":"磷化膜","originalKeyword":"磷化膜"},{"id":"beee69d4-3ffd-45d0-823e-f4ef5d177ac5","keyword":"喷淋设备","originalKeyword":"喷淋设备"},{"id":"a20eacca-f598-47cc-bbab-f01e62dab3a9","keyword":"外观","originalKeyword":"外观"}],"language":"zh","publisherId":"ddjs200005008","title":"磷化膜外观与喷淋磷化设备关系的探讨","volume":"22","year":"2000"},{"abstractinfo":"为使磷化实现清洁生产,开发了一种用于钢铁表面涂装前处理的清洁型常温锌系磷化液,实现了磷化液的所有分子均能参加成膜反应且产物为磷化膜、水、沉渣或在磷化膜干燥过程中挥发的设计思路.该磷化液不含亚硝酸盐、重金属(除锌外),在3~40℃下快速磷化可生成膜重≥0.90g/m2、耐CuSO4溶液点滴时间达160 s的彩色磷化膜.磷化前免表面调整,磷化后免水洗.","authors":[{"authorName":"余取民","id":"fc0d8684-a256-4d40-954c-d56acb60cf21","originalAuthorName":"余取民"}],"doi":"10.3969/j.issn.1001-1560.2006.05.009","fpage":"26","id":"2feb1e91-fc57-4275-8fc7-8c505345c88d","issue":"5","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"fb8f0054-67bb-46e0-926b-6f7c603cd444","keyword":"锌系磷化液","originalKeyword":"锌系磷化液"},{"id":"5e5b5d55-973a-47b6-9258-d37443b3e938","keyword":"清洁磷化","originalKeyword":"清洁磷化"},{"id":"0856f725-2f2a-435c-9f38-dff39584efba","keyword":"表面处理","originalKeyword":"表面处理"}],"language":"zh","publisherId":"clbh200605009","title":"清洁型常温锌系磷化液研究","volume":"39","year":"2006"}],"totalpage":5914,"totalrecord":59140}