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Microstructure Characteristics of an FeMnC TWIP Steel After Deformation

DAI Yongjuan , TANG Di , MI Zhenli , L Jianchong

钢铁研究学报(英文版)

Abstract: The present paper investigated deformatiom microstructure characteristcsl of the Fe-Mn-C TWIP steel .The results showed that the hot rolled – cold rolled - annealed sample of Fe-Mn-C TWIP steels has excellent mechanical properties, the true stress-strain curve from tension tests exhibit repeated serrations. The deformed microstructure exhibited the typical planar glide characteristics such as no cell formation, dislocation pile ups on a single slip plane, mechanical twins and stacking faults. There are equiaxial and deep dimple structures in the fractograph, it is a typical ductile fracture. microcrack initiated from inclusions and twin-twin intersections, Its deformation and mfracture processes were the formation, growth and coalescence of microvoids. Because of high amount of anganese, there are many inclusions of strip MnS, the quantity of sulphur should be controlled during steelmaking.

关键词: planar glide;deformed twinning;stack fault energy;ductile fracture

Mechanical Property and Microstructural Characterization of C-Mn-Al-Si Hot Dip Galvanizing TRIP Steel

JIANG Hai-tao , DING Wei , TANG Di , HUANG Wei

钢铁研究学报(英文版)

Mechanical properties and microstructure in high strength hot dip galvanizing TRIP steel were investigated by optical microscope (OM), transmission electron microscope (TEM), X-ray diffraction (XRD), dilatometry and mechanical testing. On the heat treatment process of different intercritical annealing (IA) temperatures, isothermal bainitic transformation (IBT) temperatures and IBT time, this steel shows excellent mechanical properties with tensile strength over 780 MPa and elongation more than 22%. IBT time is a crucial factor in determining the mechanical properties as it confirms the bainite transformation process, as well as the microstructure of the steel. The microstructure of the hot dip galvanizing TRIP steel consisted of ferrite, bainite, retained austenite and martensite during the short IBT time. The contents of ferrite, bainite, retained austenite and martensite with different IBT time were calculated. The results showed that when IBT time increased from 20 to 60 s, the volume of bainite increased from 14.31% to 16.95% and the volume of retained austenite increased from 13.64% to 16.28%; meanwhile, the volume of martensite decreased from 7.18% to 1.89%. Both the transformation induced plasticity of retained austenite and the hardening of martensite are effective, especially, the latter plays a dominant role in the steel containing 7.18% martensite which shows similar strength characteristics as dual-phase steel, but a better elongation. When martensite volume decreases to 1.89%, the steel shows typical mechanical properties of TRIP, as so small amount of martensite has no obvious effect on the mechanical properties.

关键词: TRIP steel , isothermal bainitic transformation , martensite , mechanical property

Process Simulation and Microstructure Analysis of Low Carbon SiMn Quenched and Partitioned Steel

ZHAO Cai , TANG Di , JIANG Haitao , ZHAO Songshan , LI Hui

钢铁研究学报(英文版)

The quenching and partitioning (Q&P) process was experimentally investigated on the thermomechanical simulator (Gleeble3800). The microstructure and fracture mechanism of the sheets were investigated by means of TEM. It was found that the microstructure of quenched and partitioned steel consists of fine lath martensite and thin interlath austenite films. The optimum quenching temperature of producing the maximum amount of retained austenite after final quenching at room temperature was predicted by Matlab software package. It was found that the calculations by Matlab software can provide guidance for experimental processing design reliably. The volume fraction of retained austenite at room temperature was approximately 8%, which was measured easily by the software VC60++ programming. The results verified that quenched and partitioned steel possesses a good combination of strength and plasticity due to its fine microstructure. This steel exhibited high ultimate tensile strength (exceeding 1 000 MPa) and good elongation of 25%. The results showed that the fracture mechanism of the sheets is typical tough fracture under the condition of tensile failure.

关键词: Q&P;Matlab software;microstructure;mechanical property

Effect of Heating Rate Before Tempering on Reversed Austenite in Fe-9Ni-C Alloy

ZHANG Kun , TANG Di , WU Hui-bin

钢铁研究学报(英文版)

The alloy was reheated to 580 ℃ for tempering at rates of 2, 5, 10, 20, and 40 ℃/s, respectively, after quenching. The amount, distribution, and stability of reversed austenite were investigated by X-ray diffraction (XRD) and electron back scatter diffraction (EBSD). The microstructure and cryogenic impact energy were studied by scanning electron microscope (SEM), transmission electron microscope (TEM) and Charpy V-notch (CVN) tests. The results showed that when the sample was heated at 10 ℃/s, the volume fraction of reversed austenite exhibited maximum of 8%; the reversed austenite was uniform along all kinds of boundaries; the reversed austenite contained higher concentration of carbon which enabled it to be more stable. The cryogenic toughness of the alloy was greatly improved when heated at 10 ℃/s, as the fracture surface observation showed that it mainly fractured in ductile rupture mode, which was consistent with the results of cryogenic impact energy.

关键词: 9Ni steel , heating rate , reversed austenite , cryogenic toughness

High Temperature Deformation Behavior of Fe-9Ni-C Alloy

ZHANG Kun , WU Hui-bin , TANG Di

钢铁研究学报(英文版)

The high temperature deformation behavior of the 9Ni steel has been studied by the Gleeble-3500 tester. The relationship between deformation resistance and deformation degree, deformation temperature and deformation rate was revealed. The results show that when the deformation degree is less than 02, the deformation resistance increases by about 70 to 200 MPa, while the deformation degree varied between 02 and 04, the deformation resistance increases by about 30-40 MPa, when the deformation degree is larger than 04, the deformation resistance increases slowly, some become stable gradually. The influence of deformation temperature on deformation resistance is larger, and deformation resistance at higher temperature is about 160 MPa smaller than at lower temperature. Higher deformation rate leads to larger deformation resistance. The deformation resistance increases about 70 to 110 MPa with the increase of the deformation rate. A new and highly accurate mathematical model of the steel was established to describe the deformation behavior during rolling.

关键词: 9Ni steel , high temperature deformation resistance , mathematical model

Deformation-induced gamma -> DI-alpha(2) phase transformation occurring in the twin-intersection region of TiAl alloys

Journal of Materials Research

Deformation-induced gamma -> DI-alpha(2) phase transformation was verified to occur in the twin-intersection region of a Ti-45Al-8Nb (at.%) alloy compressed at room temperature. High-resolution image observations of the deformation-induced DI-alpha(2) phase suggested that the orientation relationship between the DI-alpha(2) and gamma phases remained the typical one: (0001)(DI-alpha 2)//{111}(gamma), [11 (2) over bar0](DI-alpha 2)//< 101]gamma. The conversion of stacking sequence from ordered face-centered tetragonal to ordered nonequilibrium hexagonal close-packed structure was accomplished by the movement of a/6 < 11 (2) over bar] Shockley partial dislocations on every other {111}(gamma) plane. Compositional analysis based on energy dispersive spectra revealed that the DI-alpha(2) phase had the same composition as the matrix gamma phase. No compositional diffusion Occurred because the plastic deformation was carried out at room temperature. The strong stress concentration in the intersection region was the major force to induce the gamma -> DI-alpha(2) phase transformation in the process of room-temperature compression.

关键词: titanium aluminides;mechanical-properties;room-temperature;microstructure;intermetallics;microscopy;nb

DI材横向厚差自动控制算法及其应用

徐江华 , 李山青

上海金属

DI材是宝钢的重要产品,主要用于碳酸饮料罐和啤酒罐.DI材沿宽度方向的厚度均匀性要求十分严格.为了减少DI材的横向厚差,开发了横向厚差自动控制系统并应用在某冷连轧机上.该控制系统使用了基于鲁棒性能指标(robustness specification)的横向厚差自动控制算法,从而使厚度0.229 mm以下的DI材的横向厚差被控制在±4μm以内.

关键词: DI , 冷轧 , 横向厚差 , 自动控制

高速电镀锡薄钢板(DI材)用气相缓蚀剂的研究

王新葵 , 罗广求 , 李宁

腐蚀与防护 doi:10.3969/j.issn.1005-748X.2005.05.003

采用气相快速甄别实验和电化学方法研究了对高速电镀锡薄钢板(DI材)具有缓蚀作用的四种不同的物质.结果表明:苯甲酸钠、苯甲酸铵、肉桂酸对DI材的阳极过程有明显的抑制作用;单纯的钨酸钠对DI材的缓蚀效果不佳.通过正交试验发现:苯甲酸钠、苯甲酸铵、肉桂酸与钨酸钠的复配使用,表现出很好的协同作用,从而得到了一种新的环保、高效的用于DI材的气相缓蚀剂配方.

关键词: 气相缓蚀剂 , 正交实验 , 协同作用

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